• Title/Summary/Keyword: particle flow rate

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Effect of Conductive Particles on Electrical Conductivity using EHD Ink Jet Printing Technology (EHD Ink Jet Printing 기술을 이용한 Conductive Particle의 전기전도도에 미치는 영향)

  • Ahn, Ju-Hun;Lee, Yong-Chan;Choi, Dae-San;Lee, Chang-Yull
    • Journal of Aerospace System Engineering
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    • v.12 no.6
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    • pp.1-8
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    • 2018
  • ACF, which is used for the transparent electrode film is manufactured by the thermocompression method with conductive particles. However, the method has disadvantages since there are many wasted materials and the process is complex. To overcome the demerits of the conventional method, EHD printing technology with conductive particles ink is proposed. The line thickness of patterning is influenced by the characteristics of the inks and the printing conditions. Therefore, it is salient to find the most conducive conditions for the micro patterning. In this paper, the ink with conductive particles was manufactured, and the patterning results were obtained by varying the nozzle thickness and the flow rate. The electrical conductivity according to the ejection of the particles ink is obtained.

Remediation of Heavy Metal-Contaminated Soil Within a Military Shooting Range through Physicochemical Treatment (물리화학적 처리를 이용한 군부대 사격장 내 중금속 오염 토양의 정화)

  • Lee, Sang-Woo;Lee, Woo-Chun;Lee, Sang-Hwan;Kim, Soon-Oh
    • Journal of Soil and Groundwater Environment
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    • v.26 no.5
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    • pp.9-19
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    • 2021
  • This study evaluated the feasibility of combined use of physical separation and soil washing to remediate heavy metals (Pb and Cu) contaminated soil in a military shooting range. The soils were classified into two types based on the level of heavy metal concentrations: a higher contaminated soil (HCS) with Pb and Cu concentrations of 6,243 mg/kg and 407 mg/kg, respectively, and a lower contaminated soil (LCS) with their concentrations of 1,658 mg/kg and 232 mg/kg. Pb level in both soils exceeded the regulatory limit (700 mg/kg), and its concentration generally increased with decreasing soil particle size. However, in some cases, Pb concentrations increased with increasing soil particle size, presumably due to the presence of residues of bullets in the soil matrix. As a pretreatment step, a shaking table was used for physical separation of soil to remove bullet residues while fractionating the contaminated soils into different sizes. The most effective separation and fractionation were achieved at vibration velocity of 296 rpm/min, the table slope of 7.0°, and the separating water flow rate of 23 L/min. The efficiency of ensuing soil washing process for LCS was maximized by using 0.5% HCl with the soil:washing solution mixing ratio of 1:3 for 1 hr treatment. On the contrary, HCS was most effectively remediated by using 1.0% HCl with the same soil:solution mixing ratio for 3 hr. This work demonstrated that the combined use of physical separation and soil washing could be a viable option to remediate soils highly contaminated with heavy metals.

Development of An Improved Acetone-Water Fractional Precipitation Process for Purification of Paclitaxel from Taxus chinensis and Its Kinetic and Thermodynamic Analysis (Taxus chinensis로부터 파클리탁셀 정제를 위한 개선된 아세톤-물 분별침전 공정 개발 및 그 동역학 및 열역학적 해석)

  • Kang, Hoe-Jong;Kim, Jin-Hyun
    • Korean Chemical Engineering Research
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    • v.59 no.3
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    • pp.379-392
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    • 2021
  • In this study, an improved acetone-water fractional precipitation process for paclitaxel using ultrasonic cavitation bubbles and gas bubbles was developed. Compared to the conventional method, the time required for precipitation has been reduced by 20~25 times. In addition, the particle size of paclitaxel decreased by 3.5~5.5 times and the diffusion coefficient of paclitaxel increased by 3.5~6.7 times. In the case of precipitation using ultrasonic cavitation bubbles, as the ultrasonic power increased and the temperature decreased, the precipitation rate constant increased. In the case of precipitation using gas bubbles, as the gas flow rate increased and the temperature decreased, the precipitation rate constant increased. Thermodynamic parameters revealed the exothermic, irreversible, and nonspontaneous nature of the improved fractional precipitation.

