• Title/Summary/Keyword: pH measurement test

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Antioxidant Activity of Extracts from Smilax china Root (청미래덩굴(Smilax china) 뿌리 추출물의 항산화활성 효과)

  • Song, Hee-Sun;Park, Yeon-Hee;Jung, Sae-Heung;Kim, Dong-Pil;Jung, Yong-Hee;Lee, Mi-Kyung;Moon, Ki-Young
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.35 no.9
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    • pp.1133-1138
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    • 2006
  • Smilax china root has been used as traditional medicinal remedy in China and Korea and reported to have various biological activities such as anti-inflammatory, antimutagenic and antimicrobial activities. In this study, the possibility of development as natural antioxidants of Smilax china root extracts was investigated. For the evaluation of antioxidant activity, aqueous- and 25% EtOH extract from Smilax china root were prepared and six different evaluation assay methods, i.e., measurement of total phenolics, radical scavenging effects on 1,1-diphenyl-2-picrylhydrazyl (DPPH), nitric oxide (NO) and nitrite $(NO_2)$, reducing power, and inhibitory effect on tyrosinase activity, were used. The total phenolics content of two extracts was high as the level of 36 mg of gallic acid equivalent per 1 g of dried sample tested. The radical scavenging activities of ethanol extract toward DPPH and NO were better than those of aqueous extract (p<0.05). The $NO_2$ scavenging activity of both extracts showed the highest value at pH 1.2 (98%). Especially, the $NO_2$ scavenging activities of EtOH extract were significantly stronger than those of aqueous one at pH 4.2 (51%) and pH 6.0 (32%), respectively. In the reducing power test, both extracts revealed higher ferric ion reducing activity than known antioxidant, vitamin C at the level of $0.05\sim0.1mg/mL$ (p<0.01). The 1 mL of aqueous and 25% EtOH extract showed effective inhibition activity on tyrosinase activity as 45% and 53%, respectively. Therefore, these results suggest that two extracts from Smilax china root may serve as useful natural antioxidants.

Studies on Physico-chemical Properties of Chicken Meat Cooked in Electric Oven Combined with Superheated Steam (전기오븐에서 과열증기주입에 따른 열처리가 닭고기의 이화학적 특성변화에 미치는 영향)

  • Chun, Ji-Yeon;Kwon, Bong-Gu;Lee, Su-Hyun;Min, Sang-Gi;Hong, Geun-Pyo
    • Food Science of Animal Resources
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    • v.33 no.1
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    • pp.103-108
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    • 2013
  • This study was carried out to observe the effect of superheated steam combined with oven heating on the physico-chemical and sensory properties of chicken meat. Specially, chicken breasts and thighs were heated for 40 min in various heating formulations such as oven heating, superheated steam heating or a combination of two kinds of heating. In the physical properties measurement, the shear force was increased as superheated steam heating time and chicken thighs were higher than chicken breasts in all treatments (p<0.05). The highest level of water holding capacity was solely superheated steam treated chicken for 40 min (p<0.05). The $L^*$ value was decreased but $a^*$ value or $b^*$ value were increased after cooking. Chicken breast exhibited a higher colour value than chicken thigh. Superheated heating was effective to reduce heating loss as 22.64% (p<0.05). However, pH was not different depending on the heating formulation or part of the chicken meat (p>0.05). In the sensory test, the combination of 10 min oven heating and 30 min superheated steam heating was effective to create a good flavour of chicken meat. In this study, an optimum formulation was developed which was a combination of 10 min oven heating and 30 min superheated steam heating. It was more effective to improve the quality of chicken meat than the single heat treatment of chicken meat.

Quality Characteristics of Jeungpyun Added Paecilomyces japonica Powder according to Fermentation Time (발효시간에 따른 동충하초 첨가 증편의 품질특성)

  • Park, Geum-Soon;Park, Eo-Jin
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.33 no.10
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    • pp.1703-1708
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    • 2004
  • This study was carried out to investigate the characteristic quality of jeungpyun added Paecilomyces japonica with different fermentation time. The volume of jeungpyun added Paecilomyces japonica was more increased after fermentation. The volume was decreased when the fermentation was progressed. The pH was 5.1 before fermentation and the pH decreased when the fermentation was progressed. Moisture content was more increased as the time of fermentation became longer. Hunter color test, L value and b value appeared the highest after 1st fermentation, and it appeared lesser when the time of fermentation became longer. In measurement of texture, hardness showed the highest value when 90 minutes passed after the 2nd fermentation. Gumminess and brittleness were tend to increase when it have longer fermentation time. In scanning electron microscopic observation, organization of sponges was tend to break down as the fermentation time was longer. Sensory properties showed that color intensity was more strong when second fermentation was progressed, and hardness, toughness, sourness were high when the fermentation time was longer. In conclusion overall acceptability of jeungpyun, 3$0^{\circ}C$, 3 hours after 1st fermentation and 2nd fermentation for 30 minutes, 35$^{\circ}C$ showed the most preference.

