• Natural Product Sciences
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• v.16 no.3
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• pp.164-168
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• 2010

High-performance liquid chromatographic method with diode-array detector and electrospray ionization with multi-stage tandem mass spectroscopy (HPLC/DAD/ESI-$MS^n$) was used to identify the major constituents in a methanolic extract of Eclipta prostrata. The chromatographic separation was performed on a C18 column. Acetonitrile-water was used as a mobile phase. HPLC/DAD/ESI-$MS^n$ allowed the characterization of constituents of E. prostrata, mainly triterpenoids (eclalbasaponin I, II, III, IV, VI), flavonoids (luteolin 7-O-glucoside, demethylwedelolactone, wedelolactone, luteolin, demetylwedelolactone sulfate, luteolin sulfate, apigenin sulfate) and phenolic acids (5-O-caffeoylquinic acid, 3, 4-O-dicaffeoylquinic acid, 3, 5-O-dicaffeoylquinic acid, 4, 5-Odicaffeoylquinic acid).

• Natural Product Sciences
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• v.21 no.1
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• pp.30-33
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• 2015

Anthocyanins are water soluble plant pigments which are responsible for the blue, red, pink, violet colors in several plant organs such as flowers, fruits, leaves and roots. In recent years, anthocyanin-rich foods have been favored as dietary supplements and health care products due to diverse biological activities of anthocyanins including antioxidant, anti-allergic, anti-diabetic, anti-microbial, anti-cancer and preventing cardiovascular disease. High-performance countercurrent chromatography (HPCCC) coupled with reversed-phase medium pressure liquid chromatography (RP MPLC) method was applied for the rapid and efficient isolation of cyanidin 3-glucoside (C3G) and peonidin 3-glucoside (P3G) from black rice (Oryza sativa L., Poaceae). The crude black rice extract (500 mg) was subjected to HPCCC using two-phase solvent system composed of tert-butyl methyl ether/n-butanol/ acetonitrile/0.01% trifluoroacetic acid (TBME/B/A/0.01% TFA, 1 : 3 : 1 : 5, v/v, flow rate - 4.5 mL/min, reversed phase mode) to give enriched anthocyanin extract (37.4 mg), and enriched anthocyanin extract was sequentially chromatographed on RP-MPLC to yield C3G (16.5 mg) and P3G (8.7 mg). The recovery rate and purity of isolated C3G were 76.0% and 98.2%, respectively, and those of P3G were 58.3% and 96.3%, respectively. The present study indicates that HPCCC coupled with RP-MPLC method is more rapid and efficient than multi-step conventional column chromatography for the separation of anthocyanins.

• Membrane Journal
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• v.23 no.2
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• pp.176-184
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• 2013

To investigate the performance of VOC separation, composite hollow fiber membrane was prepared which composed of poly (ether imide) support prepared by phase separation method and poly (dimethylsiloxane) coating active layer. The performances of the membranes for the application of recovery process in terms of their morphology, gas permeance test for $N_2$ and $O_2$ gases. Durability against benzene, toluene and xylene was also investigated. And permeation test for multi-component VOCS through the membrane with different feed concentration and stage-cut were investigated. Permeance of PEI supported membrane and the membranes coated with PDMS decreased from 45,000 GPU to 63 GPU and 49,450 to 30 GPU for $N_2$ and $O_2$, respectively. Recovery efficiency and concentration of VOCs in permeate increased with decreasing stage-cut. VOCs concentration in permeate proportionally increased with increasing feed concentration but concentration ratio and recovery efficiency showed any noticeable changes with feed concentration change.

• Journal of Ocean Engineering and Technology
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• v.33 no.1
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• pp.42-49
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• 2019

Drilling mud was used once in the step of separating the gas and powder they were transported to a surge tank. At that time, the fine powder, such as dust that is not separated from the gas, is included in the gas that was separated from the mud. The fine particles of the powder are collected to increase the density of the powder and prevent air pollution. To remove particles from air or another gas, a cyclone-type separator generally can be used with the principles of vortex separation without using a filter system. In this study, we conducted numerical simulations of air-particle flow consisting of two components in a cyclone separator in a mud handling system to investigate the characteristics of turbulent vortical flow and to evaluate the collection efficiency using the commercial software, STAR-CCM+. First, the single-phase air flow was simulated and validated through the comparison with experiments (Boysan et al., 1983) and other CFD simulation results (Slack et al., 2000). Then, based on one-way coupling simulation for air and powder particles, the multi-phase flow was simulated, and the collection efficiency for various sizes of particles was compared with the experimental and theoretical results.

• 한국정보디스플레이학회:학술대회논문집
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• 2009.10a
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• pp.502-504
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• 2009

We demonstrate a pixel-isolated bistable twist-splay namatic (PI-BTSN) liquid crystal (LC) cell which has two stable states of splay and ${\pi}$-twist. Each state is stabilized by a multi-dimensional anchoring effect of pixel-isolating polymer walls without any chiral additives. Polymer walls are formed around the pixel region by anisotropic phase separation between LCs and reactive mesogens. Switching between the two states is archived by using vertical and horizontal electric fields. The memory mode of the fabricated LC cell has shown infinity memory time.

