• Resources Recycling
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• v.25 no.6
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• pp.41-49
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• 2016

The present study was intended to prepare cobalt oxide ($Co_3O_4$) powder of average particle size 50 nm or less by spray pyrolysis reaction using the raw cobalt chloride ($CoCl_2$) solution, in order to identify the change in the nature of the particles according to the change in the nozzle tip size. When the nozzle tip was 1 mm, it turned out that most of the droplets were spherical and the surface showed very tight structure. The average particle size of the finally formed particles was 20-30 nm. When the nozzle tip size was 2 mm, some of the droplets formed were spherical, but a considerable part of them showed severely disrupted form. particles formed showed an average particle size of 30 - 40 nm. For the nozzle tip size of 5 mm, spherical droplets were almost non-existent and most were in badly fragmented state. The tightness of surface structure of the droplets has greatly been reduced compared with other nozzle tip sizes. Average size of the formed particles was about 25 nm. As the nozzle tip size increased from 1 mm to 2 mm and 3 mm, the intensities of the XRD peaks have changed little, but significantly been reduced when the nozzle tip size increased to 5mm. As the nozzle tip size increased from 1 mm to 2 mm, the specific surface area of the particles decreased, but the nozzle tip size increased to 5mm, the specific surface area remarkably increased.

• Resources Recycling
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• v.13 no.6
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• pp.16-25
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• 2004

In this study, nano-sized indium oxide powder with the average particle size below 100 nm is prepared from the indium chloride solution by the spray pyrolysis process. The effects of the concentration of raw material solution, the nozzle tip size and the air pressure on the properties of powder were studied. As the indium concentration of the raw material solution increased from 40 g/l to 350 g/l, the average particle size of the powder gradually increased from 20 nm to 60 nm, yet the particle size distribution appeared more irregular, the intensity of a XRD peak increased and specific surface area decreased. As the nozzle tip size increased from 1 nm to 5 nm, the average particle size of the powder increased from 40 nm to 100 nm, the particle size distribution was much more irregular, the intensity of a XRD peak increased and specific surface area decreased. As the air pressure increased from 0.1 kg/cm$^2$ to 0.5 kg/cm$^2$, the average particle size of the powder varies slightly upto 90~100 nm. As the air pressure increased from 1 kg/cm$^2$ to 3 kg/cm$^2$, the average particle size decreased upto 50~60 nm, the intensity of a XRD peak decreased and the specific surface area increased.

• Resources Recycling
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• v.12 no.6
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• pp.38-46
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• 2003

In this study, nano-sized Ni-ferrite and $Fe_2$$O_3$＋NiO powder was fabricated by spray pyrolysis process in the condition of 1kg/$\textrm{cm}^2$ air pressure using the Fe-Ni complex waste acid solution generated during the manufacturing process of shadow mask. The average particle size of the produced powder was below 100 nm. The effects of the reaction temperature, the concentration of raw material solution and the nozzle tip size on the properties of powder were studied. As the reaction temperature increased from $800 ^{\circ}C$ to $1100^{\circ}C$, the average particle size of the powder increased from 40 nm to 100 nm, the structure of the powder gradually became solid, yet the distribution of the particle size appeared more irregular. Along with the increase of the reaction temperature, the fraction of the Ni-ferrite phase were also on the rise, and the surface area of the powder was greatly reduced. As the concentration of Fe in solution increased from 20g/l to 200g/l, the average particle size of the powder gradually increased from 30 nm to 60 nm, while the distribution of the particle size appeared more irregular. Along with the increase of the concentration of solution, tie fraction of the Ni-ferrite phase was on the rise, and the surface area of the powder was greatly reduced. Along with the increase of the nozzle tip size, the distribution of the particle size appeared more irregular, yet the average particle size of the powder showed no significant change. As the nozzle tip size increased from 1 mm to 2 mm, the fraction of the Ni-ferrite phase showed no significant change, while the surface area of the powder slightly reduced. As the nozzle tip size increased to 3 mm and 5 mm, the fraction of the Ni-ferrite phase gradually reduced, and the surface area of the powder slightly increased.