Effect of Calcium Acetate and Potassium Sorbate on Characteristics of Kakdugi (Calcium Acetate 및 Potassium Sorbate를 첨가한 깍두기의 품질 특성)

  • Kim, So-Yeon;Um, Jin-Young;Kim, Kwang-Ok
    • Korean Journal of Food Science and Technology
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    • v.23 no.1
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    • pp.1-5
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    • 1991
  • This study was conducted to examine the effect of the addition of calcium acetate and/or potassium sorbate on the characteristics of kakdugi(Korean seasoned pickles of cubed radish roots) fermented at $20^{\circ}C$ for 4 days or more. The sensory characteristics, pH, titratable acidity, non-volatile organic acids and texture by Instron were measured. The results of sensory evaluation on kakdugi stored at $20^{\circ}C$ for 4 days indicated that firmness, toughness, crispness, sour taste and overall desirability were increased by the addition of calcium acetate. Potassium sorbate was evaluated to decrease the sourness. Titratable acidity, pH and the amount of non-volatile organic acids were higher in samples containing calcium acetate than in other ones. Compression test with Instron gave the similiar result to sensory evaluation in the measurement of firmness. Calcium acetate and potassium sorbate showed synergistic effect greatly on the textural characteristics on kakdugis.

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Corrosion Mechanism of Reinforcing Steel in Ceramic Mortar (세라믹스 몰탈내의 철근 부식 메카니즘)

  • Kim, Young Man;Lee, Kang-Bong;Cho, Won Il;Ko, Jae Sik;Choi, Beom Suk;Lee, Ji Young;Kim, Young Sang
    • Analytical Science and Technology
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    • v.14 no.4
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    • pp.364-370
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    • 2001
  • The corrosion behaviors of reinforcing steels were investigated under chloride ion contained in cement mortar including gypsum by the implementation of half cell potential measurement, EPMA analysis, exterior features, weight loss and extraction experiment. The acceleration test equipment accelerated corrosion of mild steel bar in a short period of time. From observing the exterior features and weight loss, we could evaluate the measure of corrosion. Also, from the extraction experiment of ${SO_4}^{2-}$ with $Cl^-$ ions contained in the ceramic mortar, we concluded that ${SO_4}^{2-}$ ion affected more on the corrosion mechanism in comparison to pH.

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Influence of Carbon Fiber on Corrosion Behavior of Carbon Steel in Simulated Concrete Pore Solutions

  • Tang, Yuming;Dun, Yuchao;Zhang, Guodong;Zhao, Xuhui;Zuo, Yu
    • Corrosion Science and Technology
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    • v.16 no.4
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    • pp.175-182
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    • 2017
  • Galvanic current measurement, polarization curves, electrochemical impedance spectroscopy and weight loss test were used to study the corrosion behavior of carbon steel before and after carbon fibers coupling to the carbon steel in simulated concrete pore solutions, and the film composition on the steel surface was analyzed using XPS method. The results indicate that passive film on steel surface had excellent protective property in pore solutions with different pH values (13.3, 12.5 and 11.6). After coupling with carbon fibers (the area ratio of carbon steel to carbon fiber was 12.31), charge transfer resistance $R_{ct}$ of the steel surface decreased and the $Fe^{3+}/Fe^{2+}$ value in passive film decreased. As a result, stability of the film decreased and the corrosion rate of steel increased. Decreasing of the area ratio of steel to carbon fiber from 12.3 to 6.15 resulted in the decrease in $R_{ct}$ and the increase in corrosion rate. Especially in the pore solution with pH 11.6, the coupling leads the carbon steel to corrode easily.

Preparation and Physicochemical Characterization of Sea Tangle Vinegar for Utilization as Vinegar-Based Salad Dressing (식초기반 샐러드 드레싱용 다시마 식초 제조 및 이화학적 특성)

  • Han, Areum;Surh, Jeonghee
    • Korean journal of food and cookery science
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    • v.33 no.3
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    • pp.300-306
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    • 2017
  • Purpose: This study aimed to prepare sea tangle vinegar and test its applicability as a vinegar-based functional salad dressing in terms of physicochemical properties. Methods: Sea tangle vinegar was prepared by mixing sea tangle with sugar and vinegar and fermenting the mixture at room temperature for 3 months. The resulting sea tangle vinegar was examined for its physicochemical properties and antioxidant activity with brewed vinegar and persimmon vinegar as controls. Results: The sea tangle vinegar showed significantly higher viscosity than control vinegars, and shear thinning behavior that is typical for salad dressing containing polymers. In addition, storage modulus (G′) of sea tangle vinegar was relatively high in dynamic viscosity measurement while that of control vinegars remained negligible. Together with the high soluble solids content of sea tangle vinegar, rheological behavior indicates that sea tangle vinegar had soluble polysaccharides extracted from sea tangle, consequently leading to an increase in viscosity. Titratable acidity (TA) and pH were 2.52% and 3.58, respectively, which satisfies the TA and pH requirements for microbiological safety of a salad dressing. Absorbance at 285 nm and Folin Ciocalteu's reagent method revealed that sea tangle vinegar contained antioxidative phenolic compounds. Conclusion: This study demonstrates that sea tangle vinegar could be potentially developed as a vinegar-based functional salad dressing when combined with sensory evaluation in the future.

