• 한국식품조리과학회지
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• 제20권2호
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• pp.119-125
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• 2004

Mixograph를 이용하여 반죽의 물성에 미치는 화학첨가제의 영향을 조사한 결과 ammonium ferric citrate와 ferric sulfate는 0.1% 수준에서는 밀가루 반죽의 탄성에 뚜렷한 영향을 미치지 않았으나, MgSO$_4$, CaCl$_2$ 및 ZnO는 반죽의 탄성을 증가시키며 최적반죽시간을 연장시켜 반죽 시간이 길어졌다. 그러나 Ca과 Mg을 각각 갖는 calcium citrate와 MgCl$_2$는 반죽 시간이나 탄성에 뚜렷한 영향을 나타내지 않았다. 빵의 부피에 미치는 영향은 0.1% MgSO$_4$와 CaCl$_2$가 브롬산 칼륨을 전혀 첨가하지 않은 대조구보다 부피 팽창이 더 커져서 브롬산 칼륨과 같은 팽창제로서의 기능을 확인하였으며, 이들을 첨가한 빵의 속과 겉껍질의 색은 모두 대조구보다 더 밝아서 첨가한 화학첨가제들이 빵의 색을 밝게 하는 것을 확인할 수 있었다. 밀가루의 내재된 효소를 불활성화 시키기 위하여 볶음처리와 UV 및 microwave 조사된 밀가루는 최적 반죽시간을 초과하여 계속 반죽하여도 최적반죽시간 후 반죽의 탄성저하현상이 처리하지 않은 대조구에 비하여 감소되어 반죽의 안정성이 향상되었으나, 열처리한 밀가루로 제조한 빵은 부피가 대조구에 비하여 적었으므로 열처리는 반죽의 안정성은 향상시킬 수는 있으나 빵의 부피 증가에는 효과적이지 못하였다.

• Journal of Welding and Joining
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• 제30권5호
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• pp.64-69
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• 2012

Sn-Bi eutectic alloy has been widely used as one of the key solder materials for step soldering at low temperature. The Sn-58Bi solder paste containing chloride flux was adopted to compare with that using the chloride-free flux. The paste was applied on the electroless nickel-immersion gold (ENIG) surface finish by stencil printing, and the reflow process was then performed at $170^{\circ}C$ for 10 min. After reflow, the solder joints were aged at $125^{\circ}C$ for 100, 200, 300, 500 and 1000 h in an oven. The interfacial microstructures were obtained by using scanning electron microscopy (SEM), and the composition of intermetallic compounds (IMCs) was analyzed using energy dispersive spectrometer (EDS). Two different IMC layers, consisting of $Ni_3Sn_4$ and relatively very thin Sn-Bi-Ni-Au were formed at the solder/surface finish interface, and their thickness increased with increasing aging time. The wettability of solder joints was investigated by wetting balance test. The mechanical property of each aging solder joint was evaluated by the ball shear test in accordance with JEDEC standard (JESD22-B117A). The results show that the highest shear force was measured when the aging time was 100 h, and the fracture mode changed from ductile fracture to brittle fracture with increasing aging time. On the other hand, the chloride flux in the solder paste did not affect the shear force and fracture mode of the solder joints.

• Journal of the Korean Wood Science and Technology
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• 제43권4호
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• pp.494-503
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• 2015

본 연구는 초임계 이산화탄소 추출법과 증류법에 의해 얻어진 편백 정유의 수율과 화학적 조성의 변화를 비교분석 하였다. 초임계 이산화탄소 추출은 $40^{\circ}C$, 100~400 bar의 압력범위에서 수행하였다. 편백 정유의 성분 분석은 GC-MS를 이용하여 수행하였다. 초임계 이산화탄소 추출 시 300 bar 압력에서 4.4%의 최대수율을 얻었으며 이는 증류법에 의해 얻어진 1.9% 수율에 비해 높았다. 초임계 이산화탄소 추출에 의해 얻어진 추출물은 증류법에 의한 정유에 비해 sesquiterpene류의 함량이 높았다. Sesquiterpene류는 초임계 이산화탄소 추출물의 약 39%~46%를 구성하고 있으며 monoterpenes, diterpene, lignan순으로 함유되어 있다. 추출압력에 따라 각 성분의 함유율은 차이를 보였다. 따라서 초임계 이산화탄소 추출조건은 편백 정유의 수율과 함유성분에 중요한 영향을 주는 것으로 보인다.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2012년도 제42회 동계 정기 학술대회 초록집
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• pp.250-250
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• 2012

