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The Characteristic Control of Spherical Silica Particle Using by W/O Type Emulsion(I);The analysis of Particle shape and size distribution of silica as a function mixing speed

W/O형 에멀젼을 이용한 구형 실리카 입자의 특성제어(제1보);교반속도에 따른 실리카 입자의 형태 및 입도 분석

  • Published : 2006.03.31

Abstract

The W/O emulsion was formed by mixing hydrophobic nonion surfactants of span 80 and tween 60 with kerosine, and by adding sodium silicate aqueous solution. Precipitating the W/O emulsion by sodium bicarbonate resulted in spherical silica particles. Shape and size distribution of silica particles were observed. The particles were spherical and they have narrow size distribution. Particle sizes were 9.29, 7.39 and $5.73\;{\mu}m$ at homogenizer speed of 2500, 3000, and 3500 rpm, respectively. The particle size was decreased by increasing agitation speed due to the formation of emulsion droplet. At fixed agitation speed, absorbed paraffin oil weight were measured and the $SiO_2/Na_2O$ mole ratio effects on particle size were investigated. Particle size was decreased by increasing the mole ratio of $SiO_2/Na_2O$.

Keywords

References

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