• Title/Summary/Keyword: nano material

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Development of Nano-sized WC Powder for Hardmetals

  • Yamamoto, Yoshiharu;Mizukami, Masahiko
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.342-343
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    • 2006
  • In order to develop the nano-sized WC powder that improved the hardness of hardmetals, carbothermal reduction of WO3 by C was examined by using the thermogravimetric analysis. At the direct carburization reaction path of $WO_3{\rightarrow}WO_{2.72}{\rightarrow}WO_2{\rightarrow}W{\rightarrow}W_2C{\rightarrow}WC$, the nano-sized grain was generated at the reaction stage $WO_{2.72}$ to $WO_2$ and W. For trial production, the intermediate products which consists of metal and carbide phases obtained by the first heating has been carburized to the final WC powder. We succeeded in the development of the WC powder of about 70nm. In addition, the nano-sized WC powder in which the vanadium of the most effective grain growth inhibitor was uniformly dispersed was developed.

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Synthesis of PMMA Plate with Nano-Sized Pattern on Anodized Aluminum Oxide Template (AAO 나노기공을 형틀로 이용한 PMMA 나노패턴 형성 기술)

  • Lee, B.W.;Lee, K.W.;Lee, C.H.;Lee, T.S.;Hong, C.;Chung, Jae-Hoon;Kim, C.K.;Lee, J.H.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.11a
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    • pp.382-383
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    • 2007
  • PMMA plate with nano-sized pattern was synthesized on anodized aluminum oxide template by bluk polymerization method. Anodized aluminum oxide was used as a template to synthesize the PMMA plate with nano-sized pattern. The polymerization of MMA was performed at $75-79^{\circ}C$. It is verified from SPM results that the nano-sized pattern on synthesized PMMA plate was well transferred from that of anodized aluminum oxide template.

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High Concentrated Silver Nano Ink Formulation for the Inkjet Applications (잉크젯 응용기술을 위한 고농도 은 나노 잉크 배합)

  • Kim, Tae-Hoon;Cho, Hye-Jin;Joung, Jae-Woo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.559-560
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    • 2006
  • Inkjet Printing is very attractive method for direct patterns with no masks, In order to Achieve direct printing with nano metal, It is often necessary to print them with highly concentrated Ink We research the High Concentrated silver nano ink. Formulation which has a good thermal stability and storage stability and jet stability using a ethylene glycol ether. Normally Alcohol-based inks can be sensitive But High boiling point ethylene glycol ether base Ink is creating a stable meniscus and minimum maintenance issues. We are reaching a 50~60wt% high Silver Ink using a Hydrophilic Ag Nano powder. (30~50nm)

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Mechanical Properties of Cement Paste with Nanomateirals (나노재료를 혼입한 시멘트 페이스트의 역학적 특성)

  • Choi, Ik-Je;Kim, Ji-Hyun;Chung, Chul-Woo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2020.06a
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    • pp.193-194
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    • 2020
  • Recently, as the use of high-performance concrete has become common, various problems related to high-performance concrete have become an issue. Among them, self-shrinkage of cement paste due to low water cement ratio is known to cause problems in the volume stability of concrete. To improve this, studies related to the mixing technology of cement-based materials and nano materials have been actively conducted. Looking at the results of prior research related to nano material mixing technology, generally, research results have been reported in which nano materials are incorporated into cement-based materials to improve material properties1). Among them, it was shown that the mechanical performance and various types of functionality of the cement composite are expressed. Among nano materials, carbon nanotubes (hereinafter referred to as CNTs) and graphenes are used in a mixture with cement-based materials. Accordingly, this study intends to compare the mechanical properties by incorporating various CNTs and graphene into cement paste.

