• 한국결정성장학회지
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• 제25권3호
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• pp.93-97
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• 2015

본 연구에서는 고순도 균질 마이크로 Ag 입자를 얻기 위하여 용매추출법과 RF-LPP법을 이용하여 Air 분위기에서 $500^{\circ}C$에서 3시간 동안 열처리하여 Ag 입자를 합성하였다. 합성된 마이크로 Ag 입자를 XRD에 의해 비교 분석한 결과 주요 peak들이 JCPDS card(No. 87-0719)와 일치하는 것을 확인하였다. RF-LPP법을 이용함으로써, 핵 생성 싸이트 제어를 통해 균질 마이크로 Ag 입자를 합성하였으며, 환원처리 후 산소의 함유가 줄어드는 것을 확인하였다. 본 연구를 통하여 재활용 기술에 큰 기여를 할 것이라 기대한다.

• 한국가시화정보학회:학술대회논문집
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• 한국가시화정보학회 2001년도 Proceedings of 2001 Korea-Japan Joint Seminar on Particle Image Velocimetry
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• pp.1-5
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• 2001

A particle image velocimetry (PIV) was applied to a flow measurement in a transonic centrifugal impeller. A phase locked measurement technique every $20\%$ blade pitch enabled a reconstruction of a velocity field over one blade pitch. The measured velocity field at the inducer of impeller clearly showed a shock wave generated on the suction surface of a blade.

• Journal of Korean Society for Atmospheric Environment
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• 제21권E1호
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• pp.13-21
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• 2005

Atmospheric concentrations of PCBs were monitored in Ansung-city, Kyonggi province during the 2001/2002 to characterize the concentration distribution and seasonal variation of particle polychlorinated biphenyls (PCBs). Average concentration of particle bound PCB showed maximum value for penta-CBs and minimum value for octa-CBs. Seasonal contributions $(%\)$ of total particle PCBs showed the highest value in winter months and lowest value in summer month, This result indicated that concentration of total particle PCBs increased with decreasing temperature in the atmosphere. Therefore, particle PCBs were easily formed by the condensation of gas phase PCBs in winter months. The total particle PCBs exhibited an inverse correlation with temperature (p<0.01) which suggested that particle PCBs were easily formed by condensation of gaseous PCBs in winter months.

• Macromolecular Research
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• 제17권5호
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• pp.339-345
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• 2009

The core/shell type structure of the highly crosslinked poly(glycidylmetharylate-co-divinylbenzene) microspheres prepared in the precipitation polymerization in acetonitrile was thoroughly verified by means of swelling, $^1H$ NMR, XPS, TEM and TGA measurements. In the XPS measurement, the higher the GMA content, the higher the oxygen content was observed, implying that the higher content of GMA is observed in the particle surface. The further verification of the core/shell structure of the poly(GMA-co-DVB) particles was carried out using $^1H$ NMR and TEM techniques, resulting in the poly(GMA-co-DVB) particles with the GMA rich-phase and DVB rich-phase. In overall, the poly(GMA-co-DVB) microspheres consist of a highly crosslinked DVB rich-phase in the core and slightly or non-crosslinked GMA rich-phase in the shell part due to the different reaction ratios between two monomers and self-crosslinking density of DVB.

• 한국원자력학회:학술대회논문집
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• 한국원자력학회 1996년도 춘계학술발표회논문집(2)
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• pp.537-542
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• 1996

In the present work the influence of various physical parameters on the two-phase flow behavior in a self-heated porous medium has been studied using a numerical model, that is, the effects of heat generation rate, of porosity, of particle size, and of system pressure on the dryout process. To analyze the effect of these parameters, the variation of both liquid volumetric fraction and liquid axial velocity is evaluated at the steady state or at the onset of a first boiled-out region. The analysis of computational results indicate that a qualitative tendency exists between the parameters such as heat generation rate, porosity, effective particle diameter and the temporal development of the liquid volumetric fraction field up to dryout. In addition to these parameters, a variation of fluid properties such as phase density, phase viscosity due to a change of system pressure can be used for gaining insight into the nature of two-phase flow behavior up to dryout.

