• Title/Summary/Keyword: particle size analyzer

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A Study on the $H_2S$ Removal with Utilization of Seashell Waste(I) -The Characteristics of Sulfided Reaction Using Thermal Gravimetric Analyzer- (패각 폐기물을 이용한 $H_2S$ 제거에 관한 연구(I) -열중량분석기를 이용한 황화반응특성-)

  • 김영식
    • Journal of Environmental Health Sciences
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    • v.29 no.2
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    • pp.45-49
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    • 2003
  • In this study, lots of methods have been studing to utilize energy and decrease contaminated effluents. There has been great progress on IGCC (Integrated gasification combined cycle) to reduce thermal energy losses. The following results have been conducted from desulfurization experiments using waste shell to remove H$_2$S. According to TGA results, temperature had influenced on H$_2$S removal efficiency. As desulfurization temperature increased, desulfurization efficiency increased. Also, maximum desulfurization efficiency was observed at 80$0^{\circ}C$. Desulfurization was related to calcination temperature. Considering temperature ranges of exhausted gas from hot gas gasification equipment were 400~80$0^{\circ}C$. Thus, desulfurization efficiency would be increased desulfurization temperature situation at highly. Experiments by TGA showed that particle size of sorbents had influenced on desulfurization capacity. Maximum desulfurization capacity was observed at 0.631 mm for oyster and clam. Rest of sorbents showed similar capacity within 0.171~0.335 mm particle size range. So, particle size would be considered. When would be used waste shells as IGCC sorbents. According to the results about desulfurization capacity by TGA, oyster had the best desulfurization capacity among limestone and waste shell. We would be identify to substituted oyster for existing sorbents

Synthesis of Platinum Nanoparticles by Liquid Phase Reduction (액상환원공정을 이용한 백금 나노 입자의 합성)

  • Lee, Jin-Ho;Kim, Se-Hoon;Kim, Jin-Woo;Lee, Min-Ha;Kim, Young-Do
    • Journal of Powder Materials
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    • v.19 no.1
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    • pp.60-66
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    • 2012
  • In this study, Platinum(Pt) nanoparticles were synthesized by using polyol process which is one of the liquid phase reduction methods. Dihydrogen hexachloroplatinate (IV) hexahydrate $(H_2PtCl_6{\cdot}6H_2O)$, as a precursor, was dissolved in ethylene glycol and silver nitrate ($AgNO_3$) was added as metal salt for shape control of Pt particle. Also, polyvinylpyrrolidone (PVP), as capping agent, was added to reduce the size of particle and to separate the particles. The size of Pt nanoparticles was evaluated particle size analyzer (PSA). The size and morphology of Pt nanoparticles were observed by transmission electron microscopy (TEM) and high resolution TEM (HRTEM). Synthesized Pt nanoparticles were studied with varying time and temperature of polyol process. Pt nanoparticles have been successfully synthesized with controlled sizes in the range 5-10 and 20-40 nm with cube and multiple-cube shapes.

THE DISTRIBUTION OF DIGESTA PARTICLES AND MEAN PARTICLE SIZE OF DIGESTA OBTAINED FROM THE DIVERSE PARTS OF THE GASTROINTESTINAL TRACT OF RUMINANTS

  • Sekine, J.;Fujikura, T.;Oura, R.;Asahida, Y.
    • Asian-Australasian Journal of Animal Sciences
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    • v.5 no.1
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    • pp.13-18
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    • 1992
  • Three cattle, a sheep and a goat were slaughtered to determine the distribution of digesta particles and mean size of digesta particles. Aliquot samples of digesta in the diverse sites of the digestive tracts were fractionated by a wet sieving technique. Fractionated particles were analyzed by the magnetic grid analyzer system constructed by authors. Results showed that the proportion of particles in digesta was similar among the omasum, abomasums cecum, colon and rectum, but that for the reticulo-ruminal digesta was different from the others. The pattern of the mass base frequency distribution of particles was also similar in the post-ruminal digesta. Average Heywood's diameter (the diameter equivalent to that of a circle with equal area to a projected area of a given particle) was about 1.2 mm in the reticulo-ruminal digesta and decreased to 0.65 mm for cattle or to about 0.35 mm for sheep and goat in the omasal digesta. Average Heywood's diameter was about the same in the post-ruminal digesta. It is concluded that mean particle size and particle distribution in digesta of the rectum or feces reflect those in digesta of the omasum.

