• Title/Summary/Keyword: optical constant

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Fluctuation in Plasma Nanofabrication

  • Shiratani, Masaharu
    • Proceedings of the Korean Vacuum Society Conference
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    • 2016.02a
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    • pp.96-96
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    • 2016
  • Nanotechnology mostly employs nano-materials and nano-structures with distinctive properties based on their size, structure, and composition. It is quite difficult to produce nano-materials and nano-structures with identical sizes, structures, and compositions in large quantities, because of spatiotemporal fluctuation of production processes. In other words, fluctuation is the bottleneck in nanotechnology. We propose three strategies to suppress such fluctuations: employing 1) difference between linear and nonlinear phenomena, 2) difference in time constants, and 3) nucleation as a bottleneck phenomenon. We are also developing nano- and micro-scale guided assembly using plasmas as a plasma nanofabrication.1-5) We manipulate nano- and micro-objects using electrostatic, electromagnetic, ion drag, neutral drag, and optical forces. The accuracy of positioning the objects depends on fluctuation of position and energy of an object in plasmas. Here we evaluate such fluctuations and discuss the mechanism behind them. We conducted in-situ evaluation of local plasma potential fluctuation using tracking analysis of fine particles (=objects) in plasmas. Experiments were carried out with a radio frequency low-pressure plasma reactor, where we set two quartz windows at the top and bottom of the reactor. Ar plasmas were generated at 200 Pa by applying 13.56MHz, 450V peak-to-peak voltage. The injected fine particles were monodisperse methyl methacrylate-polymer spheres of $10{\mu}m$ in diameter. Fine particles were injected into the reactor and were suspended around the plasma/sheath boundary near the powered electrode. We observed binary collision of fine particles with a high-speed camera. The frame rate was 1000-10000 fps. Time evolution of their distance from the center of mass was measured by tracking analysis of the two particles. Kinetic energy during the collision was obtained from the result. Potential energy formed between the two particles was deduced by assuming the potential energy plus the kinetic energy is constant. The interaction potential is fluctuated during the collision. Maximum amplitude of the fluctuation is 25eV, and the average is 8eV. The fluctuation can be caused by neutral molecule collisions, ion collisions, and fluctuation of electrostatic force. Among theses possible causes, fluctuation of electrostatic force may be main one, because the fine particle has a large negative charge of -17000e and the corresponding electrostatic force is large compared to other forces.

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A Study on Evaporative Characteristics of Multi-component Mixed Fuels Using Mie Scattered Light and Shadowgraph Images (Mie 산란광법 및 Shadowgraph법을 이용한 다성분 혼합연료의 증발특성연구)

  • Yoon, Jun-Kyu;Myong, Kwang-Jae;Jiro Senda;Fujimoto Hajime;Cha, Kyung-Ok
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.30 no.7 s.250
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    • pp.682-691
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    • 2006
  • This study was conducted to assess the effect of mixed fuel composition and mass fraction on spray inner structure in evaporating transient spray under the various ambient conditions. Spray structure and spatial distribution of liquid phase concentration are investigated using a thin laser sheet illumination technique on the multi-component mixed fuels. A pulsed Ar+ laser was used as a light source. The experiments were conducted in a constant volume vessel with optical access. Fuel was injected into the vessel with electronically controlled common rail injector. Used fuel contain $i-octane(C_8H_{18}),\;n-dodecane(C_{12}H_{26})$ and $n-hexadecane(C_{16}H_{34})$ that are selected as low-, middle- and high-boiling point fuel, respectively. Experimental conditions are 25Mpa, 42MPa, 72MPa and 112MPa in injection pressure, $5kg/m^3,\;15kg/m^3\;and\;20kg/m^3$ in ambient gas density, 400K, 500K, 600K and 700K in ambient gas temperature, 300K and 368K in fuel temperature, and different fuel mass fraction. Experimental results indicate that the more high-boiling point component, the longer the liquid phase it were closely related to fuel physical properties, but injection pressure had no effect on. And there was a high correlation between the liquid phase length and boiling temperature at 75% distillation point.

