• 제목/요약/키워드: optimum measurement

검색결과 703건 처리시간 0.046초

적외선 센서 재료로 사용되는 고순도 ZnTe박막의 평가 (Evaluation of the High Purity ZnTe which is an Far-Infrared Sensor Material)

  • Kim, B.J.
    • 한국표면공학회지
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    • 제35권5호
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    • pp.305-311
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    • 2002
  • Optical measurements have been used to study the biaxial tensile strain in heteroeptaxial ZnTe epilayers on the (100) GaAs substrate by hot wall epitaxy (HWE) with Zn reservoir. It is effect on the low-temperature photoluminescence spectrum of the material. Optimum growth condition has been determined by a four-crystal rocking curve (FCRC) and a low temperature photoluminescence measurement (PL). It was found that Zn partial pressure from Zn reservoir has a strong influence on the quality of grown films. Under the determined optimum growth condition, ZnTe epitaxial films with thickness of 0.72~24.8$\mu\textrm{m}$ were grown for studying the effect of the thickness on crystalline quality. The PL and FCRC results indicated that the quality of ZnTe films becomes higher rapidly with increase of thickness up to 6$\mu\textrm{m}$. The best value of the FWHM of the four crystal rocking curve, 66 arcsec, was obtained on the film with 12$\mu\textrm{m}$ in thickness. The PL spectrum shows the splitted strong free exciton emissions and very weak deep band emissions. These results show the high quality of films.

레이저빔 조사에 의한 압력용기용 강의 피로강도 향상방법 개발 (Fatigue Strength Improvement of Pressure Vessel Steel by Lasler Beam Radiation)

  • 권재도;진영준;김상태;최선호
    • 대한기계학회논문집
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    • 제18권2호
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    • pp.519-528
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    • 1994
  • Degradation problem due to long term service in machine or structure is now one of important problems in whole industrial field. In this study, pressure vessel steel, Cr-Mo steel, which was used more than 60,000 hours, was surface-modified by laser beam radiation for the improvement of fatigue strength. To find out optimum radiation condition, hardness, residual stress measurement and fatigue tests were carried out with the specimen of different radiation conditions. Experimental results show that micro-hardness values on the surface of the radiated specimens were approximately 2.2 times higher than those of un-radiated ones. In the depth direction of the specimen, hardness on the surface showed maximum value and was decreased at the inside the specimen. Different hardness values are due to the energy density Q which was absorbed by the specimen. Fatigue tests show that fatigue life was improved by the compressive residual stress after laser beam radiation. However, some specimens with differednt conditions show the shorter fatigue life. It means that laser beam radiation with optimum parameter can improve thae fatigue strength.

해양구조물용 RE36강 용접부의 부식거동 및 기계적 특성에 미치는 용접후 열처리 효과에 관한 연구 (A Study on the Post-Weld Heat Treatment Effect Affecting Corrosion Behavior and Mechanical Property of Welding Part of RE36 Steel for Marine Structure)

  • 김성종;문경만
    • Journal of Welding and Joining
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    • 제19권1호
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    • pp.65-74
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    • 2001
  • A study on the corrosion behavior in case of As-welded and PWHT temperature 55$0^{\circ}C$ of welding part of RE36 steel for marine structure was investigated with parameters such as micro-Vickers hardness, corrosion potential measurement of weld metal(WM), base metal(BM) and heat affected zone(HAZ), both Al anode generating current and Al anode weight loss quantity under sacrificial anode cathodic protection conditions. And also we carried out slow strain rate test(SSRT) in order to research both limiting cathodic polarization potential for hydrogen embrittlement and optimum cathodic protection potential as well as mechanical properties by post-weld heat treatment(PWHT) effect. Hardness of HAZ was the highest among three parts(WM, BM and HAZ) and the highest galvanic corrosion susceptibility was HAZ. And the optimum cathodic polarization potential showing the best mechanical properties by SSRT method was from -770mV to -875mV(SCE). In analysis of SEM fractography, applied cathodic potential from -770mV to -875mV(SCE) it appeared dimple pattern with ductile fracture while it showed transgranular pattern (Q. C : quasicleavage) under -900mV(SCE). However it is suggested that limiting cathodic polarization potential indicating hydrogen embrittlement was under -900mV(SCE).