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Analysis of Surface Tracking of Micro and Nano Size Alumina Filled Silicone Rubber for High Voltage AC Transmission

  • Loganathan, N.;Chandrasekar, S.
    • Journal of Electrical Engineering and Technology
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    • v.8 no.2
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    • pp.345-353
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    • 2013
  • This paper discusses the experimental results in an effort to understand the tracking and erosion resistance of the micro and nano size $Al_2O_3$ filled silicone rubber (SIR) material which has been studied under the AC voltages, with ammonium chloride as a contaminant, as per IEC 60587 test procedures. The characteristic changes in the tracking resistance of the micro and nano size filled specimens were analyzed through leakage current measurement and the eroded masses were used to evaluate the relative erosion and tracking resistance of the composites. The fundamental, third and fifth harmonic of the leakage current during the tracking study were analyzed using moving average current technique. It was observed that the harmonic components of leakage current show good correlation with the tracking and erosion resistance of the material. The thermogravimetry-derivative thermo gravimetric (TG-DTG) studies were performed to understand the thermal degradation of the composites. The physical and chemical studies were carried out by using scanning electron microscope (SEM), Energy Dispersive X-ray analysis (EDAX) and Fourier Transform Infra-red (FTIR) Spectroscopy. The obtained result indicated that the performance of nano filled SIR was better than the micro filled SIR material when the % wt. of filler increased.

Properties of Nano-Hybrid Coating Films Synthesized from Colloidal Silica-Silane (콜로이달 실리카와 실란으로부터 합성된 나노하이브리드 코팅 박막의 특성)

  • Na, Moon-Kyong;Ahn, Myeong-Sang;Kang, Dong-Pil
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.232-233
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    • 2006
  • In recent years the interest in organic/inorganic hybrid materials has increased at a fast rate. Nano organic-inorganic hybrid composites have shown advantages for preparing hard coating layers. Especially, nano hybrid composite has low environmental pollution. It has high transparency, hardness, toughness, thermal dissociation temperature, hydrophobicity by using nano sized inorganic material. There are many ways in which these materials may be synthesized, a typical one being the use of silica and silanes using the sol-gel process. The structure of sol-gel silica evolves as a result of these successive hydrolysis and condensation reactions and the subsequent drying and curing. The sol-gel reactions are catalyzed by acids and produce silica sol solutions. The silica sol grows until they reach a size where a gel transition occurs and a solid-like gel is formed. Colloidal silica(CS)/silane sol solutions were synthesized in variation with parameters such as different acidity and reaction time. In order to understand their physical and chemical properties, sol-gel coating films were fabricated on glass. From all sol-gel solutions, seasoning effect of sol-gel coating layer on glass was observed.

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Effect of Allyl Modified/Silane Modified Multiwalled Carbon Nano Tubes on the Electrical Properties of Unsaturated Polyester Resin Composites

  • Swain, Sarojini;Sharma, Ram Avatar;Patil, Sandip;Bhattacharya, Subhendu;Gadiyaram, Srinivasa Pavan;Chaudhari, Lokesh
    • Transactions on Electrical and Electronic Materials
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    • v.13 no.6
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    • pp.267-272
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    • 2012
  • Considering the properties of the carbon nano tubes (CNT), their inclusion into the polymer matrix vastly increases the properties of the resultant composite. However, this is not the case due to the poor interfacial adhesion of the CNT and the polymer matrix. The present approach focuses on increasing the interaction between the polymer matrix and the CNT through the chemical modification of the CNT resulting in allyl ester functionalized carbon nanotubes (ACNT) and silane functionalized carbon nano tubes (SCNT) which are capable of reacting with the polymer matrix during the curing reaction. The addition of ACNT/SCNT into unsaturated polyester resin (UPR) resulted in the improvement of the electrical properties of resulted nanocomposites in comparison to the CNT. The surface resistivity, volume resistivity, dielectric strength, dry arc resistivity, and the comparative tracking index of the nanocomposites were significantly improved in comparison to CNT. The chemical modification of CNT was confirmed via spectroscopy.