• Aerospace Engineering and Technology
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• v.6 no.2
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• pp.197-204
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• 2007

Effect of rotor tip geometry on the performance of supersonic impulse turbine was investigated experimentally. Using the shrouded supersonic impulse turbine of the 30ton class liquid rocket engine turbopump as a base model, the measured performance of de-shrouded rotor was compared. The effect of nozzle-rotor overlap also has been investigated. It has been found that the magnitude of turbine efficiency is largely affected by the existence of the rotor shroud. However, measured efficiency sensitivity of the de-shrouded supersonic impulse turbine with respect to turbine tip clearance was relatively smaller than that of high performance reaction turbine. It also has been found that there exists nozzle-rotor overlap value which results optimum efficiency in supersonic impulse turbine.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2011.11a
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• pp.662-665
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• 2011

Pintle technology, which is one of the thrust control method for solid rocket motor, can control the thrust by the control of nozzle throat area through the pintle moving. For studying the unsteady flow characteristics of pintle nozzle by needle type pintle moving, cold flow test and numerical analysis were performed. The pressure distribution on the pintle tip was varied for pintle moving and stopping and thrust was varied by this effects.

• Journal of the Korean Society of Propulsion Engineers
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• v.12 no.2
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• pp.8-14
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• 2008

Solid Rocket Motor(SRM) has advantages such as - high specific impulse, operational safety and simplicity in design and manufacturing process but thrust magnitude can't be controlled. For studying of pintle nozzle that can control the thrust magnitude of SRM, cold flow test and numerical analysis about needle type pintle shape were performed and results were presented in this paper. As the results of this study, pintle tip's shape and nozzle contour were important design parameters because thrust performance and variable thrust range of pintle nozzle depend on them. Especially, the thrust of needle typed pintle nozzle adopted in this test was predicted 13% higher than normal nozzle without pintle.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2007.04a
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• pp.289-294
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• 2007

Solid Rocket Motor(SRM) has advantages such as - high specific impulse, operational safety and simplicity in design and manufacturing process, but thrust magnitude can't be controlled. For studying of pintle nozzle that can control the thrust magnitude of SRM, cold flow test and numerical analysis about needle type pintle shape were performed and results were presented in this paper. As the results of this study, pintle tip's shape and nozzle contour were important design parameters because thrust performance and variable thrust range of pintle nozzle depend on them. Especially, the thrust of needle typed pintle nozzle adopted in this test was predicted 13% higher than normal nozzle without pintle.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.44 no.8
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• pp.641-648
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• 2016

In this study, the effect of injection nozzle shape on the supersonic film cooling performance is analyzed using CFD. The design parameters are inside and outside angles of upper plate of nozzle and nozzle tip thickness. It is observed that the mass flow rate of film cooling decreases with increase of inside angle, while the effect of the change of mass flow rate on the film cooling effectiveness is relatively small. In addition, cooling performance is generally reduced, except ahead of the local region where shock wave interaction with film cooling occurs, in accordance with the growth of the outside angle and tip thickness. In this paper, the CFD simulation is performed using a commercial software, ANSYS Fluent V15.0, and the CFD model is validated by comparing it with the experimental data shown in preceding research.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.37 no.5
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• pp.476-482
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• 2009

The effect of pintle shape on the thrust level of pintle-nozzle Solid Rocket Motor(PNSRM) was studied numerically using the Spalart-Allmaras turbulent model of Fluent. Mass flow rate of PNSRM was always less than theoretical value and the extent of decrease in mass flow rate grew in the large pintle because of increase in the relative boundary layer thickness between pintle body and nozzle wall. The bigger pintle size was, the more thrust of pintle tip pressure was obtained. Meanwhile the more thrust of nozzle and chamber pressure decreased. Hence, total thrust of big pintle was less than a small pintle under same throat area condition. Specific impulse was relatively flat for all pintle shape.

• Proceedings of the KAIS Fall Conference
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• 2003.06a
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• pp.95-97
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• 2003

본 연구에서는 새도우마스크 제조공정에서 발생되는 Fe-Ni 계 폐산 용액에 Ni 성분을 용해시킨 복합 산용액을 원료용액으로 사용하여 분무열분해법에 의해 입도분포 및 조성이 균일하며, 입자형태가 구상이면서 평균입도가 100nm 이하인 Ni-ferrite 나노 분말을 제조하며 원료용액의 유입속도, nozzle tip 크기 및 공기압력의 반응조건 변화에 따른 생성분말의 특성 변화를 파악하였다.