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국보 제24호 석굴암의 보존환경 (Investigation on Conservation Environment of the Seokguram Grotto (National Treasure No. 24))

  • 홍정기;엄두성
    • 보존과학연구
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    • 통권24호
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    • pp.169-184
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    • 2003
  • Yearly mean temperature and relative-humidity of the Seokguram Grotto was measured $19~23^{\circ}C$, 40~44% from May, 1998 to December,2002. The measurement has little differences comparing to the optimum guideline (temperature : $20^{\circ}\pm2^{\circ}C$, relative-humidity : $50^{\circ}\pm5%$). It is necessary to increase humidity in the Seokguram Grotto during winter because of heating and decrease the temperature during summer because of a higher temperature of outside. In addition, the diurnal range keep in $4^{\circ}C$ of temperature and in 10% of relative-humidity. Yearly mean concentration of $CO_2$(carbon dioxide) was measured538~658ppm that is higher than concentration of normal atmosphere(360 ppm). The $CO_2$ has an cumulative effect on the surface of stone cultural properties as a form of carbonic acid($H_2CO_3$) after reaction with water. HVAC (Heating, Ventilation and Air Conditioning) system should be operated to maintain ideal state for the preservation according to the optimum guideline. Also, the entrance into the Seokguram Grotto should be controlled to prevent a sudden fluctuation of humidity and temperature. Human could carry small particles like a microdust, microbe, etc., into the Seokguram Grotto and also could damage the surface by a direct touch.

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마이크로 스펙트로미터 적외선 센서용 저응력 SiNx Membrane상에서의 최적화된 Thermopile 제작 및 특성 (Characteristics and Fabrication of Optimal Thermopile on SiNx Membrane for Microspectrometer)

  • 김동식
    • 전자공학회논문지 IE
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    • 제44권1호
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    • pp.6-9
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    • 2007
  • 본 연구는 마이크로 스펙트로미터 적외선 센서용으로 thermopile 소자 구조를 이용하여 설계, 제작되어 특성을 평가하였다. MEMS 공정기술을 이용하여 열적 고립 구조를 갖는 Low-stress SiNx 멤브레인상에서 마이크로 thermopile 적외선 센서를 제작하고 특성을 평가하였다. 마이크로 thermopile 적외선 센서를 측정한 결과 열전대 길이, 개수, 멤브레인 넓이에 기전력이 비례하여 출력되고 열전대 물질의 선폭에는 반비례하는 것으로 나타났다. 5가지 요소를 독립적으로 변화시켜 측정한 결과 마이크로 thermopile 적외선 센서는 멤브레인 넓이가 다른 요소에 비해 더 큰 영향을 미쳤다. 이러한 결과로 미루어 본 연구에서 제작된 마이크로 thermopile 적외선 센서는 마이크로 스펙트로미터용 적외선 센서로서 활용이 가능할 것으로 생각되었다.

전기화학형 광전변환 셀의 고효율 전해질 제작에 관한 실험적 고찰 (Experimental Investigation on High Efficient Electrolytes of Electrochemical Photovoltaic Cells)

  • 김두환;한치환;성열문
    • 전기학회논문지
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    • 제60권1호
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    • pp.100-104
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    • 2011
  • In this work, an optimum condition of electrolytes preparation for photovoltaic cells application was investigated experimentally in terms of impedance and conversion efficiency of the cells. 3-methoxyppropionitrie and redox pairs with LiI and $I_2$ were used as stable solvents for fabrication of electrolyte. Efficiency comparison of the prepared cells carried out for various additives and ionic liquids. From the results, there was an optimum concentration (about 0.3 M) of ionic liquids for efficient cell fabrication. For case of electrolyte using single DMAp additive, the maximum conversion efficiency of the cell was 6.4%($V_{oc}$: 0.78V, $J_{sc}$: 14.4 mA/$cm^2$, ff: 0.57). For case of electrolyte using both DMAp and CEMim additives, the maximum conversion efficiency of the cell was 7.2%($V_{oc}$: 0.79V, $J_{sc}$: 16 mA/$cm^2$, ff: 0.57). From the result of electrochemical impedance measurement, both Z1 and Z3 values of binary additives-based cell decreased compared to those of single additive-based. This is due to the decreased in internal and charge transfer resistivities of the cells.

에너지스펙트럼 분석을 통한 폴리스타이렌 기반 플라스틱 섬광체의 파장쉬프터 비율 최적화 (Optimization of the Wavelength Shifter Ratio in a Polystyrene Based Plastic Scintillator through Energy Spectrum Analysis)

  • 김예원;문명국;김명수;유현준;이대희;조규성
    • 방사선산업학회지
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    • 제10권4호
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    • pp.167-171
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    • 2016
  • The scintillation efficiency of the polystyrene based plastic scintillator depends on the ratio of the wavelength shifters, organic fluors(PPO and POPOP). Thus, 24 samples of the plastic scintillator were fabricated in order to find out the optimum ratio of the wavelength shifters in the plastic scintillator. The fabricated plastic scintillators were trimmed through a cutting and polishing process. They were used in gamma energy spectrum measurement with the $^{137}Cs$ emitting mono-energy photon with 662 keV for the comparison of the scintillation efficiency. As a result, it was found out that the scintillator sample with 1.00 g of PPO (2,5-Diphenyloxazole) and 0.50 g of POPOP (1,4-Bis(5-phnyl-2oxidazolyl)benzene) dissolved in 100 g of styrene solution has the optimum ratio in terms of the light yield of the polystyrene based plastic scintillator.

