• Title/Summary/Keyword: particle size control

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Effect of Particle Size on the Physicochemical and Nutritional Properties of Egg Yolk Porridge (입자 크기에 따른 난황죽의 이화학적 및 영양학적 특성)

  • Kim, Hye-Ran;Kim, Mee-Ree
    • Journal of the East Asian Society of Dietary Life
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    • v.20 no.1
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    • pp.77-83
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    • 2010
  • The study was conducted to investigate the effect of particle size on the physicochemical properties of egg yolk-rice porridge. The pH of egg yolk-rice porridge was decreased when compared to that of the control, while the lightness and yellowness was increased as the rice particle size increased. The viscosity of whole particle egg yolk porridge was highest among the three porridges at $40^{\circ}C$. The protein content of the egg yolk-rice porridge was increased three-fold, when compared to that of the rice porridges. The total amino acid content of egg yolk-rice porridge was 1,500.6 mg/100 g, while that of rice was 1,147.5 mg/100 g. The Lys and Thr content of the amino acid content of egg yolk-rice porridge were also increased. Sensory evaluation results revealed that the half particle size rice egg yolk-rice porridge had the highest scores in color, taste and over-all preference. Based on these results, the half particle size egg yolk-porridge had good quality with respect to both the physicochemical and nutritional properties.

Synthesis and Particle Size Control of δ-FeOOH Using H2O2 Oxidizing Agent (H2O2 산화제를 이용한 δ-FeOOH의 합성과 입자 크기 제어)

  • Seongmin Shin;Kyunghwan Kim;Jeongsoo Hong
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.37 no.3
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    • pp.292-296
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    • 2024
  • In this study, Iron (III) oxide-hydroxide (δ-FeOOH) was successfully synthesized using hydrogen peroxide (H2O2) as an oxidizing agent. The synthesis of δ-FeOOH was carried out by controlling the amount of H2O2, and pure δ-FeOOH was successfully synthesized in ranges from 0.2 mL to 0.6 mL of H2O2. The size of the synthesized δ-FeOOH particles was compared by controlling the amount of oxidant H2O2. The average particle size of the synthesized pure δ-FeOOH particles increased from 875.1 nm to 897.2 nm as the amount of H2O2 was increased. The optical properties of δ-FeOOH synthesized under these specific conditions were investigated. All δ-FeOOH showed a similar trend of increasing and decreasing light absorption from 800 nm to 400 nm, although there was a slight difference in the amount of light absorption, with the largest amount of light absorption at 410 nm. The band gap energy of δ-FeOOH through the Tauc plot method was about 2.1~2.2 eV when H2O2 was 0.2~1.4mL. With a sufficient small particle size, simple control of that particle size, and a small band gap energy enough to absorb light in the visible spectrum, δ-FeOOH could be useful in a variety of applications, including photoelectrochemistry and battery electrodes.

Particle Sizing Using Light Scattering and Neural Networks (산란이론과 신경회로에 의한 입자크기계측)

  • 남부희;이상재;박민현;이영진;이석원;류태우;방병렬
    • Journal of Institute of Control, Robotics and Systems
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    • v.6 no.6
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    • pp.447-453
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    • 2000
  • Using the scattering theory of laser light, we analyze the particle sizing method. The scattered profile measured by the photodetector is sampled, scale conditioned by a 32 channel analog-to-digital converter, and is analyzed with the transform matrix from the light energy signals to the weights of the particle sizes. The particle size distribution is classified using the Hopfield neural network method as well as the conventional nonnegative least square method.

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The Characteristic Control of Spherical Silica Particle Using by W/O Type Emulsion(I);The analysis of Particle shape and size distribution of silica as a function mixing speed (W/O형 에멀젼을 이용한 구형 실리카 입자의 특성제어(제1보);교반속도에 따른 실리카 입자의 형태 및 입도 분석)

  • Park, Heung-Cho;Kim, Sang-Chun
    • Journal of the Korean Applied Science and Technology
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    • v.23 no.1
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    • pp.1-11
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    • 2006
  • The W/O emulsion was formed by mixing hydrophobic nonion surfactants of span 80 and tween 60 with kerosine, and by adding sodium silicate aqueous solution. Precipitating the W/O emulsion by sodium bicarbonate resulted in spherical silica particles. Shape and size distribution of silica particles were observed. The particles were spherical and they have narrow size distribution. Particle sizes were 9.29, 7.39 and $5.73\;{\mu}m$ at homogenizer speed of 2500, 3000, and 3500 rpm, respectively. The particle size was decreased by increasing agitation speed due to the formation of emulsion droplet. At fixed agitation speed, absorbed paraffin oil weight were measured and the $SiO_2/Na_2O$ mole ratio effects on particle size were investigated. Particle size was decreased by increasing the mole ratio of $SiO_2/Na_2O$.

Preparation of Ultrafine Nickel Powders by Wet Reduction Process (습식 환원법에 의한 니켈 미분말의 제조)

  • Lee, Yoon-Bok;Moon, Young-Tae;Shin, Dong-Woo;Kim, Kwang-Ho
    • Korean Journal of Materials Research
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    • v.12 no.10
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    • pp.803-808
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    • 2002
  • Nickel powders were prepared from nickel chloride solution by wet reduction process, and the size control of the particles was investigated with reactant concentration, dispersant agent, and the addition of ethanol as an organic solvent in NiCl$_2$ aqueous solution. The size of the particle decreased with the increase of nickel chloride concentration. Their average particle size were 1.9$\mu\textrm{m}$, 1.6$\mu\textrm{m}$ and $1.5\mu\textrm{m}$ with 0.5M, 0.8M and 1.0M of nickel chloride concentration respectively. The spherical particle was easily controlled by the addition of ethanol as an organic solvent. Especially, in 30 vol% of ethanol, the average particle size and specific surface area were about 0.2$\mu\textrm{m}$ and 8.98m$^2$/g, respectively.

