• Title/Summary/Keyword: particle size control

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Effect of Grain Size on the Physicochemical & Nutritional Properties of Beef Porridge (쇠고기죽 제조 시 쌀입자 크기가 죽의 품질에 미치는 영향)

  • Kim, Hye-Ran;Kim, Min-Jee;Yang, Yun-Hyoung;Lee, Kum-Jong;Kim, Mee-Ree
    • Journal of the Korean Society of Food Culture
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    • v.25 no.1
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    • pp.70-75
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    • 2010
  • The object of this study was to investigate the effects of rice particle size on the physicochemical properties of beef-rice porridge. The pH of beef-rice porridge was decreased as compared to that of the control, while the redness of beef porridge increased according to rice particle size. The viscosity of flour in the beef-rice porridge was the highest among three porridges, at $40^{\circ}C$. The protein content of beef-rice porridge was increased 3-fold over that of rice porridges. The total amino acid content of the beef-rice porridge was 3071.2 mg/100 g, and that of rice porridge was 1147.5 mg/100 g. As compared to rice porridge, the maximum amounts of the amino acids Lys and Thr were increased beef-rice porridge. Sensory evaluation results showed that the beef-rice porridge with a particle size half that of rice had the highest scores in color, taste, texture, and overall preference. Based on these results, it is suggested that beef-rice porridge with a particle size half (0.7-2.5 mm) that of rice has optimal quality in terms of both physicochemical and sensory properties.

Research on Acceleration Mechanism of Inflight Particle and Gas Flow Effect for the Velocity Control in Vacuum Kinetic Spray Process (진공상온분사(VKS) 공정에서의 비행입자 가속 기구 및 속도제어를 위한 가스 유량 효과에 관한 연구)

  • Park, Hyungkwon;Kwon, Juhyuk;Lee, Illjoo;Lee, Changhee
    • Korean Journal of Materials Research
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    • v.24 no.2
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    • pp.98-104
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    • 2014
  • Vacuum kinetic spray(VKS) is a relatively advanced process for fabricating thin/thick and dense ceramic coatings via submicron-sized particle impact at room temperature. However, unfortunately, the particle velocity, which is an important value for investigating the deposition mechanism, has not been clarified yet. Thus, in this research, VKS average particle velocities were derived by numerical analysis method(CFD: computational fluid dynamics) connected with an experimental approach(SCM: slit cell method). When the process gas or powder particles are accelerated by a compressive force generated by gas pressure in kinetic spraying, a tensile force generated by the vacuum in the VKS system accelerates the process gas. As a result, the gas is able to reach supersonic speed even though only 0.6MPa gas pressure is used in VKS. In addition, small size powders can be accelerated up to supersonic velocity by means of the drag-force of the low pressure process gas flow. Furthermore, in this process, the increase of gas flow makes the drag-force stronger and gas distribution more homogenized in the pipe, by which the total particle average velocity becomes higher and the difference between max. and min. particle velocity decreases. Consequently, the control of particle size and gas flow rate are important factors in making the velocity of particles high enough for successful deposition in the VKS system.

Formation of Nanoparticles by Spark Discharge in Liquid (용액 내 스파크 방전을 이용한 나노입자 제조 및 특성 평가)

  • Choi, Hoomi;Kim, Jangah;Jung, Seungkyo;Yoon, Juho;Kim, Taesung
    • Particle and aerosol research
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    • v.8 no.1
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    • pp.37-43
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    • 2012
  • In this study, we designed a 'spark in liquid' system. The spark discharge between two electrodes were used to generate particles by using sufficient temperature to evaporate a part of electrodes. The power supply system provides a continuous spark discharge by discharging of the capacitor to ionize the electrodes in liquid. The DC spark discharge system operates with 1-10 kV voltage. Processed copper and graphite rods were used to both electrodes with 1-3 mm diameter. There are several variables which can control the particle size and concentration such as gap distance between electrodes, applied voltage, operating liquid temperature, electrode type and liquid type. So we controlled these variables to confirm the change of particle size distribution and concentration of particles contained in liquid as wt%. 'spark in liquid' system is expected to apply nanoink by control of concentration with analysis of characteristics.

