• 제목/요약/키워드: nickel powder

검색결과 265건 처리시간 0.027초

Preparation of Cube-textured Nickel-alloy Tape using Metal Powders

  • Lee, Hee-Gyoun;Oh, Hyun-Suk;Hong, Gye-Won
    • Progress in Superconductivity
    • /
    • 제1권2호
    • /
    • pp.120-124
    • /
    • 2000
  • Ni-13%Cr and Ni-70%Cu alloy tapes were prepared by using high purity metal powders as starting materials. The Ni-13%Cr and the Ni-70%Cu mixtures were isostatically pressed, sintered, rolled and texture-annealed. SEM EDS analysis showed that copper and nickel atoms were completely mixed, while the alloying between the chromium powders and the nickel powders was incomplete. In spite of incomplete alloying between nickel and chromium powders, sharp cube-texture was developed for the Ni-13%Cr tape as well as the Ni-70%Cu tape.

  • PDF

다황화암모늄에 의해 제조된 황화니켈을 이용한 리튬전지의 전기 화학적 특성 평가 (Electrochemical Properties of Lithium Batteries with Nickel Sulfide by Ammonium Polysulfide)

  • 유호석
    • 한국수소및신에너지학회논문집
    • /
    • 제32권6호
    • /
    • pp.612-617
    • /
    • 2021
  • In the case of a metal sulfide electrode, it is used as an anode or cathode active material in a lithium battery. The reason is that the voltage exists between 0.8 and 2.0 V via lithium electrode and the discharge and charge capacity is high. In order to manufacture nickel sulfide for electrode, which are widely used, nano-nickel powder was sulfided using ammonium polysulfide, and single-phase NiS electrodes were manufactured through heat treatment. The prepared NiS electrode had a high initial capacity of 500 mAh/g or more, and was stabilized after 20 cycles to maintain a capacity of 400 mAh/g or more until 100 cycles.

습식 환원법에 의한 니켈 미분말의 제조 (Preparation of Ultrafine Nickel Powders by Wet Reduction Process)

  • 이윤복;문영태;신동우;김광호
    • 한국재료학회지
    • /
    • 제12권10호
    • /
    • pp.803-808
    • /
    • 2002
  • Nickel powders were prepared from nickel chloride solution by wet reduction process, and the size control of the particles was investigated with reactant concentration, dispersant agent, and the addition of ethanol as an organic solvent in NiCl$_2$ aqueous solution. The size of the particle decreased with the increase of nickel chloride concentration. Their average particle size were 1.9$\mu\textrm{m}$, 1.6$\mu\textrm{m}$ and $1.5\mu\textrm{m}$ with 0.5M, 0.8M and 1.0M of nickel chloride concentration respectively. The spherical particle was easily controlled by the addition of ethanol as an organic solvent. Especially, in 30 vol% of ethanol, the average particle size and specific surface area were about 0.2$\mu\textrm{m}$ and 8.98m$^2$/g, respectively.

CBD(Chemical Bath Deposition) 법으로 제조된 전기화학식 캐패시터용 NiO 나노박편 필름 (Nickel Oxide Nano-Flake Films Synthesized by Chemical Bath Deposition for Electrochemical Capacitors)

  • 김영하;박수진
    • 한국신재생에너지학회:학술대회논문집
    • /
    • 한국신재생에너지학회 2010년도 춘계학술대회 초록집
    • /
    • pp.163.2-163.2
    • /
    • 2010
  • In this work, nano-flake shaped nickel oxide (NiO) films were synthesized by chemical bath deposition technique for electrochemical capacitors. The deposition was carried out for 1 and 2 h at room temperature using nickel foam as the substrate and the current collector. The structure and morphology of prepared NiO film were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). And, electrochemical properties were characterized by cyclic voltammetry, galvanostatic charge-discharge, and AC impedence measurement. It was found that the NiO film was constructed by many interconnected NiO nano-flakes which arranged vertically to the substrate, forming a net-like structure with large pores. The open macropores may facilitate the electrolyte penetration and ion migration, resulted in the utilization of nickel oxide due to the increased surface area for electrochemical reactions. Furthermore, it was found that the deposition onto nickel foam as substrate and curent collector led to decrease of the ion transfer resistance so that its specific capacitance of a NiO film had high value than NiO nano flake powder.

  • PDF

In-situ 환원/소결법을 이용한 다공성 니켈 멤브레인 가스필터의 제조 및 평가 (Fabrication and Characterization of Porous Nickel Membrane for High Precision Gas Filter by In-situ Reduction/Sintering Process)

  • 김남훈;송한복;최성철;좌용호
    • 한국분말재료학회지
    • /
    • 제16권4호
    • /
    • pp.262-267
    • /
    • 2009
  • Disk type porous nickel membrane was fabricated by in-situ reduction/sintering process using compacted NiO/PMMA (PMMA; Polymethyl methacrylate) mixture at $800^{\circ}C$ in hydrogen atmosphere. The porosity (49$\sim$58%) of these membrane was investigated as an amount of PMMA additive. The thermal decomposition and reduction behavior of NiO/PMMA were analyzed by TG/DTA in hydrogen atmosphere and the activation energy for the hydrogen reduction of NiO and thermal degradation of PMMA was calculated as 61.1 kJ/mol, evaluated by Kissinger method. Finally, the filtering performance and pressure drop were measured by particle counting system.