Preparation of the Large Size Polybutadiene Latexes by Membrane Emulsification Process (막유화법을 이용한 대구경 폴리쿠타디엔 라텍스의 제조에 관한 연구)

  • 이해준;김중현
    • Membrane Journal
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    • v.6 no.3
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    • pp.166-172
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    • 1996
  • For the preparation of polybutadiene latexes with suitable particle size, membrane e$$\mu$sification, which is capable of easy and uniform control of particle size, was used in this study. The parameters were the type and amount of surfactants, amount of additive and pressure. Particle size and distribution of prepared latexes were measured and compared with those of e$$\mu$sion prepared by homogenizer. To investigate the membrane e$$\mu$sification mechanism, theoretical drop size was calculated by Harkins-Brown equation. When the amount of surfactant with more than 0.2 wt%(based on DDI water) was added in the continuous phase, the stable e$$\mu$sion was prepared. Other parameters showed little relationship with particle size and distribution. In this membrane e$$\mu$sification, the essential factor for determining the particle size was the pore size of the membrane.

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Particle Detachment in Granular Media Filtration (입상여과에서 입자물질의 탈리)

  • Kim, Jinkeun
    • Journal of Korean Society of Water and Wastewater
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    • v.18 no.5
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    • pp.673-679
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    • 2004
  • Particle breakthrough can occur by either the breakoff of previously captured particles (or flocs) or the direct passage of some influent particles through the filter. Filtration experiments were performed in a laboratory-scale filter using spherical glass beads with a diameter of 0.55 mm as collectors. A single type of particle suspension (Min-U-Sil 5, nearly pure $SiO_2$) and three different destabilization methods (pH control, alum and polymer destabilization) were utilized. The operating conditions were similar to those of standard media filtration practice: a filtration velocity of 5 m/h. To assess the possibility of particle detachment during the normal filtration, a hydraulic shock load (20% increase of flow rate) was applied after 4 hours of normal filtration. The magnitude of particle detachment was proportional to the particle size for non-Brownian particles. At the same time, less favorable particles, i.e., particles with larger surface charge, were easily detached during the hydraulic shock load. Therefore, proper particle destabilization before filtration is crucial for maximum particle removal as well as minimum particle breakthrough.

Development of Particle Deposition System for Cleaning Process Evaluation in Semiconductor Fabrication (반도체 세정 공정 평가를 위한 나노입자 안착 시스템 개발)

  • Nam, Kyung-Tag;Kim, Ho-Joong;Kim, Tae-Sung
    • Proceedings of the KSME Conference
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    • 2007.05b
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    • pp.3168-3172
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    • 2007
  • As the minimum feature size decreases, control of contamination by nanoparticles is getting more attention in semiconductor process. Cleaning technology which removes nanoparticles is essential to increase yield. A reference wafer on which particles with known size and number are deposited is needed to evaluate the cleaning process. We simulated particle trajectories in the chamber by using FLUENT and designed a particle deposition system which consists of scanning mobility particle sizer (SMPS) and deposition chamber. Charged monodisperse particles are generated using SMPS and deposited on the wafer by electrostatic force. The experimental results agreed with the simulation results well in terms of particle number and deposition area according to particle size, flow rate and deposition voltage.

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Effect of Solvent Content on Morphology and Rubber Particle Size Distribution of High Impact Polystyrene (용매 함량이 내충격성 폴리스티렌의 형태구조 및 고무 입도분포에 미치는 영향)

  • 정한균;박정신;장대석;이성재
    • Polymer(Korea)
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    • v.26 no.3
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    • pp.307-315
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    • 2002
  • Major factors affecting the impact resistance of high impact polystyrene (HIPS), the rubber-toughened grade of polystyrene, are rubber-phase particle size and size distribution, molecular weight, morphology, and degree of grafting. Accordingly, it is important to control or investigate these factors. In this study, the effect of solvent content was analyzed by the morphology and particle size distribution of rubber phase, and final properties in bulk-solution polymerization of HIPS. The prepolymerization time was, first, determined by measuring the evolution of particle size distribution of dispersed phase to explain the phase inversion with time. As the solvent content increased, the size of rubber particle increased and then gradually decreased. Rubber-phase morphology was likely to have higher degree of grafting as the solvent content increased. Rheological and mechanical properties decreased as the solvent content increased because of the decrease of matrix molecular weight due to the chain transfer reaction to solvent and the existence of residual solvent. Nevertheless, the impact resistance seemed to increase when the rubber particle size increased.

Decreasing Particle Size of (+)-Dihydromyricetin Using Hydrophilic Polymer in Fractional Precipitation (분별침전에서 친수성 고분자 물질을 이용한 (+)-dihydromyricetin의 입자크기 감소)

  • Ji, Seong Bin;Kim, Jin-Hyun
    • Korean Chemical Engineering Research
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    • v.56 no.3
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    • pp.370-375
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    • 2018
  • In this study, we have applied fractional precipitation with hydrophilic polymer in order to decrease the particle size of the (+)-dihydromyricetin from plant materials. When compared with the case where no hydrophilic polymer was employed, the addition of hydrophilic polymer in fractional precipitation resulted in a considerable decrease in the size of the (+)-dihydromyricetin precipitate. Among the polymers used, HPMC 2910 was the most effective for inhibition of precipitate growth. A polymer concentration of 0.1% (w/v) yielded the smallest particle size. The particle size was reduced by ~40% compared to control. In addition, the precipitate size was inversely correlated with the absolute value of the zeta potential of the suspension with polymer.