Recently, multiferroic materials have attracted much attention due to their fascinating fundamental physical properties and potential technological applications in magnetic/ferroelectric data storage systems, quantum electromagnets, spintronics, and sensor devices. Among single-phase multiferroic materials, $BiFeO_3$, in particular, has received considerable attention because of its very interesting magnetoelectric properties for application to spintronics. Enhanced ferromagnetism was found by Fe-site ion substitution with magnetic ions. In this study, $BiFe_{1-x}Ni_xO_3$ (x=0 and 0.05) bulk ceramic compounds were prepared by solid-state reaction and rapid sintering. High-purity $Bi_2O_3$, $Fe_3O_4$ and NiO powders were mixed with the stoichiometric proportions, and calcined at $450^{\circ}C$ for 24 h to produce $BiFe_{1-x}Ni_xO_3$. Then, the samples were directly put into the oven, which was heated up to $800^{\circ}C$ and sintered in air for 20 min. The crystalline structure of samples was investigated at room temperature by using a Rigaku Miniflex powder diffractometer. The Raman measurements were carried out with a Raman spectrometer with 514.5-nm-excitation Ar+-laser source under air ambient condition on a focused area of $1-{\mu}m$ diameter. The field-dependent magnetization and the temperature-dependent magnetization measurements were performed with a vibrating-sample magnetometer. The x-ray diffraction study demonstrates the compressive stress due to Ni substitution at the Fe site. $BiFe_{0.95}Ni_{0.05}O_3$ exhibits the rhombohedral perovskite structure R3c, similar to $BiFeO_3$. The lattice constant of $BiFe_{0.95}Ni_{0.05}O_3$ is smaller than of $BiFeO_3$ because of the smaller ionic radius of Ni3+ than that of Fe3+. The field-dependent magnetization of $BiFe_{0.95}Ni_{0.05}O_3$ exhibits a clear hysteresis loop at 300 K. The magnetic properties of $BiFe_{0.95}Ni_{0.05}O_3$ were improved at room temperature because of the existence of structurally compressive stress.

• 미생물학회지
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• 제37권1호
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• pp.61-65
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• 2001

식물잎권의 잎표면세균에 대한 직접관찰과 이들을 분리시킨 용액 내 세균에 대한 간접관찰을 위하여 형광염료인 4', 6-diamidino-2-phenylindole(DAPI)와 acridine orange(AO)로 염색한 후 형광현미경을 사용하였다. AO로 염색한 잎표면은 배경형광이 진한 주홍색 이나 적색을 띠어 잎표면세균의 관잘 및 계수가 극히 힘들었으나 DAPI로 염색된 잎권세균은 뚜렷한 형광 영상을 나타내었다. 반면 잎표면세균 분리용액의 여과지에 대한 형광염색 결과는 DAPI와 AO 모두가 관찰이 가능하였다. 다만 DAPI가 AO에 비하여 형광 영상이 좀 더 뚜렷하였고 AO 염색과정에서는 염색된 여과지에 대한 세척과정이 필수적이었다. 최적의 DAPI 염색법은 잎과 여과지 모두가 5 $\mu$g/ml의 농도에서 5분 동안 염색하는 것이었다. 잎권의 형광현미경 관찰에 있어서 핵심적인 요소는 잎에서 나오는 수분을 최소화하는 것으로서 염색된 잎 시료를 거름종이 위에 올려놓고 공기 중에서 말리는 대신 $70^{\circ}C$를 유지한 건조기에서 2분 동안 말린 다음 바로 현미경으로 관찰하는 것이 가장 종은 방법인 것으로 확인되었다. 이렇게 확립된 형광현미경 관찰법을 떡갈나무의 잎권세균을 성공적으로 관찰하고 계수할 수 있었다.

• 공업화학
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• 제2권2호
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• pp.97-107
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• 1991

실리카가 많이 함유된 제올라이트 즉 silicalite(end member of ZSM-5)를 2.55 $Na_2O-5.0$ TPABr-100 $SiO_2-2800H_2O $ 조성으로 $180^{\circ}C$에서 7일간 반응시켜 합성하였다. Silicalite 합성을 위한 최초 반웅물들이 담겨진 autoclave들은 반응기간 중 고중력장을 얻기 위하여 특수제작된 열풍식 항온조 내에서 원심분리되었다. 반응은 1, 30 및 50G에서 수행되었다. 30 및 50G의 고중력하에서 합성된 silicalite의 평균 및 최대 결정크기는 동일 조건하의 1G에서 합성된 결정들보다 현저하게 증가되었고, 수율도 4 %에서 55 %정도까지 약 11배가 증가되었다. 1G에서 얻어진silicalite 결정의 평균크기는 1 일에서 7 일에 걸친 전 반응기간을 통하여 $50-70{\mu}m$에 불과한 반면, 30 및 50G에서 얻어진 결정의 평균크기는 $160-190{\mu}m$로 2-3배 증가된 결과가 나타났다. 더욱 특이할만한 현상으로 고중력하에서는 핵심생성과 결정성장이 뚜렷하게 2 단계에 걸쳐 나타남이 관측되었다. 예로써 50G하에서는 단지 2 내지 3 일간의 반응 후에 평균 $135\mu}m$ 정도의 silicalite 결정이 생성되는 비교적 빠른 제 1 성장단계(first growing stage)를 보였고, 이어 5일에 이르기까지 평균 $200{\mu}m$ 정도의 결정이 되는 매우 빠른 제 2 성장단계(second growing stage)가 관찰되었다. 위의 2 단계 결정성장과정에서 얻어진 최대결정 크기는 각각 190 및 $300{\mu}m$이었다. 고중력이 결정핵 생성, 성장, 수율 및 silicalite 결정의 크기에 미치는 영향들에 관하여 자세히 논의하였다.