MgNi계 수소흡장합금의 충방전특성 (Charge-discharge Characteristic of the Mg-Ni Hydrogen Storage Alloy System)

  • 오명학;정원섭;김인곤
    • 한국수소및신에너지학회논문집
    • /
    • 제10권3호
    • /
    • pp.177-184
    • /
    • 1999
  • The charge-discharge characteristics of the $Mg_2Ni-x$ wt.%Nd (x = 0~3) electrodes were investigated. The electrodes were prepared by the mechanical grinding of the induction-melted $Mg_2Ni$ alloy powders with Ni and/or Nd using planetary ball mill apparatus. The discharge capacity of the $Mg_2Ni$ alloy increased with the increase in the nickel content. The electrode possessing 100 wt.% nickel powder showed the initial capacity of 760 mAh/g and the capacity decay with the cycle number was less than that of the 55 wt.% nickel powder. The Nd was added to this composition. It was found that the $Mg_2Ni-100$ wt.%Ni -0.2 wt.%Nd alloy showed an excellent charge-discharge cycle characteristics compared with the other reported Mg-Ni alloy system. The discharge capacity was 400 mAh/g after 70 cycles. Such an improved cycle life seems to be attributed to the improvement in the corrosion characteristics of the alloy. The anodic polarization curve of the $Mg_2Ni-100$ wt.%Ni-0.2 wt.%Nd alloy exhibited better passivating behavior than that of the $Mg_2Ni-100$ wt.%Ni.

  • PDF

이송식 아크 플라즈마를 이용한 MLCC용 니켈 나노분말의 합성 (Preparation of Nickel Nanopowder using the Transferred Arc Plasma for MLCCs)

  • 정다운;오성민;박동화
    • Korean Chemical Engineering Research
    • /
    • 제46권4호
    • /
    • pp.701-706
    • /
    • 2008
  • 이송식 아크 열플라즈마를 이용하여 벌크상태의 니켈을 증발시킨 후 급속한 냉각과정을 거쳐 니켈 나노입자를 합성하였다. 플라즈마에 의해 질소가 용이하게 해리되어 용융된 니켈속으로 용해되고 과포화된 질소원자는 질소 분자로 가스화반응을 하여 반응열을 발산하는데 그 반응열에 의해 다량의 니켈증기가 생성된다. 생성된 니켈증기는 희석가스와 냉각가스를 이용하여 나노 입자 크기의 니켈분말로 제조된다. 희석가스 유량이 증가할수록 입자크기는 감소하였으며 그 분포경향이 작은 크기에서 좁게 나타났다. 평균입자크기는 희석가스 유량이 250 l/min에서 202 nm로 분석되었으며 모든 입자는 250 nm 이하 크기에서 존재함을 확인하였다.

Electrical properties of polyethylene composite films filled with nickel powder and short carbon fiber hybrid filler

  • Mironov, V.S.;Kim, Seong Yun;Park, Min
    • Carbon letters
    • /
    • 제14권2호
    • /
    • pp.105-109
    • /
    • 2013
  • Effects of the amount of nickel powder (Ni) in Ni-carbon fiber (CF) hybrid filler systems on the conductivity(or resistivity) and thermal coefficient of resistance (TCR) of filled high density polyethylene were studied. Increases of the resistivity and TCR with increasing Ni concentration at a given hybrid filler content were observed. Using the fiber contact model, we showed that the main role of Ni in the hybrid filler system is to decrease the interfiber contact resistance when Ni concentration is less than the threshold point. The formation of structural defects leading to reduced reinforcing effect resulted in both a reduction of strength and an increase of the coefficient of thermal expansion in the composite film; these changes are responsible for the increases of both resistivity and TCR with increasing Ni concentration in the hybrid filler system.

분말합금을 이용한 블리스크 제조용 캔 설계 (Can design for Blisk of Nickel-base Superalloy Powder)

  • 임정숙;염종택;권영삼;박노광
    • 한국소성가공학회:학술대회논문집
    • /
    • 한국소성가공학회 2004년도 추계학술대회논문집
    • /
    • pp.171-174
    • /
    • 2004
  • Superalloys with many strengthening alloying elements are frequently used in powder form to alleviate harmful effects of alloy segregation. HIP (hot isostatic pressing) and DB (diffusion bonding) as a form of solid-state bonding process is often used to make turbine components, such as integrated turbine rotors. HIP/DB process requires many technical overcomes related to dimensional changes as well as microstructural control. In this research, HIP/DB process for nickel base superalloys, Udimet 720, were investigated with a view to control the dimensional change during the consolidation process. Simple disc-shaped cans were used to select the conceptual die design for the control of the dimensional change especially in radial direction. The change in the shape of consolidated shape was investigated using commercial FE code with constitutive equations for low temperature plasticity and creep deformation.

  • PDF

Tribological Behavior of Electro-pressure Sintered Cobalt-Iron, Cobalt-Nickel, and Cobalt-Iron-Nickel Compacts

  • Kim, Yong-Suk;Kwon, Yong-Jin;Kim, Tai-Woong
    • 한국분말야금학회:학술대회논문집
    • /
    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
    • /
    • pp.1124-1125
    • /
    • 2006
  • Dry sliding wear behavior of electro-pressure sintered Co-Fe, Co-Ni and Co-Fe-Ni compacts was investigated. Pin-on-disk wear tests were performed on the sintered compacts disk specimens against alumina $(Al_2O_3)$ and silica $(SiO_2)$ ball counterparts at various loads ranging from 3N to 12N. Two sliding speeds of 0.1m/sec and 0.2m/sec and a fixed sliding distance of 1,000m were employed. Worn surfaces and cross sections of them were examined by a scanning electron microscopy, and wear mechanism of the compacts was investigated. Effects of the oxide layer that was formed on wearing surface of the compacts on the wear were also studied.

  • PDF