Effects of the Addition of Metallic Salts and Polyhydric Alcohols on the Formation of Zinc Complex-compound Particle (아연 착화합물 입자형성에 미치는 금속염 및 다가알코올 첨가의 영향)

  • In, Se-Jin
    • Applied Chemistry for Engineering
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    • v.23 no.1
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    • pp.8-13
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    • 2012
  • The experiments have been performed to obtain zinc complex compound with smaller particle size, which is used as a charge control agent in manufacturing toner. Metallic salts and polyhydric alcohols have been studied to investigate their effects on the formation of different sizes of zinc complex-compound particle. Reactants such as zinc chloride and 3,5-di-tert-butyl salicylic acid have been used to form the complex compound. Polyethylene glycol (PEG-300), glycerin and ethylene glycol have been added into the zinc chloride solution beforehand to lower the reaction rate in the formation of zinc complex-compound. Zirconium (IV) oxychloride octahydrate has been mixed in the zinc chloride solution beforehand to restrain crystals from growing. When PEG-300 and zirconium (IV) oxychloride octahydrate are used to lower the reaction rate and to restrain the particle size from growing, the average particle size of zinc complex compound decreases from 5.28 to 1.84 ${\mu}m$, which is 34.9% of 5.28 ${\mu}m$.

Studies on Particle Size Control and Stability of Lead Chromate Pigment Particles (크롬산납 무기안료 입자 제어 및 안정성에 관한 연구)

  • Park, Chan Kyu;Jung, Dae Yoon;Chang, Sang Mok;Lee, Sang Rok
    • Applied Chemistry for Engineering
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    • v.19 no.3
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    • pp.264-269
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    • 2008
  • For the synthesis of lead chromate pigments, we investigated the characteristics of particle growth with reacting conditions in the synthetic process, the effect of additives, and its micro-capsulation. The more tiny and uniform dispersion particles could be obtained at a lower pH and diluter intial concentration. The variation range of average pigment size was increased with the agitating speed. The pigment size could be controlled by adding aluminum sulfate as an additive, which maintained the optimum particle dispersion. It was found that the optimum micro-capsulation conditions were pH 9~10 and above $90^{\circ}C$ during the micro-capsulation of lead chromate pigment, and below 0.5% humidity after micro-capsulation.

Particle Size Distribution of Suspended Particulates in the Atmosphere of a Seoul Residential Area (한 도시 분진의 유해성 입도 분포에 대한 조사 연구)

  • Han, Eui-Jung;Chung, Yong;Kwon, Sook-Pyo
    • Journal of Preventive Medicine and Public Health
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    • v.19 no.1 s.19
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    • pp.130-136
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    • 1986
  • The particle size of suspended particulates was measured by a Anderson air sampler from Mar. 1982 to Feb. 1984 in a part of Seoul. It was concluded as follows : 1) The arithmetic concentration of suspended particulates was $147.8{\mu}g/m^3$ in Spring, 136.9 in Summer, 131.9 in Autumn and 158.1 in Winter respectively. 2) The cumulative distribution of suspended particulates size in logarithmic diagram showed similar to normal log distribution. 3) The atmospheric particulate matters showed a bimodal size distribution on the base of unit particle concentrations, which divided at approximately $2{\mu}m$ in the diameter. 4) While the fine particulates less than $2.1{\mu}m\;was\;35.4{\sim}45.0%$, the coarse particulates was $55.0{\sim}64.5%$. 5) The higher the concentration of suspended particulates, the more increased the ratio of fine particulates. The higher the concentration of suspended particulates, the lower median size of suspended particulate as well. 6) The respirable dust particulates less than $4.7{\mu}m\;was\;52.2{\sim}62.9%$ in seasonal average through the 2 year samples. With the above result, air pollution concerned with public health could be evaluated and the control measures also are suggested.

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Effect of Precursor Alumina Particle Size on Pore Structure and Gas Permeation Properties of Tubular α-alumina Support Prepared by Slip Casting Process (초기 알루미나 분체의 입자크기가 주입성형법에 의해 제조된 튜브형 α-알루미나 지지체의 기공구조 및 기체 투과 특성에 미치는 영향)

  • Yang, Eun-Mok;Lee, Hye Ryeon;Cho, Churl-Hee
    • Membrane Journal
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    • v.26 no.5
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    • pp.372-380
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    • 2016
  • The present paper reports the effect of precursor alumina particle size on pore structure and single gas permeation properties of tubular ${\alpha}$-alumina supports, prepared by a combined process of slip casting and sintering. Pore diameter of as-prepared ${\alpha}$-alumina support was highly dependent on precursor ${\alpha}$-alumina particle size. Although, increase in the precursor particle size increases the pore diameter, but the porosity of ${\alpha}$-alumina support mainly control by sintering temperature. Sintering studies reveal that as sintering temperature increased porosity of support decreased. Single gas permeance results indicate that permence is proportional to the square of pore diameter and linearly to porosity. These dependencies revealed that gas permeation trough as-prepared ${\alpha}$-alumina support was governed by viscous flow mechanism. The present announces that precursor ${\alpha}$-alumina particle size and sintering temperature are key parameters to control gas permeantion properties of ${\alpha}$-alumina supports.

