• 제목/요약/키워드: phase center

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레시틴 오가노겔을 이용한 난용성 제니스테인의 용해도 향상 (Development of Lecithin Organogel to Improve Solubility of Genistein)

  • 이수진;김정아;강내규;박선규;이천구
    • 대한화장품학회지
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    • 제41권3호
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    • pp.201-208
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    • 2015
  • 오가노겔은 반고형상이며 3차원의 네트워크 구조로 이루어진 친유성 용매로 이루어져 있다. 본 연구에서는 유상과 수상에서 모두 난용성 특징을 가진 제니스테인을 포함하는 레시틴 오가노겔을 개발하였다. 이 시스템은 안정할 뿐만 아니라 경피 흡수 실험에서도 높은 흡수율을 보였다. 본 오가노겔 제형에 적합한 원료들을 선별한 결과, 수화된 레시틴, 해바라기유, dipropylene glycol (DPG), polyethylene glycol (PEG)이 이 시스템에서 주로 사용되었다. 레시틴 오가노겔의 제조에 적합한 원료의 함량은 phase ternary diagram 작성을 통하여 결정하였다. 제조된 레시틴 오가노겔을 organoleptic characteristics, stability, pH, rheology, phase transition temperatures, microscopic analysis, skin penetration 실험을 통해 평가하였다. 본 연구 결과를 통해 본 논문에서 제시하는 레시틴 오가노겔 제형은 안정한 상태에서 난용성 물질을 높은 농도로 피부에 효과적으로 전달할 수 있는 제형으로 활용될 수 있을 것이라 생각된다.

위상변화를 이용한 표면탄성파 가스센서 (Surface acoustic wave gas sensors by utilizing the phase change)

  • 김진상;정용철;강종윤;김달영;남창우;윤석진
    • 센서학회지
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    • 제14권3호
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    • pp.186-190
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    • 2005
  • This paper describes the development of a surface acoustic wave gas sensor that is designed to detect volatile gas by monitering phase change of output signal as a function of time. The sensor consists of SAW oscillators with a center frequency of 100 MHz fabricated on $128^{\circ}$ Y-Z $LiNbO_{3}$ substrates. Experimental results, which show the phase change of output signal under the absorption of volatile gas onto sensors, are presented. The proposed sensor has the properties of high sensitivity compare to the conventional SAW gas sensor and chemical selectivity. Thus, it is thought these results are applicable for use in sensor array of an high performance electronic nose system.

Comparative Genome-Scale Expression Analysis of Growth Phase-dependent Genes in Wild Type and rpoS Mutant of Escherichia coli

  • Oh, Tae-Jeong;Jung, Il-Lae;Woo, Sook-Kyung;Kim, Myung-Soon;Lee, Sun-Woo;Kim, Keun-Ha;Kim, In-Gyu;An, Sung-Whan
    • 한국미생물생명공학회:학술대회논문집
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    • 한국미생물생명공학회 2004년도 Annual Meeting BioExibition International Symposium
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    • pp.258-265
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    • 2004
  • Numerous genes of Escherichia coli have been shown to growth phase-dependent expression throughout growth. The global patterns of growth phase-dependent gene expression of E. coli throughout growth using oligonucleotide microarrays containing a nearly complete set of 4,289 annotated open reading frames. To determine the change of gene expression throughout growth, we compared RNAs taken from timecourses with common reference RNA, which is combined with equal amount of RNA pooled from each time point. The hierarchical clustering of the conditions in accordance with timecourse expression revealed that growth phases were clustered into four classes, consistent with known physiological growth status. We analyzed the differences of expression levels at genome level in both exponential and stationary growth phase cultures. Statistical analysis showed that 213 genes are shown to, growth phase-dependent expression. We also analyzed the expression of 256 known operons and 208 regulatory genes. To assess the global impact of RpoS, we identified 193 genes coregulated with rpoS and their expression levels were examined in the isogenic rpoS mutant. The results revealed that 99 of 193 were novel RpoS-dependent stationary phase-induced genes and the majority of those are functionally unknown. Our data provide that global changes and adjustments of gene expression are coordinately regulated by growth transition in E. coli.

