• Title/Summary/Keyword: non-destructive technique

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An Analysis of the Characteristics of Glass Beads from the Joseon Dynasty Using Non-destructive Analysis (비파괴 분석을 활용한 조선시대 유리구슬의 특성 분석)

  • Lee Sujin;Kim Gyuho
    • Conservation Science in Museum
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    • v.30
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    • pp.71-88
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    • 2023
  • This paper examined the visible characteristics and chemical composition of glass beads from the Joseon Dynasty as well as the associations thereof. It also explored the characteristics and uses of glass beads by region. This study covered a total of 1,819 pieces excavated from 25 locations in the Gyeonggi, Chungcheong, and Gyeongsang regions, of which 537 pieces were analyzed for their chemical composition. Glass beads of the Joseon Dynasty take a variety of shapes such as a Round, Coil, Floral, Segmented, Flat, Oval, and Calabash. Colors vary from shades of brown (brown, lemon yellow) and shades of blue (Bluish-Green, greenish-Blue, Purple-Blue) to shades of white (colorless, white) and shades of green (Green, Greenish-Blue, Greenish-Brown). Brown accounts for the largest percentage, followed by Bluish-Green, greenish-Blue. It was identified that Drawing technique was the most common glass bead production technique of the Joseon Dynasty. Potassium oxide (K2O) was the most common flux agent for glass beads, while the potash glass and mixed alkali glass groups account for the largest quantity. The choice of stabilizers depended on the type of flux agents used, but the most common were calcium oxide (CaO) and aluminum oxide (Al2O3). The potash glass and potash lead glass groups are high in CaO and low in Al2O3, the mixed alkali glass group is high in CaO, and the lead glass group is low in CaO. In terms of the association between color and shape, most of the beads with shade of brown and blue have round shapes of brown and blue have spherical shapes, while the coil shape is prominent in blue beads. A high percentage of green and colorless beads also take the shape of a coil, while white beads in general have a floral shape. In terms of the association between shape and chemical composition, round, floral and segmented shapes account for a high percentage of the potash glass group, while coil and flat shapes are common in the mixed alkali glass group. This paper also analyzed the colorants for each color based on the association between color and chemical composition. Iron (Fe) was used as the colorant for brown and white, and titanium (Ti) and iron were used for light yellow. Purple-Blue was produced by by cobalt (Co), and greenish-Blue, Bluish-Green, green, Greenish-Blue were produced by iron and copper (Cu). Colorless beads had a generally low colorant content.

Defect Depth Measurement of Straight Pipe Specimen Using Shearography (전단간섭계를 이용한 직관시험편의 결함 깊이 측정)

  • Chang, Ho-Seob;Kim, Kyung-Suk
    • Journal of the Korean Society for Nondestructive Testing
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    • v.32 no.2
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    • pp.170-176
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    • 2012
  • In the nuclear industry, wall thinning defect of straight pipe occur the enormous loss in life evaluation and safety evaluation. To use non-destructive technique, we measure deformation, vibration, defect evaluation. But, this techniques are a weak that is the measurement of the wide area is difficult and the time is caught long. In the secondary side of nuclear power plants mostly used steel pipe, artificiality wall thinning defect make in the side and different thickness make to the each other, wall thinning defect part of deformation measure by using shearography. In addition, optical measurement through deformation, vibration, defect evaluation evaluate pipe and thickness defects of pressure vessel is to evaluate quantitatively. By shearography interferometry to measure the pipe's internal wall thinning defect and the variation of pressure use the proposed technique, the quantitative defect is to evaluate the thickness of the surplus. The amount of deformation use thickness of surplus prediction of the actual thickness defect and approximately 7 percent error by ensure reliability. According to pressure the amount of deformation and the thickness of the surplus through DB construction, nuclear power plant pipe use wall thinning part soundness evaluation. In this study, pressure vessel of thickness defect measure proposed nuclear pipe of wall thinning defect prediction and integrity assessment technology development. As a basic research defected theory and experiment, pressure vessel of advanced stability and soundness and maintainability is expected to contribute foundation establishment.