Development, validation and implementation of multiple radioactive particle tracking technique

  • Mehul S. Vesvikar;Thaar M. Aljuwaya;Mahmoud M. Taha;Muthanna H. Al-Dahhan
    • Nuclear Engineering and Technology
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    • v.55 no.11
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    • pp.4213-4227
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    • 2023
  • Computer Automated Radioactive Particle Tracking (CARPT) technique has been successfully utilized to measure the velocity profiles and mixing parameters in different multiphase flow systems where a single radioactive tracer is used to track the tagged phase. However, many industrial processes use a wide range of particles with different physical properties where solid particles could vary in size, shape and density. For application in such systems, the capability of current single tracer CARPT can be advanced to track more than one particle simultaneously. Tracking multiple particles will thus enable to track the motion of particles of different size shape and density, determine segregation of particles and probing particle interactions. In this work, a newly developed Multiple Radioactive Particle Tracking technique (M-RPT) used to track two different radioactive tracers is demonstrated. The M-RPT electronics was developed that can differentiate between gamma counts obtained from the different radioactive tracers on the basis of their gamma energy peak. The M-RPT technique was validated by tracking two stationary and moving particles (Sc-46 and Co-60) simultaneously. Finally, M-RPT was successfully implemented to track two phases, solid and liquid, simultaneously in three phase slurry bubble column reactors.

Preparation of Pt/C catalyst for PEM fuel cells using polyol process (Polyol Process를 통한 PEM Fuel Cell용 Pt/C촉매 제조)

  • Oh, Hyoung-Seok;Kim, Han-Sung
    • 한국신재생에너지학회:학술대회논문집
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    • 2006.11a
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    • pp.443-446
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    • 2006
  • Carbon-supported Platinum (Pt) is the potential electro-catalyst material for anodic and cathodic reactions in fuel cell. Catalytic activity of the metal strongly depends on the particle shape, size and distribution of the metal in the porous supportive network. Conventional preparation techniques based on wet impregnation and chemical reduction of the metal precursors often do not provide adequate control of particle size and shape. We have proposed a novel route for preparing nano sized Pt colloidal particles in solution by oxidation of ethylene glycol. These Pt nano particles were deposited on large surface area carbon support. The process of nano Pt colloid formation involves the oxidation of solvent ethylene glycol to mainly glycolic acid and the presence of its anion glycolate depends on the solution pH. In the process of colloidal Pt formation glycolate actsas stabilizer for the Pt colloidal particle and prevents the agglomeration of colloidal Pt particles. These mono disperse Pt particles in carbon support are found uniformly distributed in nearly spherical shape and the size distribution was narrow for both supported and unsupported metals. The average diameter of the Pt nano particle was controlled in the range off to 3 nm by optimizing reaction parameters. Transmission electron microscopy, CV and RRDE experiments were used to compliment the results.

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Characteristics of Powder with Change of Temperature in Production of Tantalum Powder by MR-EMR Combination Process (MR-EMR 복합공정에 의한 탄탈륨분말의 제조시 온도변화에 따른 분말의 특성)

  • 배인성;윤재식;박형호;윤동주;이민호;설경원;김병일
    • Journal of Powder Materials
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    • v.10 no.6
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    • pp.395-405
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    • 2003
  • In the conventional metallothermic reduction (MR) process for obtaining tantalum powder in batch-type operation. it is difficult to control morphology and location of deposits. On the other hand, a electronically mediated reaction (EMR) process is capable to overcome these difficulties and has a merit of continuous process, but it has the defect that the reduction yield is poor. MR-EMR combination process is a method that is able to overcome demerits of MR and EMR process. In this study, a MR-EMR combination process has been applied to the production of tantalum powder by sodium reduction of $K_2$TaF$_{7}$. The total charge passed through external circuit and average particle size (FSSS) were increased with increasing reduction temperature. The proportion of fine particle (-325 mesh) was decreased with increasing reduction temperature. The yield was improved from 65% to 74% with increasing reduction temperature. Considering the charge, impurities, morphology, particle size and yield, an reduction temperature of 1,123 K was found to be optimum temperature for MR-EMR combination process.