• Bulletin of the Korean Chemical Society
• /
• 제22권2호
• /
• pp.159-163
• /
• 2001

Si3N4 powder has been analyzed by inductively coupled plasma atomic emission spectrometry (ICP-AES). The sample was dissolved by high-pressure acid digestion with HF, H2SO4 (1+1), and HNO3 mix ture. This technique is well suited for the impurity analysis of Si3N4 because the matrix interference is eliminated. A round-robin samples trace elements, such as Ca, W, Co, Al, Fe, Mg, and Na, were determined. For the direct analysis, slurry nebulization of 0.96 mm Si3N4 powder also has been studied by ICP-AES. Emission intensities of Fe were measured as ICP operational conditions were changed. Significant signal difference between slurry particles and aqueous solution was observed in the present experiment. Analytical results of slurry injection and high-pressure acid digestion were compared. For the use of aqueous standard solution for calibration, k-factor was determined to be 1.71 for further application.

• 한국초지조사료학회지
• /
• 제31권4호
• /
• pp.415-422
• /
• 2011

본 연구는 최근 조사료의 신속한 품질평가 방법으로 근적외선 분광법의 이용성이 확대되고 있는 시점에 근적외선 분광기의 현장 적용성을 평가하기 위하여 수행되었다. 실험실용 근적외선분광기와 소형 근적외선분광기의 조사료 품질평가의 예측 정확성을 평가하기 위하여 전남지역에서 이탈리안 라이그라스 사일리지 67점을 수집하여 각각의 근적외선 분광기를 이용하여 스펙트럼을 측정한 후 사료가치의 실험실 분석값과 다변량회귀분석을 통하여 검량식을 유도하여 예측 정확성을 평가하였다. 이탈리안 라이그라스 사일리지의 수분함량에 대한 예측정확성은 실험실용 근적외선분광기와 소형근적외선분광기에서 각각 SEC = 2.50% ($R^2$=0.96), SEC = 2.83% ($R^2$=0.95)로 매우 신뢰성이 우수한 결과를 나타내었으나 사일리지의 발효품질의 주요 평가항목인 pH와 젖산함량은 실험실용 근적외선분광기의 결과가 SEC = 0.21% ($R^2$=0.82), SEC = 0.24% ($R^2$=0.83)로 소형 근적외선분광기 보다 우수한 결과를 나타내었다. 또한 ADF, NDF 및 조단백질 함량은 실험실용 근적외선분광기의 예측 정확성이 각각 SEC = 0.59% ($R^2$=0.96), SEC = 0.74% ($R^2$=0.97), SEC = 0.67% ($R^2$=0.82)로 높게 나타났다.

• 한국전산구조공학회논문집
• /
• 제24권4호
• /
• pp.383-389
• /
• 2011

본 논문에서는 통계적인 방법을 이용하여 점탄성 제진재인 합성고무의 물성에 대한 변동성을 평가하는 방법을 제안하고 측정데이터를 이용하여 합성고무에 대한 평가를 수행하고 합성고무로 이루어진 고무 마운트에 대한 동특성 해석을 수행하였다. 고무 물성의 불확실성 인자로는 외기 온도의 변화와 실험 데이터의 오차 및 점탄성 물질모델의 오차를 고려하였다. 고무는 분수차 미분모델로 표현되었고, 온도의 영향은 비선형 이동계수모델을 도입하여 복소계수로 나타내어 동강성과 감쇠를 표현하였다. 이러한 물성모델을 바탕으로 고무에 대한 물성 실험데이터와 물성계수의 확률밀도함수 사이에 정의된 우도함수를 최대화하는 통계적 보정방법을 이용하여 물성모델의 물질계수들에 대한 변동성을 추정하였다. 합성고무로 이루어진 제진용 고무 마운트에 대하여 유한요소모델을 이용하여 동특성을 계산하였다. 동특성의 계산시 추정된 물성의 통계값을 적용하고 몬테카를로 해석을 통하여 동강성의 변동성을 살펴서 그 변동성이 매우 큼을 확인하였다.