Light Propagation in Multimode GRIN(graded-index) Fibers with Intrusion Sensing Capability (침입 감지기능을 가진 다중모드 GRIN(graded-index) 광섬유 내에서의 광파의 전파)

  • Sohn, Young-Ho
    • Journal of Sensor Science and Technology
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    • v.11 no.5
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    • pp.273-278
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    • 2002
  • An intrusion-sensitive capability of multimode graded-index (GRIN) optical fibers under bending has been investigated. In this system, the data light is transmitted in the fundamental mode while alarm monitor light is launched in a high-order mode at the same time. An attempted intrusion to drain data by bending the fiber results in greater attenuation of a monitor signal in higher order modes, thereby setting off an alarm at the receiver. Light propagation in a multimode graded-index fiber is also analyzed theoretically when the fundamental mode is selectively excited and the fiber is bent around a constant radius mandrel. The bending generates coupling between the various modes of the fiber. Power transitions of the fundamental mode by changing the bending radius were also analyzed numerically using program simulation. It is shown that Asawa-Taylor model[4] is valid up to 1cm of the radius of curvature of the fiber bend.

Theoretical analysis of the lightwave localization phenomenon on the random transmission line (part 1) : localization characteristics of the solution of propagation equation (랜덤 선로상의 광 국재현상에 관한 해석(1) : 해의 국재성에 대한 이론적 고찰)

  • 최영규
    • Korean Journal of Optics and Photonics
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    • v.14 no.4
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    • pp.429-433
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    • 2003
  • We try to analyse the localization phenomenon of a lightwave in random media by means of considering the solution of the propagation equation on a transmission line in which the propagation constants are randomly distributed. Lightwave localization is generated at the turning point where the solution is changed suddenly from an increase to a decrease. First, in order to investigate the changing process of the solution, we have derived the approximated one-dimensional Schrodinger equation from the two-dimensional wave equation by using the Brags condition. Considering the many types of solutions of the wave equation, we have investigated the conditions that allow the solutions to exist. Also, we have investigated the relationships between the localization of the solution and the variation of the propagation constant. In case of the exponential solution, we know that the permittivity $\varepsilon$=(0,0$\varepsilon$$_{0}$) is a very important parameter to influence the phase of the lightwave and to generate the localization.

AN EXPERIMENTAL STUDY ON THE FATIGUE FRACTURE OF LAMINATE PORCELAIN (치과용 라미네이트 도재의 피로파괴에 관한 실험적 연구)

  • Park Charn-Woon;Bae Tae-Sung;Lee Sang-Don
    • The Journal of Korean Academy of Prosthodontics
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    • v.31 no.4
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    • pp.482-505
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    • 1993
  • The purpose of this study was to evaluate the fracture characteristics and the effect of resin bonding of laminate porcelain. In order to characterize the indentation-induced crack, Young's moduli and characteristic indentation dimensions were measured. The fatigue life under three point flexure test was measured using the electro-dynamic type fatigue machine, and the crack propagation with thermocycling was investigated on the condition of 15 second dwell time each in $5^{\circ}C\;and\;55^{\circ}C$ bath. The Vickers indentation pattern and the fracture surface were examined by an optical microscope and a scanning electron microscope (SEM). The results obtained were summarized as follows ; 1. Young's moduli(E) of the laminate porcelain and the resin cement used in this experiment were $62.56{\pm}3.79GPa$ and $15.01{\pm}0.12GPa$, respectively. 2. The initial crack size of the laminate porcelain was $69.19{\pm}5.94{\mu}m$ when an indentation load of 9.8N was applied, and the fracture toughness was $1.065{\pm}0.156MPa\;m^{1/2}$. 3. The fatigue life of laminate porcelain showed the constant fracture range at the stress level 27.46-35.30MPa. 4. When a cyclic flexure load was applied, the fatigue life of resin-bonded laminate porcelain was more decreased than that of laminate porcelain. 5. When a thermocycling was conducted, the crack growth rate of resin-bonded laminate porcelain was more increased than that of laminate porcelain. 6. Fracture surface showed the radial crack, the lateral crack, and the macroscopic crack branching region beneath the plastic deformation region when an indentation load of 9.8N was applied.