DETERMINATION OF SUGARS AND ORGANIC ACIDS IN ORAGE JUICES USING NEAR INFRARED DIFFUSE REFLECTANCE SPECTROSCOPY

  • Tewari, Jagdish;Mehrotra, Ranajana;Gupta, Alka;Varma, S.P.
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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    • 2001.06a
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    • pp.1522-1522
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    • 2001
  • Beverages based on fruit juices are among the most popular commercially available drinks. There is an ever-increasing demand for these juices in the market. Orange juice is one of the most common as well as most favorite flavor. The fruit processing industries have a tremendous responsibility of quality control. For quality evaluation estimation of various components of the juice is necessary. Sucrose, glucose, fructose, citric acid and malic acid are the prime components of orange juice. Little information is available on analysis of orange juice. However, conventional and general wet chemistry procedures are currently being used which are no longer desired by the industry owing to the time involved, labor input and harmful chemicals required for each analysis. Need to replace these techniques with new, highly specific and automated sophisticated techniques viz. HPLC and spectroscopy has been realized since long time. Potential of Near Infrared Spectroscopy in quantitative analysis of different components of food samples has also been well established. A rapid, non-destructive and accurate technique based on Near Infrared Spectroscopy for determination of sugars and organic acids in orange juice will be highly useful. The current study is an investigation into the potential of Near Infrared Diffuse Reflectance Spectroscopy for rapid quantitative analysis of sucrose, glucose, fructose citric acid and malic acid in orange juice. All the Near Infrared measurements were peformed on a dispersive NIR spectrophotometer (ELICO 153) in diffuse reflectance mode. The spectral region from 1100 to 2500nm has been explored. The calibration has been performed on synthetic samples that are mixtures of sucrose, glucose, fructose, citric acid and malic acid in different concentration ranges typically encountered real orange juice. These synthetic samples are therefore considered to be representatives of natural juices. All the Near Infrared spectra of synthetic samples were subjected to mathematical analysis using Partial Least Square (PLS) algorithm. After the validation, calibration was applied to commercially available real samples and freshly squeezed natural juice samples. The actual concentrations were compared with those predicted from calibration curve. A good correlation is obtained between actual and predicted values as indicated by correlation coefficient ($R^2$) value, which is close to unity, showing the feasibility of the technique.

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Ultrasonic Wave Propagation Analysis for Damage Detection in Heterogeneous Concrete Materials (콘크리트 내부결함 탐지를 위한 초음파 전파 해석)

  • Jung, Hwee Kwon;Rhee, Inkyu;Kim, Jae-Min
    • Journal of the Computational Structural Engineering Institute of Korea
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    • v.33 no.4
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    • pp.225-235
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    • 2020
  • Ultrasonic investigation of damage detection has been widely used for non-destructive testing of various concrete structures. This study focuses on damage detection analysis with the aid of wave propagation in two-phase composite concrete with aggregate (inclusion) and mortar (matrix). To fabricate a realistic simulation model containing a variety of irregular aggregate shapes, the mesh generation technique using an image processing technique was proposed. Initially, the domains and boundaries of the aggregates were extracted from the digital image of a typical concrete cut-section. This enables two different domains: aggregates and mortar in heterogeneous concrete sections, and applied the grids onto these domains to discretize the model. Subsequently, finite element meshes are generated in terms of spatial and temporal requirements of the model size. For improved analysis results, all meshes are designed to be quadrilateral type, and an additional process is conducted to improve the mesh quality. With this simulation model, wave propagation analyses were conducted with a central frequency of 75 kHz of the Mexican hat incident wave. Several void damages, such as needle-shaped cracks and void-shaped holes, were artificially introduced in the model. Finally, various formats of internal damage were detected by implementing energy mapping based signal processing.