• Journal of Advanced Marine Engineering and Technology
• /
• 제38권2호
• /
• pp.123-132
• /
• 2014

The maritime sector is advancing with dedicated endeavor to reduce greenhouse gas in addressing issues with regards to global warming. Since 01 January 2013, the International Maritime Organization (IMO) regulation mandatory requirement for Energy Efficiency Design Index (EEDI) has been in place and should be satisfied by newly-built ships of more than 400 gross tonnage and the Ship Energy Efficiency Management Plan (SEEMP) for all ships type. Therefore, compliance to this necessitates planning during the design stage whereas verification can be carried-out through an acceptable method during sea trial. The MEPC-approved 2013 guidance, ISO 15016 and ISO 19019 on EEDI serves the purpose for calculation and verification of attained EEDI value. Individual ships EEDI value should be lower than the required value set by these regulations. The key factors for EEDI verification are power and speed assessment and their synchronization. The shaft power can be measured by telemeter system using strain gage during sea trial. However, calibration of shaft power onboard condition is complicated. Hence, it relies only on proficient technology that operates within the permitted ISO allowance. On the other hand, the ship speed can be measured and calibrated by differential ground positioning system (DGPS). An actual test on a newly-built vessel was carried out to assess the correlation of power and speed. The Energy-efficiency Design Index or Operational Indicator Monitoring System (EDiMS) software developed by the Dynamics Laboratory-Mokpo Maritime University (DL-MMU) and Green Marine Equipment RIS Center (GMERC) of Mokpo Maritime University was utilized for this investigation. In addition, the software can continuously monitor air emission and is a useful tool for inventory and ship energy management plan. This paper introduces the synchronization and identification method between shaft power and ship speed for EEDI verification in accordance with the ISO guidance.

• 한국물환경학회지
• /
• 제30권6호
• /
• pp.673-682
• /
• 2014

A watershed model was constructed using Hydrological Simulation Program Fortran to predict the water temperature at major tributaries of Nakdong River basin, Korea. Water temperature is one of the most fundamental indices used to determine the nature of an aquatic environment. Most processes of an aquatic environment such as saturation level of dissolved oxygen, the decay rate of organic matter, the growth rate of phytoplankton and zooplankton are affected by temperature. The heat flux to major reservoirs and tributaries was analyzed to simulate water temperature accurately using HSPF model. The annual mean heat flux of solar radiation was estimated to $150{\sim}165W/m^2$, longwave radiation to $-48{\sim}-113W/m^2$, evaporative heat loss to $-39{\sim}-115W/m^2$, sensible heat flux to $-13{\sim}-22W/m^2$, precipitation heat flux to $2{\sim}4W/m^2$, bed heat flux to $-24{\sim}22W/m^2$ respectively. The model was calibrated at major reservoir and tributaries for a three-year period (2008 to 2010). The deviation values (Dv) of water temperature ranged from -6.0 to 3.7%, Nash-Sutcliffe efficiency(NSE) of 0.88 to 0.95, root mean square error(RMSE) of $1.7{\sim}2.8^{\circ}C$. The operational water temperature forecasting results presented in this study were in good agreement with measured data and had a similar accuracy with model calibration results.

• Earthquakes and Structures
• /
• 제10권3호
• /
• pp.523-538
• /
• 2016

Besides their spiritual significance, minarets are humanity's cultural heritage to the future generations due to their historical and architectural attraction. Currently, many historical masonry minarets are damaged and destroyed due to several reasons such as earthquakes and wind. Therefore, safety of these religiously significant buildings needs to be thoroughly investigated. The utmost care must be taken into account while investigating these structures. Our study investigated earthquake behavior of historical masonry minaret of Haci Mahmut Mosque. Destructive and non-destructive tests were carried out to determine earthquake safety of this structure. Brick-stone masonry material properties of structure were determined by accomplishing ultrasonic wave velocity, Schmidt Hammer, uniaxial compression (UAC) and indirect tension (Brazilian) tests. Determined material properties were used in the finite element analysis of the structure. To validate the numerical analysis, Operational Modal Analysis was applied to the structure and dynamic characteristics of the structure were determined. To this end, accelerometers were placed on the structure and vibrations due to environmental effects were followed. Finite element model of the minaret was updated using dynamic characteristics of the structure and the realistic numerical model of the structure was obtained. This numerical model was solved by using earthquake records of Turkey with time history analysis (THA) and the realistic earthquake behavior of the structure was introduced.

• 한국콘텐츠학회논문지
• /
• 제19권2호
• /
• pp.349-367
• /
• 2019

부산광역시의 시내버스 준공영제 실시 이후 운영 효율성 요인을 실증적으로 분석하였다. DEA 분석결과, CRS의 경우 지하철 1호선과 환승 가능한 버스노선의 연도별 효율성은 2010년도가 가장 높았다. 지하철 2호선과 환승 가능한 버스노선의 연도별 효율성은 CRS 평균이 연차적으로 점차 향상되어 2016년 0.923로 가장 크게 나타났다. 지하철 3호선과 환승 가능한 버스노선의 연도별 효율성이 2009년부터 2015년까지는 점차 향상되는 모습을 보이다가 2016년도에는 다시 하락하였다. 전체 134개 노선의 4개 연도 536개 노선 중 비효율적으로 나타난 노선은 205개이다. 205개 노선의 효율성을 제고하기 위해서는 규모의 축소 즉, 노선의 운행횟수 등을 감축해야 함을 시사하고 있다. 또한 Tobit 회귀분석을 활용하여 분석결과, 운영 효율성 지수에 유의미한 영향을 미치는 요인으로서는 소요시간이 가장 컸고, 그 다음으로 이용객수, 환승객수의 순으로 나타났다.