Determination of Aluminum Leached from Cooking Utensils by using Flow Injection Analysis (흐름주입분석법에 의한 주방용기로부터 용출된 알루미늄의 정량)

  • Choi, Yong Wook
    • Journal of Korean Society on Water Environment
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    • v.20 no.3
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    • pp.281-289
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    • 2004
  • Optimal analytical conditions have been established for mixing and reaction coil length, concentrations of ECR, CTAB, and acetate, reaction temperature and pH in the determination of aluminum by using flow injection analysis(FIA). Detection limit and repeatability for this system were $3{\mu}g/L$ and better than 1% of relative standard deviation, respectively. The interference from iron(III) was suppressed up to 6mg/L of iron(III) by $0.1{\mu}M$ ascorbic acid, and the interference from fluoride could be tolerated in absorption of Al/ECR/CTAB derivative by 10mM boric acid at pH 3.5 adjusted with nitric acid. This FIA system was applied to the determination of aluminum leached from cooking utensils by distilled and tap water containing fluoride ranged from 0.5 to 2mg/L by measurement of absorbance for Al/ECR/CTAB at 585nm. The leached aluminum content was increased with increasing concentration of fluoride. The aluminum contents leached from aluminum utensils by tap water were about 9 fold higher than those leached by distilled water, whereas aluminum contents leached by distilled water containing fluoride were about 2 fold higher compared to those leached by distilled water. That represented that other dissolved substances as well as fluoride in tap water contributed to liberation of aluminum from aluminum utensils. A comparison between FIA data and ICP-AES data by correlation and paired t test showed that the FIA system could be accepted as a good alternative method for the determination of aluminum in tap water.

Evaluation of Field Application for the mix properties of the thixotropic grout (가소성그라우트의 배합특성 및 현장 적용성 평가)

  • Kim, Hak-Moon;Jang, Kyung-Jun
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.12 no.9
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    • pp.4223-4238
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    • 2011
  • The advantages of grouting are the simple instrument, the simple procedure of practice and the simple verification of grouting result. but the more grouting practice there is, the more damages of environment from grouting practice and grouting materials there are. so, the grouting materials and methods with the character of environment friendly are introduced in construction field, recently. This paper is to study of the physical characteristics that has thixotropic character and that consists of inorganic and polycarboxylate co-polymer. In study, various testing methods are performed such as a viscosity, a thixotropy, a compressive strength, a heavy metal detection and pH measurement in lab test and a low pressure injection test and a high pressure injection test in field with different soil type. As a result, a optimum mix ratio is proposed by analyzing the result of lab test. the field applicability is verified by checking a injection pressure, a grout volume and a hardened body of grout by excavating the practice site.

Effect of Lactic Acid Bacteria and Temperature on Kimchi Fermentation (II) (젖산균과 온도가 김치 발효에 미치는 영향(II))

  • Cho, Young;Rhee, Hei-Soo
    • Korean journal of food and cookery science
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    • v.7 no.2
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    • pp.89-95
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    • 1991
  • The effects of lactic acid bacteria on the chemical and microbial changes of fermented kimchi at various temperatures were studied. Kimchi was homogenized and was sterilized by ultra violet (UV), then Lactobacillus plantarum, Leuconostoc mesenteroides, Pediococous acidilactici, Lactobacillus brevis and the mixture of these bacteria inoculated on sterilized kimchi, respectively. The measurement of alcohol by gas chromatography, and changes of sugar content and total viable count were investigated and palatability test was carried while inoculated kimchi was fermented at $30^{\circ}C$, $21^{\circ}C$ and $7^{\circ}C$. Ethyl alcohol was detected by GC in sample I (original Kimchi homogenate), III(inoculated Leu. mesenteroides), V(inoculated with Lac. brevis), then especially, more content were detected at $14^{\circ}C$. Sugar content reduced in accordance with fermentation proceeding. Total viable count increased at early fermentation stage, but thereafter decreased slowly. In the result of palatability test, sample I was the highest at all temperatures, sample III and IV (inoculated with mixed lactic acid bacteria) was the following in that kimchi odor and taste and the temperature.

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