• Journal of Biosystems Engineering
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• 제1권1호
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• pp.55-55
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• 1976

An experimental work was conducted to develop an optimum operating system of various hay drying systems ; sun-drying with long hay, sun-drying after chopping, sun-drying after crushing, heated air drying after chopping using batch-type dryer and heated air drying after crushing using tunnel-type dryer. Seombody having 60 cm long and initial moisture content of approximately 79 % in wet basis was used for the experiment. The criteria selected for determining the optimum operating condition were the drying performance rate, the production cost and quality of dried matter of each drying systems. The result of this study are summarized as follows : 1. Drying characteristics of leaves of long stem hay, chopped seombody and crushed one were obtained by maintaining the oven temperature at 70 degrees centigrade. The required drying times for various samples to approximately 15% moisture content in wet basis were about 50 min .for leaves ; 160 min. for crushed hay ; 250 min. for chopped hay ; 340min. for ling hay and more than 360 min .for stems. The drying time of crushed hay was required about 50 % of that for the uncrushed long hay. Such a significant difference of drying of time between the leaf and long stem may indicate that an effective drying of seombody may not be achieved unless any kind of special process treatment for the whole hay is undertaken. 2. In each individual drying system, the following conclusions were drawn: a. After 8 days sun-drying on concrete floor under good days with average tempe?rature at $256{\circ}C$ and relative humidity at 55% at 2 P.M., the moisture content of long hay was still above 25 5'~ and the leaf loss during drying caused by wind and rough handling was more than 50 ~G. b. It was possible to dry the chopped seombody by sun-drying down to about 10 % moisture content within 5 days, however, a stock of heat and discolouration phenomena were observed during the drying, which may be due to the increased deposit-density by chopping, resulting in lowering the quality of the dried product. c. Sun-drying for the crushed material by hay-conditioner was required about 4 days to reduce the moisture content to about 10 %, keeping the quality of dried product at good grade. o. The optimum deposit-depth of the chopped seombody in the batch-type dryer used was about 28cm with about 42kg/hr of drying performance rate. However, it was necessary to overturn the materials between the upper and lower layers in order to obtain a good quality of dried product. d. The drying performance rate by the tunnel-type drier was highest among those of drying systems tested, giving the rate of approximately 400kg/day. 3. On reviewing the individual drying system for seombody, it was possible to draw conclusion that the best system was tunnel drying with the crushed seombody as far as the performance rate was concerned. However, the methods gives the highest operational cost. The system for the lowest operational cost with good quality of dried product was the sun-drying with the crushed material. Accordingly, it may be recommended that the system of sun-drying for the crushed seombody may be the most feasible system presently applicable to farm-level operation.

• Journal of Biosystems Engineering
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• 제1권1호
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• pp.56-63
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• 1976