A Comparative Study on the Conditioning and Dewaterability of Digested Sludge from Intermittent Aerobic Digestion (간헐포기 소화슬러지의 개량과 탈수 특성에 관한 비교 연구)

  • Kim, Seong Hong;Choi, Young Gyun;Chung, Tai Hak
    • Journal of Korean Society on Water Environment
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    • v.20 no.4
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    • pp.370-375
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    • 2004
  • Synthetic organic polyelectrolytes can be used to condition sludges to enhance their dewaterability. When conditioning biological sludges, the charge on the polymer has a significant impact on the effectiveness of the polymer as a conditioner. The objectives of this investigation were to determine the most effective type and dosage of polymer for conditioning digested sludge prior to dewatering, and to investigate the relationship between dewaterability and particle size. 3 types of digested sludge were used under the different digestion processes like anaerobic digestion, aerobic digestion and intermittent aerobic digestion. CST(capillary suction time), TTF(time-to-filter) and SRF(specific resistance to filtration) were tested as a dewaterability index and the number of particle distribution was analyzed using particle size analyzer. The results indicate that cationic polymer appears to be required for effective conditioning of these 3 types digested sludge and the optimal polymer dosage is about 0.6% of SS. CST and TTF are well correlated with mean particle diameter of which the dimension order is 1.7.

Fuel Spray Characteristics of Dimethyl Ether (DME 연료의 분무 특성에 관한 연구)

  • Lee, Sang Hoon;Chon, Mun Soo
    • Journal of Institute of Convergence Technology
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    • v.3 no.2
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    • pp.51-56
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    • 2013
  • This paper describes the atomization characteristics, as well as the velocity and size distribution, of DME spray based on common-rail injection system. To analyze the possibility of using DME fuel as an alternative fuel of diesel, spray atomization characteristics were investigated. For this investigation, two-dimensional phase Doppler analyzer system was used to obtain droplet size and velocity distribution simultaneously. Velocity and droplet size measurements were performed at various injection pressures. Results showed that increasing pressure from 25MPa to 50MPa leads to higher spray droplet velocities and smaller droplet diameter but injection pressure above 40MPa, no signifiant reduction was observed. With the droplet velocity and SMD comparison between diesel and DME fuel, it can be observed that DME has smaller SMD and droplet velocity due to its low surface tension.

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Calibration and Uncertainty Measurement of Differential Mobility Analyzer Using 100 nm NIST SRM 1963 (100 nm NIST 표준입자를 이용한 미분형 전기 이동도 분석기의 교정 및 불확실도 측정)

  • Lee, Snag-Jin;Ahn, Jin-Hong;Ahn, Kang-Ho
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.27 no.12
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    • pp.1766-1771
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    • 2003
  • House made differential mobility analyzer(DMA) is calibrated with NIST SRM 1691(300 nm PSL). Then the particle size and uncertainty for differential mobility analyzer(DMA) using the NIST SRM 1963(100 nm PSL). In result, calibration of prototype DMA is measured using 300 nm NIST SRM 1691, then sheath air flow was corrected 126.67 ㎤/s. Corrected sheath air flow is used in uncertainty measurement of prototype DMA. Uncertainty analysis is performed using NIST SRM 1963(100 nm PSL). The experimental result shows that NIST SRM 1963 is measured as 102.17 nm with a type A uncertainty of 0.33 nm.