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Effect of Zirconia Addition on Mechanical Properties of Spinel/Zirconia-glass Dental Crown Composites Prepared by Melt-infiltration (용융침투법으로 제조한 인공치관용 스피넬/지르코니아-유리 복합체의 기계적 특성에 미치는 지르코니아 첨가효과)

  • Lee, Deuk-Yong;Kim, Byung-Soo;Jang, Joo-Wung;Lee, Myung-Hyun;Park, Il-Seok;Kim, Dae-Joon
    • Journal of the Korean Ceramic Society
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    • v.39 no.11
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    • pp.1028-1034
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    • 2002
  • Spinel/zirconia-glass composites prepared by melt-infiltration were fabricated to investigate the effect of zirconia addition on mechanical and optical properties of the composites. The infiltration distance was parabolic with respect to time as described by the Washburn equation and the penetration rate constant, K, decreased due to the reduction in pore size as the amount of zirconia rose. Although the optimum strength(308 MPa) of the Spinel/zirconia-glass composites was observed when the zirconia was added up to 20 wt%, K and transmittance decreased as the zirconia content rose. In conclusion, it suggested that the positive effect of strength as a result of the addition of zirconia was not effective.

A Study on the Characteristics of Delayed Hydride Cracking in Zr-2.5Nb Pressure Tube with the Heating-up and Heat-treatment (열처리 및 가열방식에 따른 Zr-2.5Nb 압력관의 수소지연균열 특성에 관한 연구)

  • Na, Eun-Young
    • Journal of Ocean Engineering and Technology
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    • v.23 no.2
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    • pp.69-73
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    • 2009
  • The objective of this study was to obtain a better understanding of the delayed hydride cracking (DHC) of Zr-2.5Nb alloy. The DHC model has some defects: first, it cannot explain why the DHC velocity (DHCV) becomes constant regardless of an applied stress intensity factor, even though the stress gradient is affected by the applied stress intensity factor at the notch tip. Second, it cannot explain why the DHCV has a strong dependence on the method of approaching the test temperature by a cool-down or a heating-up, even under the same stress gradient, and third, it cannot predict any hydride size effect on the DHC velocity. The DHC tests were conducted on Zr-2.5Nb compact tension specimens with the test temperatures reached by a heating-up method and a cool-down method. Crack velocities were measured in hydrided specimens, which were cooled from solution-treatment temperatures at different rates by being furnace-cooled, water-quenched, and liquid nitrogen-quenched. The resulting hydride size, morphology, and distributions were examined by optical metallography. It was found that fast cooling rates, which produce very finely dispersed hydrides, result in higher crack growth rates. This different DHC behavior of the Zr-2.5Nb tube with the cooling rate after a homogenization treatment is due to the precipitation of the $\gamma$-hydrides only in the water-quenched Zr-2.5Nb tube. This experiment will provide supporting evidence that the terminal solid solubility of a dissolution (TSSD) of $\gamma$-hydrides is higher than that of $\delta$-hydrides.

A Comparative Study on the Marginal Fit between Castable Ceramic(Dicor) Crowns and Metal-Ceramic Crowns (주조도재관과 도재전장주조관의 치경부 변연적합도에 관한 비교 연구)