[ $H_2$ ] uptake of the Li dispersed nickel oxide nanotubes (리튬이 첨가된 니켈 산화물 나노튜브의 수소저장)

  • Lee, Jin-Bae;Lee, Soon-Chang;Lee, Sang-Moon;Lee, Young-Seak;Kim, Hae-Jin
    • Journal of Hydrogen and New Energy
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    • v.17 no.1
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    • pp.39-46
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    • 2006
  • Highly ordered Li dispersed nickel oxide nanotubes were prepared with anodic aluminum oxide (AAO) template for hydrogen storage. Electron microscope results showed that uniform length and diameter of nickel oxide nanotubes were obtained. The wall thickness and outer diameter of nickel oxide nanotubes are about 40 - 50 nm and 200 - 400 nm, respectively. It was observed that the diameter of nickel oxide nanotubes is bigger than the pore diameter of AAO template. Li dispersed nickel oxide were consisted of nanoflakes and had structures of nanotubes and nanorods. For increasing the hydrogen adsorption and desorption capacity, the Li dispersed nickel oxide nanotubes were fluorinated. The fluorinated Li dispersed nickel oxide nanotubes showed 1.65 wt% of the hydrogen adsorption capacities at 77 K under 47 atm.

Preparation of cotton fabri coated with Zinc alginate (Zinc alginate가 피복된 면 직물의 특성)

  • Lee, Ju-Hyun;Kim, Jong-Hwan;Lee, Woo-Seung;Son, Tae-Won
    • Proceedings of the Korean Society of Dyers and Finishers Conference
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    • 2012.03a
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    • pp.66-66
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    • 2012
  • 최근 환경파괴, 병원성 세균감염 등 각종질병과 환경문제로 인한 피부염 등 우리 몸을 보호하기 위하여 친환경 소재의 용품들이 소비자들의 이목을 끌고 있다. 또한, 부가가치를 높이고 특수한 기능성을 나타내는 기능성 섬유에 대한 관심이 증가하고 있으며 이러한 기능성 섬유들 중에서 항균성을 가지는 천연섬유를 주제로 연구를 진행하고 있다. 대표적인 천연섬유인 면 직물에 Zinc alginate로 코팅시켜 부가적인 기능들을 부여시키는 방법으로 실험을 진행하였다. 미처리 면직물과 Zinc alginate가 코팅 된 면직물을 서로 비교하여 분석하였다. 증류수와 생리식염수로 흡습량과 흡습시간을 동시에 측정 후 비교하였으며 접촉각은 Contact angle system OCA20을 이용하여 측정하였다. Zinc alginate의 흡착량은 EDS(EX-250, HORIBA, Japan)를 이용하여 확인하였다. 표면과 단면의 형태는 주사전자현미경(S-4100, Hitachi Co., Japan)으로 x300, x500 배율로 측정하였다.

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Inkjet Printing Using Cu Nano Powder Ink Coated with 1-Octanethiol in Dry Method (건식법으로 1-Octanethiol 코팅한 Cu 나노 분말 잉크의 잉크젯 인쇄 기술 적용)

  • Her, Jae-Hak;Park, Shin-Young;Haque, Mominul Md.;Lee, Caroline Sun-Yong
    • Journal of Powder Materials
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    • v.18 no.4
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    • pp.322-326
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    • 2011
  • Inkjet printing was successfully done using Cu nano powder ink after these Cu nano powders were dry-coated with 1-octanethiol for oxidation prevention. 1-octanethiol, which is Self-Assembled Multi-layers (SAMs), was coated approximately 10-nm thick on the surface of Cu nano powders. 1-Octanol, which has the same chain length as that for 1-octanethiol, was used as a solvent to make the ink for inkjet printing. As a result, the fabricated ink was dispersed for about 4 weeks, and after printing and heat treatment at $350^{\circ}C$ for 4 hours, the resistivity for the printed pattern was measured to be $1.15{\times}10^{-5}{\Omega}{\cdot}cm$.