Study on the real-time measurement equipment for nanoparticle in low-pressure processes (저압공정 중 발생하는 나노입자 실시간 측정장비에 관한 연구)

  • Na, Jeong-Gil;Cho, Dae-Geun;Choi, Jae-Boong;Kim, Young-Gin;Kim, Tae-Sung
    • Journal of the Korean Vacuum Society
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    • v.16 no.6
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    • pp.468-473
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    • 2007
  • In this paper, we discussed about the development of the PBMS(Particle Beam Mass Spectrometer) that can measure the nanoparticles on real-time in low-pressure processes. To calibrate this equipment, a DMA(Differential Mobility Analyzer) was used to generate NaCl particles which are charged to +1. Total aerosols flow rate was 1 lpm and 0.086 lpm of that was introduced into the PBMS through the pressure-reducing critical orifice. Transport efficiency through PBMS was 50$\sim$60 % compared to particle current for DMA and PBMS according to the particle size. Results of mesurements are in good agreement with size distributions obtained by DMA.

The Study for Stability of Useful Glycyrrhiza uralensis (Licorice Root) Using Nanosolve and PMMA (Nanosolve와 PMMA를 이용한 유용성감초산의 안정화에 대한 연구)

  • Ji, Hong-Geun;Kim, Ju-Duck;Kim, Jeong-Dong;Choi, Jung-Sik
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.30 no.2
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    • pp.207-210
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    • 2004
  • Glycyrrhiza uralensis (licorice root) is very useful medicinal herb because of strong anti-inflammatory and anti-wrinkle effect. Therefore, it is widely used in functional cosmetics. However, it is insoluble and easily decomposed by light, heat, oxygen, etc. In this study, we first prepared NanoSolve-Licorice (30-50nm) using Glycyrrhiza uralensis and propylene glycol! hydrogenated lecithin/caprylic/capric triglyceride/glycerin/water system with microfluidizer. And then, NanoSolve-Licorice and porous PMMA are dispersed in ethanol. Finally, we could get a stabilized system with high-pressure homogenizer (1,000 Bar, 3 passes). According to HPLC measurement for glabridin content, our system is more stable compared with general liposome ones. Capsulated licorice has an enhanced anti-inflammatory effect on account of excellent skin penetration. We also evaluated our final product through image analyzer, particle size analyzer, FF-TEM and chromameter.

Spray Characteristics of the Rotating Fuel Nozzle with Orifice Geometry (회전연료노즐 형상변경에 따른 분무특성)

  • Jang, Seong-Ho;Choi, Hyun-Kyung;Lee, Dong-Hun;You, Gyung-Won;Choi, Seong-Man
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2008.05a
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    • pp.240-243
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    • 2008
  • An experimental study was conducted to understand spray characteristics of rotating fuel nozzle by using high speed rotational system. The experimental apparatus consist of a fuel injection system, high speed rotational system, and acrylic case. The test is performed with several diameters and number of injection orifices. Spray characteristics such as droplet size and velocity are measured by PDPA(Phase Doppler Particle Analyzer). From the test results, we could understand the spray characteristics of rotating fuel nozzle with orifice number and diameter.

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Behavior Characteristics of Swirl-Twin Spray with Changing Swirl Angle (선회각도변화에 따른 2유체 선회분무의 거동특성)

  • Kang, Wan-Bong;Cha, Keun-Jong;Kim, Duck-Jool
    • Proceedings of the KSME Conference
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    • 2000.04b
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    • pp.943-948
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    • 2000
  • The Twin-fluid Swirl Nozzles are used in many parts of the industry to produce homogeneous spray. This study is to investigate the effects of outer air swiller and inner water swiller on atomization of liquid.. The experiment was carried out with increasing air-flow rate at constant liquid-flow rate and with changing outer air swiller angle and inner water swiller angle. A Particle Dynamics Analyzer(PDA) was used to measure drop size, mean and ms values of axial velocity, number density and Sauter mean diameter(SMD). The axial mean velocity and SMD of droplets were measured along the center line and radial directions. It was found that the higher air flow-rate resulted in the smaller Sauter mean diameter of liquid spray and the higher axial mean velocity of droplets. This experimental results will be conveniently used for the preliminary design stage of twin-fluid nozzle development.

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