  • Kim, Jeong-Ho;Yang, Jae-Ho;Lee, Sun-Hyung
    • The Journal of Korean Academy of Prosthodontics
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    • v.26 no.1
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    • pp.51-61
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    • 1988
  • The recently introduced castable glass ceramics incorporate properties characteristic of natural teeth and they are regarded as an ideal material to restore lost tooth structure. The purpose of this study was to compare the marginal fit of castable ceramic crown with that of the metal-ceramic crown in the process of heat treatment. Two master dies for castable ceramic crowns and metal-ceramic crowns were fabricated from being cast with the base metal. Each master die was duplicated with addition silicone and hard stone. Ten castable ceramic crowns were made on each hard stone die and their marginal openings were measured three times first, after casting; second, after ceramming; third, after shading. The other ten metal-ceramic crowns were made on each hard stone die and their marginal openings were measured three times : first, after casting; second, after degassing; third, after porcelain veneering. Each crown was seated on its master die with the constant force delivered by loading jig. And then, marginal openings were measured on four locations by optical projector at X50 magnification. The results were as follows: 1. The mean marginal openings of castable ceramic crowns were $31.1{\pm}12.7{\mu}m$ after casting; $44.6{\pm}12.8{\mu}m$ after ceramming; $51.2{\pm}16.8{\mu}m$ after shading. 2. The mean marginal openings of the metal-ceramic crowns were $26.2{\pm}13.8{\mu}m$ after casting; $29.8{\pm}10.3{\mu}m$ after degassing; $38.0{\pm}14.5{\mu}m$ after porcelain veneering. 3. There was significant increase in the marginal opening of castable ceramic crowns after ceramming, while metal-ceramic crowns sho(wed significant increase after porcelain veneering (p<0.05). 4. Marginal fit of metal-ceramic crown was better than that of castable ceramic crown (p<0.01).

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Development of a 6 degrees-of-freedom micro stage for ultra precision positioning (초정밀작업을 위한 6자유도 마이크로 스테이지의 개발)

  • Kim, Kyung-Chan;Kim, Soo-Hyun;Kwak, Yoon-Keun
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.22 no.2
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    • pp.372-379
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    • 1998
  • A new 6 degrees-of-freedom micro stage, based on parallel mechanisms and actuated by using piezoelectric elements, has been developed for the application of micro positioning such as semiconductor manufacturing devices, high precision optical measurement systems, and high accurate machining. The micro stage structure consists of a base platform and an upper platform(stage). The base platform can effectively generates planar motion with yaw motion, while the stage can do vertical motion with roll and pitch motions with respect to the base platform. This separated structure has an advantage of less interference among actuators. The forward and inverse kinematics of the micro stage are discussed. Also, through linearization of kinematic equations about an operating point on the assumption that the configuration of the micro stage remains essentially constant throughout a workspace is performed. To maximize the workspace of the stage relative to fixed frame, an optimal design procedure of geometric parameter is shown. Hardware description and a prototype are presented. The prototype is about 150mm in height and its base platform is approximately 94mm in diameter. The workspace of the prototype is obtained by computer simulation. Kinematic calibration procedure of the micro stage and its results are presented.

Experimental Study to Examine Wear Characteristics and Determine the Wear Coefficient of Ductile Cast Iron (DCI) Roll (Ductile Cast Iron (DCI) 롤의 마모 특성 고찰 및 마모계수 도출을 위한 실험적 연구)

  • Byon, Sang-Min
    • Tribology and Lubricants
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    • v.33 no.3
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    • pp.98-105
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    • 2017
  • A pin-on-disk test is performed to measure the wear volume of a ductile cast iron (DCI) roll when it wears down using a high carbon steel and two alloy steels at different sliding velocities between the roll and the material (steel). Normal pressure is set as constant and test temperatures are 400, 500 and $600^{\circ}C$. In addition, thermal softening behavior of the DCI roll is examined using a high-temperature micro-hardness tester and the surface hardness variation of the DCI roll is expressed in terms of temperature and heating time. Based on experimental data, a wear coefficient used in Archard's wear model for each material is obtained. The wear volume is clearly observed when the test temperature is $400^{\circ}C$ and sliding velocity varies. However, it is not measured at temperatures of $500^{\circ}C$ and $600^{\circ}C$ even with variations in sliding velocity. From the optical photographs of the pin and disk, the abrasive wear is observed at $400^{\circ}C$ clearly, but no at $500^{\circ}C$ and $600^{\circ}C$. At higher temperatures, the pin surface is not smooth and has many tiny caves distributed on it. It is found that wear volume is dependent on the carbon contents rather than alloy contents. Results also reveal that the variations of wear coefficients are almost linearly proportional to the carbon contents of the material.