A Development of Dielectric Measurement System for Detecting Physical Parameters of Ground in Subsurface Dam (지하댐 지반 물성치 측정을 위한 유전율 측정 시스템 개발)

  • Kim Man-il;Jeong Gyo-Cheol;Park Chang-Kun
    • The Journal of Engineering Geology
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    • v.14 no.4 s.41
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    • pp.361-369
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    • 2004
  • The authors designed a new technique to measure dielectric constant of a soil media by Frequency Domain Reflectometry (FDR) system and its measurement sensor probe with different length such as 7m, 10cm and 15cm for estimating the variations of dielectric constant. Measurement of dielectric constant of soil material is possible to measure an interference wave generated by between incidence wave and reflection wave which are detected to electro-magnetic wave through the directional coupler at the high frequency range,0.1 to 1.7GHz, by FDR system. The obtained experimental results verified that the technique is very promising for non-destructive and continuous soil volumetric water content measurement monitoring in a laboratory. The relationship between the soil volumetric water content and the dielectric constant of soil media (standard sand) was expressed by a single regression ewe independent of soil texture at a small experimental error. Also the derived regression curve coincided well with that obtained by Topp curve.

Development of Non-Destructive Sorting Technique for Viability of Watermelon Seed by Using Hyperspectral Image Processing (초분광 영상기술을 이용한 수박종자 발아여부 비파괴 선별기술 개발)

  • Bae, Hyungjin;Seo, Young-Wook;Kim, Dae-Yong;Lohumi, Santosh;Park, Eunsoo;Cho, Byoung-Kwan
    • Journal of the Korean Society for Nondestructive Testing
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    • v.36 no.1
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    • pp.35-44
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    • 2016
  • Seed viability is one of the most important parameters that is directly related with seed germination performance and seedling emergence. In this study, a hyperspectral imaging (HSI) system having a range of 1000-2500 nm was used to classify viable watermelon seeds from nonviable seeds. In order to obtain nonviable watermelon seeds, a total of 96 seeds were artificially aged by immersing the seeds in hot water ($25^{\circ}C$) for 15 days. Further, hyperspectral images for 192 seeds (96 normal and 96 aged) were acquired using the developed HSI system. A germination test was performed for all the 192 seeds in order to confirm their viability. Spectral data from the hyperspectral images of the seeds were extracted by selecting pixels from the region of interest. Each seed spectrum was averaged and preprocessed to develop a classification model of partial least square discriminant analysis (PLS-DA). The developed PLS-DA model showed a classification accuracy of 94.7% for the calibration set, and 84.2% for the validation set. The results demonstrate that the proposed technique can classify viable and nonviable watermelon seeds with a reasonable accuracy, and can be further converted into an online sorting system for rapid and nondestructive classification of watermelon seeds with regard to viability.

A Scientific Analysis of Pigments for A Scroll Painting in Daeungjeon Hall of Bulguk Temple (불국사 대웅전 석가모니후불탱화 안료의 과학적 분석)

  • Kim, So Jin;Han, Min Su;Lee, Han Hyoung
    • Korean Journal of Heritage: History & Science
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    • v.45 no.3
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    • pp.212-223
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    • 2012
  • Pigments used paintings, ornaments, weapons and various objects have been recognised as important elements to ascertain the history, manufacturing technique and cultural migration. Since the understanding of composition of pigments by analysis began in 1963, its technique and methodology has much advanced in recent years; recent study used the portable X-ray Fluorescence as non-destructive analysis has been practiced in particular. However the study on pigments necessitates overall and systematic research because it is difficult to understand periodical and regional use of pigments. by fractional studies. Therefore this research investigates the coloring materials and painting techniques of the scroll painting depicting preaching scene of Sakyamuni Buddha in Daeungjeon Hall, a main hall of Bulguk temple, through scientific analysis and comparison of various pigments which had been applied to the buddhist paintings of Joseon Dynasty. Consequently, it is confirmed that the scroll painting used pigments of white lead[$2PbCO_3{\cdot}Pb(OH)_2$] for ground layer and used mixture of different pigments such as cinnabar (HgS) minium($Pb_3O_4$) malachite($2CuO{\cdot}CO_2{\cdot}H_2O$) hematite($Fe_2O_3$) gold(Ag) for presenting various colors on the painting layer. It has been also believed that mineral pigments were applied to the scroll painting, yet it is difficult to confirm whether it is natural or synthetic pigments because the crystal structures of pigments were not analyzed. The results of this study, however, provide useful reference data for the understanding of the components of pigments and manufacturing techniques of buddhist scroll paintings, in particular, of Joseon Dynasty.