Analysis of Cyclic Adenosine Monophosphate (cAMP) Separation via RP-HPLC (reversed-phase high-performance liquid chromatography) by the Moment Method and the van Deemter Equation (역상 크로마토그래피에서 모멘트 방법과 van Deemter 식을 이용한 고리형 아데노신 일인산의 분리특성 연구)

  • Lee, Il Song;Ko, Kwan Young;Kim, In Ho
    • Korean Chemical Engineering Research
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    • v.53 no.6
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    • pp.723-729
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    • 2015
  • The moment analysis of cyclic adenosine monophosphate (cAMP) was performed using chromatograms that were obtained with the pulse input method from an octadecyl silica (ODS) high-performance liquid chromatography (HPLC) column. The general rate (GR) model was employed to calculate the first absolute moment and the second central moment. Three important coefficients for moment analysis, which are molecular diffusivity ($D_m$), external mass transfer coefficient ($k_f$), and intra-particle diffusivity ($D_e$), were estimated by the Wilke-Chang equation, Wilson-Geankoplis equation, and comparing van Deemter equation to theoretical plate number equation, respectively. Experiments were conducted by various conditions of flow rates, methanol volume ratio of the mobile phase, and solute concentration. After the moment analysis, results were organized by van Deemter plots. Also van Deemter coefficients were compared each other to effect $H_{ax}$, $H_f$, and $H_d$ on height equivalent to a theoretical plate (HETP, $H_{total}$). The value of intraparticle diffusion ($H_d$) was the primary factor which makes for HETP whereas external mass transfer ($H_f$) was disregardable factor.

Sediment Transport Characteristics in a Pressure Pipeline (압력 원형관로내 유사이송특성 연구)

  • Son, Kwang Ik;Kim, Hyun Jung
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.31 no.3B
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    • pp.205-209
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    • 2011
  • The low carrying capacity caused by the deposition in a sewer line is one of the main reason of the urban flood. Therefore, an efficient maintenance and management of the storm water drainage system is very important to prevent urban flood. In this research, the sediment transport characteristics through a pressure pipeline were examined with laboratory experiments. Bed-forms in a pipeline, sediment rates, roughness due to sediments were examined. Experimental system consists of flow circulation system with a pump and a sediment feeder at the upstream of the pipeline. Sediments were supplied into a 60 mm-diameter and 8 m-long pipe. Maximum flow rate is $30m^3/hr$, and the sediment feeding rate range is 5 g/s~19 g/s. Governing parameters and estimation equation for sediment transport rate were developed. The mean velocity (U), coefficient of viscosity (${\mu}$), unit width bed load ($q_b$), mean diameter of particle ($d_{50}$), unit weight of sediment in water (${\gamma}^{\prime}_s$) were adopted as the most influencing factors of sediment transport patterns. The prediction equation for sediment transport rate were developed with two dimensionless terms. These two dimensionless terms showed a linear relationship with high correlation coefficient.

In situ analysis of capturing dynamics of magnetic nanoparticles in a microfluidic system

  • Munir, Ahsan;Zhu, Zanzan;Wang, Jianlong;Zhou, H. Susan
    • Smart Structures and Systems
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    • v.12 no.1
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    • pp.1-22
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    • 2013
  • Magnetic nanoparticle based bioseparation in microfluidics is a multiphysics phenomenon that involves interplay of various parameters. The ability to understand the dynamics of these parameters is a prerequisite for designing and developing more efficient magnetic cell/bio-particle separation systems. Therefore, in this work proof-of-concept experiments are combined with advanced numerical simulation to design and optimize the capturing process of magnetic nanoparticles responsible for efficient microfluidic bioseparation. A low cost generic microfluidic platform was developed using a novel micromolding method that can be done without a clean room techniques and at much lower cost and time. Parametric analysis using both experiments and theoretical predictions were performed. It was found that flow rate and magnetic field strength greatly influence the transport of magnetic nanoparticles in the microchannel and control the capturing efficiency. The results from mathematical model agree very well with experiments. The model further demonstrated that a 12% increase in capturing efficiency can be achieved by introducing of iron-grooved bar in the microfluidic setup that resulted in increase in magnetic field gradient. The numerical simulations were helpful in testing and optimizing key design parameters. Overall, this work demonstrated that a simple low cost experimental proof-of-concept setup can be synchronized with advanced numerical simulation not only to enhance the functional performance of magneto-fluidic capturing systems but also to efficiently design and develop microfluidic bioseparation systems for biomedical applications.