• 한국가시화정보학회지
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• 제1권2호
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• pp.52-57
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• 2003

The present paper investigated the effect of ultrasonic vibrations on the melting process of a phase-change material (PCM). The melting process in the square cavity with a heated vertical wall has been studied in terms of acoustic streaming. In the present study, applying with ultrasonic vibrations to the liquid were found to induce acoustic streaming which was clearly observed using by a particle image velocimetry (PIV) and a thermal infrared camera. The experimental results revealed that acoustic streaming could accelerate the melting process as much as 2.5 times, compared to the rate of natural melting (i. e., the melting without acoustic streaming). In addition, temperature and Nusselt numbers over time provided conclusive evidence of the important role of the acoustic streaming on the melting phenomena of the PCM.

• 한국전산유체공학회:학술대회논문집
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• 한국전산유체공학회 1997년도 추계 학술대회논문집
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• pp.120-125
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• 1997

In the present work the influence of various physical parameters on the two-phase flow behavior in a self-heated porous medium has been studied using a numerical model, that is, the effects of heat generation rate, of porosity, of particle size, and of system pressure on the dryout process. To analyze the effect of these parameters, the variation of both liquid volumetric fraction (i.e., liquid saturation) and liquid axial velocity is evaluated at the steady state or at the onset of a first boiled-out region. The analysis of computational results indicate that a qualitative tendency exists between the parameters such as heat generation rate, porosity, effective particle diameter and the temporal development of the liquid volumetric fraction field up to dryout. In addition to these parameters, a variation of fluid properties such as phase density, phase viscosity due to a change of system pressure can be used for gaining insight into the nature of two-phase flow behavior up to dryout.

• 전기학회논문지
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• 제60권2호
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• pp.349-351
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• 2011

The formation of oxide superconducting phase fabrication of superconducting wire materials and fabrication of precise superconducting material were studied for developing superconductor application technique. The $ZrO_2$ addition reduced the particle size $BaZrO_3$ trapped in the matrix after the sintering growth. The added $ZrO_2$ was converted to fine particles of $BaZrO_3$ which is the conventional sintering temperature for YBaCuO, $Y_2Ba_1Cu_1O_5$ and CuO are formed as by products of the reaction between $ZrO_2$ and YBaCuO phase. The formation of highly $BaZrO_3$ particle appears to be responsible for the refinement of $BaZrO_3$ phase after the citric acid sintering process.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.482-483
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• 2006

Synthesis of iron nanopowder by room-temperature electrochemical reduction process of ${\alpha}-Fe_2O_3$ nanopowder was investigated in terms of phase evolution and microstructure. As process variables, reduction time and applied voltage were changed in the range of $1{\sim}20$ h and $30{\sim}40$ V, respectively. From XRD analyses, it was found that volume of Fe phase increased with increasing reduction time and applied voltage, respectively. The crystallite size of Fe phase in all powder samples was less than 30 nm, implying that particle growth was inhibited by the reaction at room temperature. Based on the distinct equilibrium shape of crystalline particle, phase composition of nanoparticles was identified by TEM observation.

• 설비공학논문집
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• 제2권2호
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• pp.119-126
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• 1990

In this study, the overall heat transfer coefficients are calculated on fluidized bed double pipe heat exchanger and single phase double pipe heat exchanger at the same condition. The effect of the particle size, its material, fluidizing velocity and static bed height on overall heat transfer coefficient has been investigated. The main conclusions obtained from the experiment are as follows. 1. The overall heat transfer coefficient of the fluidized bed heat exchanger is higher than that of single phase forced convective heat exchanger (maximum 2.3 times) 2. The value of the overall heat transfer coefficient increase with an increase in static bed height and decrease with an increase in particle size. 3. For the same particle size, the particle of low density can obtain higher overall heat transfer coefficient than that of high density.