A Study on Damage Assessment Technique of Railway Bridge Substructure through Dynamic Response Analysis (동적 응답 분석을 통한 철도교량 하부구조의 피해평가기법연구)

  • Lee, Myungjae;Lee, Il-Wha;Yoo, Mintaek
    • Journal of the Korean Geotechnical Society
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    • v.37 no.11
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    • pp.61-69
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    • 2021
  • In this study, scale down model bridge piers were fabricated and non-destructive experiments conducted with an impact load to determine scours in the ground adjacent to the bridge piers using the natural frequency of the bridge piers. Three scale-model bridge piers with different heights were fabricated, and they penetrated the ground at a depth of 0.35 m. The scours around the bridge piers were simulated as a side scour and foundation scour. The experiments were conducted in 13 steps, in which scouring around the model bridge piers was performed in 0.05 m excavation units. To derive the natural frequency, the impact load was measured with three accelerometers attached to the model bridge piers. The impact load was applied with an impact hammer, and the top of the model bridge pier was struck perpendicularly to the bridge axis. The natural frequency according to the scour progress was calculated with a fast Fourier transform. The results demonstrated that the natural frequency of each bridge pier tended to decrease with scour progress. The natural frequency also decreased with increasing pier height. With scour progress, a side scour occurred at 70% or higher of the initial natural frequency, and a foundation scour occurred at less than 70%.

An Experimental Study for Characteristics Evaluation of Cement Mortar Using Infrared Thermography Technique (적외선 화상기법을 이용한 시멘트 모르타르 특성의 실험적 평가)

  • Kwon, Seung-Jun;Maria, Q. Feng
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.30 no.1A
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    • pp.53-59
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    • 2010
  • Recently, NDTs (Non-Destructive Techniques) using infrared camera are widely studied for detection of damage and void in RC (reinforced concrete) structures and they are also considered as an effective techniques for maintenance of infrastructures. The temperature on concrete surface depends on material and thermal properties such as specific heat, thermal conductivity, and thermal diffusion coefficient. Different porosity on cement mortar due to different mixture proportions can show different heat behavior in cooling stage. The porosity can affect physical and durability properties like strength and chloride diffusion coefficient as well. In this paper, active thermography which uses flash for heat induction is utilized and thermal characteristics on surface are evaluated. Samples of cement mortar with W/C (water to cement ratio) of 0.55 and 0.65 are prepared and physical properties like porosity, compressive strength, and chloride diffusion coefficient are evaluated. Then infrared thermography technique is carried out in a constant room condition (temperature $20{\sim}22^{\circ}C$ and relative humidity 55-60%). The mortar samples with higher porosity shows higher residual temperature at the cooling stage and also shows reduced critical time which shows constant temperature due to back wall effect. Furthermore, simple equation for critical time of back wall effect is suggested with porosity and experimental constants. These characteristics indicate the applicability of infrared thermography as an NDT for quality assessment of cement based composite like concrete. Physical properties and thermal behavior in cement mortar with different porosity are analyzed in discussed in this paper.

Functional beamforming for high-resolution ultrasound imaging in the air with random sparse array transducer (고해상도 공기중 초음파 영상을 위한 기능성 빔형성법 적용)

  • Choon-Su Park
    • The Journal of the Acoustical Society of Korea
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    • v.43 no.3
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    • pp.361-367
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    • 2024
  • Ultrasound in the air is widely used in industry as a measurement technique to prevent abnormalities in the machinery. Recently, the use of airborne ultrasound imaging techniques, which can find the location of abnormalities using an array transducers, is increasing. A beamforming method that uses the phase difference for each sensor is used to visualize the location of the ultrasonic sound source. We exploit a random sparse ultrasonic array and obtain beamforming power distribution on the source in a certain distance away from the array. Conventional beamforming methods inevitably have limited spatial resolution depending on the number of sensors used and the aperture size. A high-resolution ultrasound imaging technique was implemented by applying functional beamforming as a method to overcome the geometric constraints of the array. The functional beamforming method can be expressed as a generalized beam forming method mathematically, and has the advantage of being able to obtain high-resolution imaging by reducing main-lobe width and side lobes. As a result of observation through computer simulation, it was verified that the resolution of the ultrasonic source in the air was successfully increased by functional beamforming using the ultrasonic sparse array.