A Study on the Reliability Analysis for Smoke Detector using Dust (분진을 이용한 연기감지기 신뢰성 분석에 관한 연구)

  • Hong, Sung Ho;Choi, Moon Soo;Lee, Young Man
    • Journal of the Korean Society of Safety
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    • v.28 no.6
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    • pp.11-16
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    • 2013
  • This paper presents a study on the analyzing reliability of smoke fire detector using accelerated life test. In general, the smoke fire detector is broken by dust which flow in smoke detection chamber. In order to conduct accelerated life test of smoke fire detector dust is set accelerated factor in this paper. The dust is fly-ash which is test particle 5th regulated by KS A 0090. The dust accelerated level is 60 g, 180 g and 360 g and failure time is measured by smoke sensitivity testing. It is considered to failure of detector if detector don't operate within 30 secconds when subjected to an air stream having a velocity of 20 cm/s~40 cm/s containing smoke with a concentration of 15% of rate of light-response of 1 m. The goodness of fit test and mean life prediction conduct using the failure time. The result show that life distribution fits the weibull distribution for failure time data and the mean lifes calculate 22.5 year in domestic product and 14.7 years in overseas product applied dust stress only.

Enrichment of valuable elements from vanadium slag using superconducting HGMS technology

  • He, Sai;Yang, Chang-qiao;Li, Su-qin;Zhang, Chang-quan
    • Progress in Superconductivity and Cryogenics
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    • v.19 no.1
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    • pp.17-21
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    • 2017
  • Vanadium slags is a kind of vanadiferous solid waste from steelmaking process. It not only occupies land, pollutes environment, but also leads to waste of resources. Based on the difference of magnetic susceptibility of different particles caused by their chemical and physical properties from vanadium slag, a new technology, superconducting high gradient magnetic separation was investigated for separation and extraction of valuable substances from vanadium slag. The magnetic concentrate was obtained under optimal parameters, i.e., a particle size -200 mesh, a magnetic flux density of 0.8 T, a slurry concentration of 5 g/L, an amount of steel wools of 25 g and a slurry flow velocity of 2 L/min. The content of $Fe_2O_3$ in concentrate could be increased from 39.6% to 55.0% and $V_2O_5$ from 2.5% to 4.0%, respectively. The recovery rate is up to 42.9%, and the vanadium slag has been effectively reused.

A Simple and Sensitive Assay for Cefepime in Human Plasma Using High Performance Liquid Chromatography

  • Kim, Young-Sun;Yim, Dong-Seok;Lee, Dong-Gun;Lee, Sang-Bok
    • The Korean Journal of Physiology and Pharmacology
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    • v.7 no.4
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    • pp.247-250
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    • 2003
  • A simple and sensitive assay method was developed for cefepime in human plasma using high performance liquid chromatography (HPLC). Cefepime and cefadroxil (the internal standard) were extracted from heparinized human plasma by simple deproteination with perchloric acid. The extract was injected into an Atlantis dC18 column ($250{\times}4.6$ mm; particle size $5{\mu}m$, Waters) and the column was eluted with methanol and 0.01 M dihydrogen phosphate at pH 3.0 (15:85 v:v) as a mobile phase at a flow rate of 0.7 mL/min. Linearity was confirmed for the range 0.25 to $200{\mu}L/mL$ and the limit of quantitation was $0.25{\mu}L/mL$. The retention times were 10.2 min and 13.4 min for cefepime and cefadroxil, respectively. This method was successfully applied to a pharmacokinetic study of cefepime in plasma from bone marrow transplant patients.

Development and Validation of a Liquid Chromatography-Tandem Mass Spectrometry Method for the Determination of ε-Acetamidocaproic Acid in Rat Plasma

  • Kim, Tae Hyun;Choi, Yong Seok;Choi, Young Hee;Kim, Yoon Gyoon
    • Toxicological Research
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    • v.29 no.3
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    • pp.203-209
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    • 2013
  • A simple and rapid liquid chromatography-tandem mass spectrometry (LC-MS/MS) method was developed and validated for the quantification of ${\varepsilon}$-acetamidocaproic acid (AACA), the primary metabolite of zinc acexamate (ZAC), in rat plasma by using normetanephrine as an internal standard. Sample preparation involved protein precipitation using methanol. Separation was achieved on a Gemini-NX $C_{18}$ column ($150mm{\times}2.0mm$, i.d., 3 ${\mu}m$ particle size) using a mixture of 0.1% formic acid-water : acetonitrile (80 : 20, v/v) as the mobile phase at a flow rate of 200 ${\mu}l/min$. Quantification was performed on a triple quadrupole mass spectrometer employing electrospray ionization and operating in multiple reaction monitoring (MRM) and positive ion mode. The total chromatographic run time was 4.0 min, and the calibration curves of AACA were linear over the concentration range of 20~5000 ng/ml in rat plasma. The coefficient of variation and relative error at four QC levels were ranged from 1.0% to 5.8% and from -8.4% to 6.6%, respectively. The present method was successfully applied for estimating the pharmacokinetic parameters of AACA following intravenous or oral administration of ZAC to rats.