• Journal of Radiation Protection and Research
• /
• 제44권2호
• /
• pp.79-88
• /
• 2019

Background: The main goal of experiments is to compare various operational and technical characteristics of D-Shuttle semiconductor personal dosimeters of the Japanese company "Chiyoda Technol Corporation" and Harshaw thermoluminescent dosimeters (TLD) manufactured by "Thermo Fisher Scientific" and DTL-02 of the Russian Research and Production Enterprise (RPE) "Doza" by their occupational and calibration exposure at various dose equivalents from 0.5 to 20 mSv of gamma-radiation. Materials and Methods: Besides dosimeters DTL-02, D-Shuttle and Harshaw TLD, there were also used: (1) the primary reference radionuclide source Hopewell Designs IAEA: G10-1-12 with $^{137}Cs$ isotope (an error is not more than 6% and activity is 20 Ci), and (2) the verification device UPGD-2M of RPE "Doza" and installed in the National Center for Expertise and Certification of the Republic of Kazakhstan (Kapchagai, the National Center for Expertise and Certification). Results and Discussion: The main results of researches are the following: (1) TLDs for Harshaw 6600 and DVG-02TM have an approximately equal measurement accuracy of the individual dose equivalents in the range from 0.5 to 20 mSv of gamma-radiation. (2) Advantages of dosimeters for Harshaw 6600 are due to the high measurement productivity and opportunity to indicate the dose on the skin $H_p$(0.07). Advantages of DVG-02TM consist of operation simplicity and lower cost than of Harshaw 6600. (3) D-Shuttles are convenient for use in the current and the operational monitoring of ionizing radiation. Measurement accuracy and 10% linearity of measurements are ensured when D-Shuttle is irradiated with dose equivalents below 1 mSv at the equivalent dose rate not higher than $3mSv{\cdot}hr^{-1}$. This allows using D-Shuttle at a routine technological activity. Conclusion: The obtained results of experiments demonstrate advantages and disadvantages of D-Shuttle semiconductor dosimeters in comparison with two TLD systems of DVG-02TM and Harshaw 6600.

• Ocean Systems Engineering
• /
• 제7권2호
• /
• pp.107-120
• /
• 2017

Spud-can is used for fixing jack-up rig on seabed. It needs to be inserted up to the required depth during the installation process to secure enough soil reaction and prevent overturning accidents. On the other hand, it should be extracted from seabed soils as fast as possible during the extraction process to minimize the corresponding operational cost. To achieve such goals, spud-can may be equipped with water-jetting system including monitoring and control. To develop such a smart spud-can, a reliable numerical simulation tool is essential and it has also to be validated against physical model tests. In this regard, authors developed a numerical simulation tool by using a commercial program ANSYS with extended Drucker-Prager (EDP) formula. Authors also conducted small-scale (1/100) physical model tests for verification and calibration purpose. By using the numerical model, a systematic parametric study is conducted both for sand and K(kaolin)-clay with varying important soil parameters and the best estimated soil properties of the physical test are deduced. Then, by using the selected soil properties, the numerical and experimental results for a sand/K-clay multi-layer case are cross-checked to show reasonably good agreement. The validated numerical model will be useful in the next-stage study which includes controllable water-jetting.

• 웰빙융합연구
• /
• 제5권3호
• /
• pp.27-41
• /
• 2022

Purpose: In this study, pollutants generated in industrial areas were measured using a Portable Air Quality Measurement System(PAQMS). This study intends to examine in detail improvement measures and operational capabilities to operate a more efficient PAQMS. Research design, data and methodology: This study compares and analyzes the measurement values of the PAQMS and the measurement values of the national air quality measurement network. It is intended to develop a PAQMS corresponding to the data of the national measurement network by minimizing the errors that occur during comparative measurement and analysis and supplementing and improving the problems that occur during the current equipment calibration. Results: A PAQMS is an essential equipment for faster and more accurate measurement and analysis of pollutants in case of untimely measurement and civil complaints due to Micro Climate(local weather and environmental influences). Currently, there are many atmospheric measurement equipment in Korea, but only equipment for each item is produced and sold. Currently, these devices on the market must satisfy various conditions such as stable power, temperature, and humidity to calculate accurate measurement values. Conclusions: Therefore, there is no equipment that satisfies the conditions for performing detailed measurement in the field where accurate measurement is required. In this study, these field work conditions and contents for stable measurement were mentioned in the text.