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http://dx.doi.org/10.6111/JKCGCT.2015.25.3.093

The synthesis of high purity micro Ag particle using the rapid firing -liquid phase precursor method  

Lim, Byeong-Seok (School of Advanced Materials Science & Engineering, Sungkyunkwan University)
Song, Young-Hyun (School of Advanced Materials Science & Engineering, Sungkyunkwan University)
Lee, Min-Ji (School of Advanced Materials Science & Engineering, Sungkyunkwan University)
Mang, Sung-Ryul (School of Advanced Materials Science & Engineering, Sungkyunkwan University)
Yoon, Dae-Ho (School of Advanced Materials Science & Engineering, Sungkyunkwan University)
Abstract
To synthesis of high purity micro silver particle, we extracted the silver from the waste by liquid-liquid extraction and used the rapid firing-liquid phase precursor (RF-LPP) method. The silver micro particle was synthesized at $500^{\circ}C$ for 3 hr in air atmosphere by RF-LPP method. As a result of the research, micro silver particle is measured X-ray diffraction (XRD), the main peak is nearly corresponded to the same as JCPDS card (No.87-0719). With using the RF-LPP method, the fine Ag micro particle indicated due to the control of nucleation site and the oxygen contents was decreased by reducing treatment. We expect this research contribute to advance in field of the recycling technology.
Keywords
Micro silver particle; Rapid firing-liquid phase precursor method; Reducing treatment; Recycling technology;
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