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Nanotubular Structure Formation on Ti-6Al-4V and Ti-Ta Alloy Surfaces by Electrochemical Methods

  • Lee, Kang;Choe, Han-Cheol;Ko, Yeong-Mu;Brantley, W.A.
    • 대한금속재료학회지
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    • 제50권2호
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    • pp.164-170
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    • 2012
  • Nanotubular structure formation on the Ti-6Al-4V and Ti-Ta alloy surfaces by electrochemical methods has been studied using the anodizing method. A nanotube layer was formed on Ti alloys in 1.0 M $H_3PO_4$ electrolyte with small additions of $F^-$ ions. The nanotube nucleation and growth of the ${\alpha}$-phase and ${\beta}$-phase appeared differently, and showed different morphology for Cp-Ti, Ti-6Al-4V and Ti-Ta alloys. In the ${\alpha}$-phase of Cp-Ti and martensite ${\alpha}^{\prime}$ and in the ${\alpha}^{{\prime}{\prime}}$ and ${\beta}$-phase of the Ti-Ta alloy, the nanotube showed a clearly highly ordered $TiO_2$ layer. In the case of the Ti-Ta alloy, the pore size of the nanotube was smaller than that of the Cp-Ti due to the ${\beta}$-stabilizing Ta element. In the case of the Ti-6Al-4V alloy, the ${\alpha}$-phase showed a stable porous structure; the ${\beta}$-phase was dissolved entirely. The nanotube with two-size scale and high order showed itself on Ti-Ta alloys with increasing Ta content.

Si(100) wafer와 SiO2/Si(100) 기판에 동시 스퍼터링법으로 증착된 NiFe 합금 박막의 상변화 및 자기적 특성 (Phase transformation and magnetic properties of NiFe thin films on Si(100) wafer and SiO2/Si(100) substrate by co-sputtering)

  • 강대식;송종한;남중희;조정호;전명표
    • 한국결정성장학회지
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    • 제20권5호
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    • pp.216-220
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    • 2010
  • Si(100) wafer와 $SiO_2$/Si(100) 웨이퍼에 증착된 NiFe 합금 박막의 결정상과 자기적 특성을 비교하고자 동시 스퍼터링법을 이용하여 두 기판 위에 150 nm의 박막을 제조하여 그의 상변화와 자기적 특성을 XRD, FE-SEM, VSM으로 비교하였다. 두 기판 위에 증착된 NiFe 박막은 BCC상으로 증착되었으나 $400^{\circ}C$에서 2시간 열처리를 한 결과 BCC에서 FCC로의 상전이가 일어나는 것을 관찰 할 수 있었으며 Si(100) wafer위에 증착된 박막에서는 $500^{\circ}C$에서 열처리 후에도 BCC와 FCC가 혼재하여 나타나는 것을 알 수 있었다. $450^{\circ}C$에서 열처리 하였을 때 각형비가 가장 높았으며 포화자화는 0.0118 emu로 나타나고 있었다. $500^{\circ}C$ 이상의 온도에서는 상전이로 인해 포화자화가 급격히 감소하는 것을 볼 수 있었다.

다상 BLDC 모터 드라이브 시스템의 개방 고장 시 효율 향상이 고려된 토크 리플 저감 대책 (Torque Ripple Reduction Method With Enhanced Efficiency of Multi-phase BLDC Motor Drive Systems Under Open Fault Conditions)

  • 김태윤;서용석;박현철
    • 전력전자학회논문지
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    • 제27권1호
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    • pp.33-39
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    • 2022
  • A multi-phase brushless direct current (BLDC) motor is widely used in large-capacity electric propulsion systems such as submarines and electric ships. In particular, in the field of military submarines, the polyphaser motor must suppress torque ripple in various failure situations to reduce noise and ensure stable operation for a long time. In this paper, we propose a polyphaser current control method that can improve efficiency and reduce torque ripple by minimizing the increase in stator winding loss at maximum output torque by controlling the phase angle and amplitude of the steady-state current during open circuit failure of the stator winding. The proposed control method controls the magnitude and phase angle of the healthy phase current, excluding the faulty phase, to compensate for the torque ripple that occurs in the case of a phase open failure of the motor. The magnitude and phase angle of the controlled steady-state current are calculated for each phase so that copper loss increase is minimized. The proposed control method was verified using hardware-in-the-loop simulation (HILS) of a 12-phase BLDC motor. HILS verification confirmed that the increase in the loss of the stator winding and the magnitude of the torque ripple decreased compared with the open phase fault of the motor.