An experimental work was conducted to develop an optimum operating system of various hay drying systems ; sun-drying with long hay, sun-drying after chopping, sun-drying after crushing, heated air drying after chopping using batch-type dryer and heated air drying after crushing using tunnel-type dryer. Seombody having 60 cm long and initial moisture content of approximately 79 % in wet basis was used for the experiment. The criteria selected for determining the optimum operating condition were the drying performance rate, the production cost and quality of dried matter of each drying systems. The result of this study are summarized as follows : 1. Drying characteristics of leaves of long stem hay, chopped seombody and crushed one were obtained by maintaining the oven temperature at 70 degrees centigrade. The required drying times for various samples to approximately 15% moisture content in wet basis were about 50 min .for leaves ; 160 min. for crushed hay ; 250 min. for chopped hay ; 340min. for ling hay and more than 360 min .for stems. The drying time of crushed hay was required about 50 % of that for the uncrushed long hay. Such a significant difference of drying of time between the leaf and long stem may indicate that an effective drying of seombody may not be achieved unless any kind of special process treatment for the whole hay is undertaken. 2. In each individual drying system, the following conclusions were drawn: a. After 8 days sun-drying on concrete floor under good days with average tempe\ulcornerrature at $256{\circ}C$ and relative humidity at 55% at 2 P.M., the moisture content of long hay was still above 25 5'~ and the leaf loss during drying caused by wind and rough handling was more than 50 ~G. b. It was possible to dry the chopped seombody by sun-drying down to about 10 % moisture content within 5 days, however, a stock of heat and discolouration phenomena were observed during the drying, which may be due to the increased deposit-density by chopping, resulting in lowering the quality of the dried product. c. Sun-drying for the crushed material by hay-conditioner was required about 4 days to reduce the moisture content to about 10 %, keeping the quality of dried product at good grade. o. The optimum deposit-depth of the chopped seombody in the batch-type dryer used was about 28cm with about 42kg/hr of drying performance rate. However, it was necessary to overturn the materials between the upper and lower layers in order to obtain a good quality of dried product. d. The drying performance rate by the tunnel-type drier was highest among those of drying systems tested, giving the rate of approximately 400kg/day. 3. On reviewing the individual drying system for seombody, it was possible to draw conclusion that the best system was tunnel drying with the crushed seombody as far as the performance rate was concerned. However, the methods gives the highest operational cost. The system for the lowest operational cost with good quality of dried product was the sun-drying with the crushed material. Accordingly, it may be recommended that the system of sun-drying for the crushed seombody may be the most feasible system presently applicable to farm-level operation.

• Journal of Biosystems Engineering
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• 제43권3호
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• pp.237-246
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• 2018

Purpose: This study (a) investigated the effect of microwave power intensity and sample thickness on microwave drying characteristics of radish strips, and (b) determined the best-fit drying model for describing experimental drying data, effective moisture diffusivity ($D_{eff}$), and activation energy ($E_a$) for all drying conditions. Methods: A domestic microwave oven was modified for microwave drying and equipped with a small fan installed on the left upper side for removing water vapor during the drying process. Radishes were cut into two fixed-size strip shapes (6 and 9 mm in thickness). For drying experiments, the applied microwave power intensities ranged from 180 to 630 W at intervals of 90 W. Six drying models were evaluated to delineate the experimental drying curves of both radish strip samples. The effective moisture diffusivity ($D_{eff}$) was determined from Fick's diffusion method, and the Arrhenius equation was applied to calculate the activation energy ($E_a$). Results: The drying time was profoundly decreased as the microwave power intensity was increased regardless of the thickness of the radish strips; however, the drying rate of thicker strips was faster than that of the thinner strips up to a certain moisture content of the strip samples. The majority of the applied drying models were suitable to describe the drying characteristics of the radish strips for all drying conditions. Among the drying models, based on the model indices, the best model was the Page model. The range of estimated $D_{eff}$ for both strip samples was from $2.907{\times}10^{-9}$ to $1.215{\times}10^{-8}m^2/s$. $E_a$ for the 6- and 9-mm strips was 3.537 and 3.179 W/g, respectively. Conclusions: The microwave drying characteristics varied depending on the microwave power intensity and the thickness of the strips. In order to produce high-quality dried radish strips, the microwave power intensity should be lower than 180 W.

• Journal of Animal Science and Technology
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• 제50권2호
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• pp.237-246
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• 2008

미트로프 제품에 열풍건조 단감분말(HP)과 동결건조 단감분말(FP)을 각각 3%(HP-3%, FP-3%)와 6%(HP-6%, FP-6%)를 첨가하도, 무첨가구를 대조구로 제조한 후 함기포장하여 5℃에 저장하면서 품질평가를 실시하였다. 수분과 조회분은 FP-6%가 유의적으로 높았고(p<0.05), 조단백질 및 조지방은 모든 제품에서 유의적인 차이가 없었다(p>0.05). pH는 대조구가 처리구보다 높았으며(p<0.05), 처리구간에서는 차이가 없었다(p>0.05). 모든 제품에서 저장기간이 경과함에 따라 TBARS값은 증가하는 경향이었으며, 처리구들 간에서는 HP-6%와 FP-6%가 유의적으로 높게 나타났다(p<0.05). 각 소재물들의 첨가비율이 높을수록 높은 TBARS와 적색도는 증가하였다. 미생물 분석결과 저장 전 기간 동안 모든 제품에서 총균수는 3.11 log10 CFU/g를 유지하여 양호하였다. 전체적인 기호도는 대조구에 비해 처리구들이 더 좋았고 첨가량에 의한 차이는 없었다(p>0.05). 이상의 결과로써 다양한 생리활성물질을 가지는 열풍 또는 동결건조 단감분말은 기능성 식품의 소재로써 미트패티류 제품에 적용할 수 있음을 확인하였다.