배양기간, 온도, pH가 인삼 근부병균 Cylindrocarpon destructans (Zinssm.) Scholten의 균사생육에 미치는 영향 (Effect of Incubation Period, Temperature and pH on Mycelial Growth of Cylindrocarpon destructans (Zinssm.) Scholten Causing Root-rot of Ginseng)

  • 조대휘;안일평
    • Journal of Ginseng Research
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    • 제19권2호
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    • pp.181-187
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    • 1995
  • Cylindvocarpon destmtalns isolate CY-92-01, pathogen of root-rot of Panax ginseng showed t the maximum mycelial growth on the Czapek solution agar among the thirteen kinds of media. Five isolates (Isolate CY-92-01, CY-92-03, CY-92-07, CY-94-01, CY-94-02) of C. destructan from various growth stages of p. ginseng recovered from several geographical sites also showed maximum growth in the Czapek-Dox broth compared with potato dextrose broth and V-8 juice broth. Rapid growth rate was maintained until 12 days after inoculation on the Czapek-Dox broth and mycelial weight was somewhat constant until 20 days. After 30 days of incubation, the mycelial weight began to decrease. The fungal growth occurred from 5$^{\circ}C$ to $25^{\circ}C$ and optimum temperature for growth was 2$0^{\circ}C$. Mycelial weight orderly decreased at 15, 25, 10, and 5$^{\circ}C$. Quantitative measurement was impossible at 5$^{\circ}C$. No fungal growth was occurred at the temperature higher than 3$0^{\circ}C$. Growth was observed at all tested pH ranges from 2.8 to 8.0. Optimum pH for growth was 4.0~5.0 followed by pH 3.3~3.5 and 5.4~6.0. The least growth occurred at pH 2.8.

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Characterization of jute fibre reinforced pine rosin modified soy protein isolate green composites

  • Sakhare, Karishma M.;Borkar, Shashikant P.
    • Advances in materials Research
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    • 제11권3호
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    • pp.191-209
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    • 2022
  • Very slow degradation of synthetic based polymers has created a severe environmental issue that increased awareness towards research in polymers of biodegradable property. Soy protein isolate (SPI) is a natural biopolymer used as matrix in green composites but it has limitations of low mechanical properties and high water sensitivity. To enhance mechanical properties and reduce water sensitivity of Jute-SPI composites, SPI was modified with pine rosin which is also a natural cross-linking agent. 30% glycerol on the weight basis of a matrix was used as a plasticizer. The fibre volume fraction was kept constant at 0.2 whereas the pine rosin in SPI ranged from 5% to 30% of the matrix. The effects of pine rosin on mechanical, thermal, water sensitivity and surface morphology have been characterized using various techniques. The mechanical properties and water absorbency were found to be optimum for 15% pine rosin in Jute-SPI composite. Therefore, Jute-SPI composite without pine rosin and with 15% pine rosin were chosen for investigation through characterization by Fourier transforms infrared spectroscopy (FTIR), Thermo-gravimetric analysis (TGA), X-Ray diffraction (XRD) and Scanning electron microscope (SEM). The surface morphology of the composite was influenced by pine rosin which is shown in the SEM image. TGA measurement showed that the thermal properties improved due to the addition of pine rosin. Antimicrobial test showed antimicrobial property in the composite occurring 15% pine rosin. The research paper concludes that the modification of SPI resin with an optimum percentage of pine rosin enhanced mechanical, thermal as well as water-resistant properties of jute fibre reinforced composites.

시험시간 관련인자가 로크웰 경도측정에 미치는 영향 (Effect of Time-Related Parameters on Rockwell Hardness Measurement)

  • 방건웅;탁내형
    • 폴리머
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    • 제29권6호
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    • pp.536-542
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    • 2005
  • 로크웰 경도시험 조건 중에서 시간과 관련이 있는 인자들이 경도측정 결과에 미치는 영향을 연구하였다. 대상 소재는 PE, PP PVC, PMMA이었으며 압입속도, 시험하중 유지시간, 그리고 계기판독 시점 등을 중심으로 시험한 결과 탄성이 큰 소재일수록 이들 인자들의 영향을 크게 받는 것으로 나타났다. 시험에 소요되는 시간 등을 고려하였을 때 최적 시험 조건은 각기 4, 15, 15초 이었으며 이 기준에 따라 순회 비교시험을 실시하였다. 순회 비교시험 결과 고분자소재의 경도를 제대로 측정하려면 부가하중을 제하하고 나서 계기판독 시점인 15초의 시간을 유지할 수 있는 기능이 중요한 것으로 나타났다. 황동 기준편으로 경도시험기를 간접 검증하는 것만으로는 탄성 회복력이 좋은 고분자 소재의 특성 때문에 경도 측정값의 신뢰도를 보증할 수 없는 것으로 나타났다.