• Journal of the Korea Concrete Institute
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• v.17 no.6 s.90
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• pp.939-946
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• 2005

The stiffness properties of heterogeneous concrete materials and their degradation were investigated at different-levels of observations with aids of the opportunities and limitations of multi-resolution wavelet analysis. The successive Haw transformations lead to a recursive separation of the stiffness properties and the response into coarse-and fine-scale features. In the limit, this recursive process results in a homogenization parameter which is an average measure of stiffness and strain energy capacity at the coarse scale. The basic concept of multi-resolution analysis is illustrated with one and two-dimensional model problems of a two-phase particulate composite representative of the morphology of concrete materials. The computational studies include the meso-structural features of concrete in the form of a hi-material system of aggregate particles which are immersed in a hardened cement paste taking due to account of the mismatch of the two elastic constituents.

• The Bulletin of The Korean Astronomical Society
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• v.42 no.1
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• pp.46.2-46.2
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• 2017

Atmospheric propagation effects at millimeter wavelengths can significantly alter the phases of radio signals and reduce the coherence time, putting tight constraints on high frequency Very Long Baseline Interferometry (VLBI) observations. In previous works it has been shown that non-dispersive (e.g. tropospheric) effects can be calibrated with the frequency phase transfer (FPT) technique. The coherence time can thus be significantly extended. Ionospheric effects, which can still be significant, remain however uncalibrated after FPT, as well as the instrumental effects. In this work, we implement a further phase transfer between two FPT residuals (i.e. so-called FPT2) to calibrate the ionospheric effects based on their frequency dependence. We show that after FPT2, the coherence time at 3 mm can be further extended beyond 8 hours, and the residual phase errors can be sufficiently canceled by applying the calibration of another source, which can have a large angular separation from the target (> $20{\circ}$). Calibrations for all-sky distributed sources with a few calibrators are also possible after FPT2. One of the strengths and uniqueness of this calibration strategy is the suitability for high frequency all-sky survey observations including very weak sources. We discuss the introduction of a pulse calibration system in the future to calibrate the remaining instrumental effects and allowing the possibility of imaging the source structure at high frequencies with FPT2, where all phases are fully calibrated without involving any sources other than the target itself.

• Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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• v.5 no.2
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• pp.123-132
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• 2007

This study was performed to evaluate the co- and mutual separation for Am, Cm and RE elements from the simulated multi-component solution equivalent to real HLW level by a Zr-DEHPA(di-(2-ethylhexyl) phosphoric acid containing Zirconium)/$NDD(n-dodecane)-HNO_3$ extraction system. Zr-DEHPA was self-synthesized and the optimal condition of (15g/L Zr-1M DEHPA)/NDD-1M $HNO_3$ was selected taking into consideration of prevention of the third phase, and effects of concentration of DEHPA, nitric acid and impregnant amount of Zr on the co-extraction of Am, Cm and RE. In that condition, the extraction yields were 81% (Am), 85% (Cm), more than 80% (RE elements), 98% (Mo), 85% (Fe), 98% (U), 73% (Np), and less than 5% (other elements) so that the system developed for the co-extraction of Am-Cm/RE was proved to be available. For that, however, U, Np, Mo and Fe was elucidated to have to be removed in advance, and Zr inducing the third phase formation was found to be practically excluded. The co-extracted Am-Cm/RE were sequentially separated in an order of Am-Cm (stripping agent : 0.05 M DTPA-1M Lactic acid of pH 3.6)${\rightarrow}RE$ (stripping agent : 5M $HNO_3$), and then their separation factors were evaluated. At above conditions, Am of 65.4%, Cm of 63.9%, RE (except for Y) of more than 85% were stripped.

• Journal of the Korean Electrochemical Society
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• v.18 no.2
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• pp.75-80
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• 2015

Multi-block sulfonated poly(arylene ether sulfone) (SPAES) copolymer was synthesized via nucleophilic aromatic substitution reaction for proton exchange membrane fuel cell application. After synthesizing the hydrophilic and hydrophobic precursor oligomers having different end-groups (F-terminated or OH-terminated), the effect of end group on the molecular weight was investigated. Hydrophilic oligomers with hydroquinone showed better performance as fuel cell membranes. SPAES membranes showed comparable proton conductivity to that of Nafion at $80^{\circ}C$ and above 70% RH. In particular, SPAES 9 with hydroquinone showed higher proton conductivity than SPAES 10 in the whole RH range studied. Increased local concentration of sulfonic acids within hydrophilic block might develop the hydrophilic-hydrophobic phase separation in the block copolymers.

• The Journal of the Acoustical Society of Korea
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• v.42 no.4
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• pp.357-363
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• 2023

In underwater signal processing, separating individual signals from mixed signals has long been a challenge due to low signal quality. The common method using Short-time Fourier transform for spectrogram analysis has faced criticism for its complex parameter optimization and loss of phase data. We propose a Triple-path Recurrent Neural Network, based on the Dual-path Recurrent Neural Network's success in long time series signal processing, to handle three-dimensional tensors from multi-channel sensor input signals. By dividing input signals into short chunks and creating a 3D tensor, the method accounts for relationships within and between chunks and channels, enabling local and global feature learning. The proposed technique demonstrates improved Root Mean Square Error and Scale Invariant Signal to Noise Ratio compared to the existing method.