위상 기반 사차원전산화단층촬영과 진폭 기반 사차원전산화단층촬영 영상에서의 위상차 평가 (Evaluation of difference in respiratory phase between amplitude- and phase-based four-dimensional computed tomography)

  • 이소향;박수연;김종식;최병기;박희철;정상훈
    • 대한방사선치료학회지
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    • 제27권1호
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    • pp.73-78
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    • 2015
  • 목 적 : 본 연구는 위상 기반 방식으로 배열 된 사차원 전산화 단층 촬영 영상(4DCT, 4-dimensional computed tomography)를 이용하여 진폭 기반 방식으로의 재구성 하였을 때의 위상 차이를 분석하였다. 대상 및 방법 : 2015년 02월부터 03월 까지 호흡동조 방사선 치료를 받은 간암 환자 10명의 사차원 전산화 단층 촬영 영상을 대상으로 분석 하였다. RPM respiratory gating (RPM 1.7.5, Varian, USA)장치를 이용하여 위상 기반 배열 방식의 호흡주기별 영상을 획득 하였으며, 획득된 호흡 주기별 영상은 치료계획시스템(Pinnacle 9.2, Philips, USA)을 이용하여 호흡주기별 복부의 움직임 값을 측정하였다. 최대 호기(50%)와 최대 흡기(0%)에서의 복부 움직임을 진폭으로 하여 10개 위상의 진폭 기반 호흡위상을 재구성하고, 이를 위상 기반 사차원영상촬영영상의 호흡 위상과 비교하였다. 결 과 : 위상 기반 및 진폭 기반 사차원단층촬영영상으로 재구성한 영상에서의 위상 차이는 최대 30% 호흡위상에서 확인할 수 있었으며, 30% 호흡 위상에서 평균 0.13 cm (최대 0.24 cm)의 위치 차이를 확인할 수 있었고, 동일 측정 점 위치가 가지는 위상차는 30% 위상에서 평균 8.7%(최대 16.5%)의 위상차를 확인하였다. 전체 호흡 구간에서 평균 위치 차이는 0.4 cm, 평균 위상 차이는 13.0% 임을 확인하였다. 결 론 : 본 연구 결과는 위상 기반 방식으로 배열된 4DCT 영상을 진폭 기반 방식으로의 변환하였을 때 계산 값과 실측값을 분석한 결과 최대 16.5% 의 위상차가 발생함을 확인하였다.

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Simultaneous Control of Phase Transformation and Crystal of Amorphous TiO2 Coating on MWCNT Surface

  • Cha, Yoo Lim;Park, Il Han;Moon, Kyung Hwan;Kim, Dong Hwan;Jung, Seung Il;Yoon, Young Soo
    • 한국세라믹학회지
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    • 제55권6호
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    • pp.618-624
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    • 2018
  • We developed a mass production method that simultaneously controls the phase transformation and crystal size of $TiO_2$ coatings on multiwalled carbon nanotubes (MWCNTs). Initially, MWCNTs were successfully coated with amorphous 15-20-nm-thick $TiO_2$ by an in-situ sol-gel method. As the calcination temperature increased in both air and argon atmospheres, the amorphous $TiO_2$ was gradually transformed into the fully anatase phase at approximately $600^{\circ}C$, a mixture of the anatase and rutile phases at approximately $700^{\circ}C$, and the fully rutile phase above approximately $800^{\circ}C$. The crystal size increased with increasing calcination temperature. Moreover, above $600^{\circ}C$, the size of crystals formed in air was approximately twice that of crystals formed in argon. The reason is thought to be that MWCNTs, which continuously supported the stresses associated with the reconstructive phase transformation, disappeared owing to complete oxidation in air at these high temperatures.

다양한 산소분압에서 소결한 NdBCO 초전도체의 열적 안정성 (Thermal Stability of Superconductor NdBCO Sintered at Various Oxygen Partial Pressures)

  • 정준기;김원정;박성창;강성구;임영진;김철진
    • Progress in Superconductivity
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    • 제10권2호
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    • pp.133-138
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    • 2009
  • The $Nd_{1+x}Ba_{2-x}Cu_3O_{7-{\delta}}$(Nd123) superconductor exhibits high performance in high magnetic field and high temperature. We have studied phase stability for Nd123 under reduced oxygen partial pressure and various heat-treatment conditions. The main phase is Nd123 and some samples contain small amounts of Nd422 depending on the temperature and oxygen partial pressure. The decomposition temperature decreases with decreasing oxygen partial pressure from $1052^{\circ}C(P(O_2)$=150 Torr) to about $845^{\circ}C(P(O_2)$=0.1 Torr). The liquidus line was steeper temperature with decreasing oxygen partial pressure. In same condition of oxygen partial pressure, the region of stable Nd123 phase was formed at slightly higher temperature than the region of stable YBCO phase.

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