• Composites Research
• /
• 제21권2호
• /
• pp.8-14
• /
• 2008

섬유강화 복합재료는 수분에 의해 강도저하가 발생하며 이로 인하여 파괴가 발생하여 인적 물적 피해를 야기하고있다. 본 논문에서는 흡습에 의한 강도저하의 원인을 규명하고자 하였다. 먼저 수분이 복합재료에 흡수되는 메커니즘을 가정하였다. 흡수 메커니즘은 step 1, step 2, 그리고 step 3로 구분하였다. 이 메커니즘을 증명하기 위하여 강화섬유 및 수지의 종류, 수분이 흡수되는 시간 등의 조건을 다르게 하여 시험을 하였으며 그 결과 건조에 의해 인장강도가 회복되는 가역(reversible)반응과 건조로 인해 회복이 불가능한 비가역(irreversible)반응이 모두 작용함을 알 수 있었다. 강도저하는 흡습율 2.5% 에서 거의 완료되며, 흡습율이 4%에 이르면 비가역반응에 의한 강도저하가 많이 작용하여 강도회복이 적어지는 경향을 보였다.

• Journal of Welding and Joining
• /
• 제18권2호
• /
• pp.222-222
• /
• 2000

PBGA(Plastic Ball Grid Array) is composed of some materials such as PCB(Printed Circuit Board), epoxy molding compound, die attach and so on. Reliability of PBGA package is weak compared with plastic packages. The weak points of reliability are the lower resistance to popcorn cracking, which is induced by moisture absorption in PCB, and the pressure cooker test corrosion, which is the basic problem due to the material characteristics of PCB. Introducing the PCB baking and the plasma treatment cleared the popcorn cracking phenomenon. The PCB baking and plasma treatment reduced the epoxy void by eliminating the source of moisture vaporization during the epoxy curing and enhanced the adhesion between PCB and epoxy. Also, plasma treatment enhanced the wettability of epoxy on PCB. The problem of corrosion is cleared using multi-functional epoxy. This type of EMC(Epoxy Molding Compound) is recommended in package using PCB as a substrate. (Received November 19, 1999)

• Journal of Welding and Joining
• /
• 제18권2호
• /
• pp.95-99
• /
• 2000

PBGA(Plastic Ball Grid Array) is composed of some materials such as PCB(Printed Circuit Board), epoxy molding compound, die attach and so on. Reliability of PBGA package is weak compared with plastic packages. The weak points of reliability are the lower resistance to popcorn cracking, which is induced by moisture absorption in PCB, and the pressure cooker test corrosion, which is the basic problem due to the material characteristics of PCB. Introducing the PCB banking and the plasma treatment cleared the popcorn cracking phenomenon. The PCB banking and plasma treatment reduced the epoxy void by eliminating the source of moisture vaporization during the epoxy curing and enhanced the adhesion between PCB and epoxy. Also, plasma treatment enhanced the wettability of epoxy on PCB. The problem of corrosion is cleared using multi-functional epoxy. This type of EMC(Epoxy Molding Compound) is recommended in package using PCB as a substrate.

• 대한화장품학회지
• /
• 제25권1호
• /
• pp.6-22
• /
• 1999

천연고분자인 키틴으로부터 저분자 키토산을 얻은 후 이를 아질산을 이용한 분해반응에 의해 세포증식효과 및 상처치유효과 등의 생리적인 효과가 있는 키토산 올리고당을 합성하였다 이를 위해 아질산을 이용하여 deamination한 후, sodium borohydride로 환원시켜 reducing-end residue들을 alditol unit로 치환하였으며 MBTH시약을 사용하여 반응이 진행하였음을 확인하였다. 얻어진 키토산 올리고 당의 분자량 분포를 HPLC로 확인한 결과 중합도가 2∼6 인 올리고당이 얻어졌음 을 알 수 있었다. 상대습도 43％와 81％에서 측정한 흡습력 실험결과, 글리세린 에 대해 각각 63％, 57％의 흡습력을 보였으며, 상대습도 43％와 실리카겔 분위기 하의 보습력 측정결과, 각각 98％, 91％의 수분잔존률을 나타내었다 키토산 올리고당은 0,000032∼0.01％ 농도 범위에서 세포증식효과를 보였으며, 2％와 20％로 처리한 경우 상처치유효과를 나타내었다.

• 한국전기전자재료학회:학술대회논문집
• /
• 한국전기전자재료학회 2000년도 하계학술대회 논문집
• /
• pp.596-598
• /
• 2000

This paper presents a new accelerating aging test facility for distribution lightning arresters. Aging parameters of lightning arrester are moisture ingress, electrical stress and surge absorption and so on. In this system, we applied 13.2kV to 6 samples and controled temperature and humidity of chamber and measured leakage currents of the all samples. Also we developed accelerating aging cycle which consists of -35$^{\circ}C$∼90$^{\circ}C$ temperature and 40%∼90% humidity. Through the aging test we found out the leakage current of aged sample increases rapidly according to the temperature rising. Hereafter we can determine the replacement guide of leakage current for field operating arresters and condition assessment of aged samples through this aging test.

• 한국농공학회지
• /
• 제21권2호
• /
• pp.81-103
• /
• 1979

The weathered granite soil involves problems in its stability in soil structures depending upon the reduction of soil strength due to the water absorption, crushability, and content of colored mineral and feldspar. As an attemt to solve the problems associated with soil stability, the crushability of weathered granite soil was investigated by conducting tests such as compaction test, CBR test, unconfined compression test, direct shear test, triaxial compression test, and permeability test on the five soil samples different in weathering and mineral compositions. The experimental results are summarized as follows: The ratio of increasing dry density in the weathered granite soil was high as the compaction energy was low, while it was low as the compaction energy was increased. The unconfined compressive strength. and CBR value were highest in the dry side rather than in the soil with the optimum moisture content, when the soil was compacted by adjusting water content. However, the unconfined compressive strength of smples, which were compacted and oven dried, were highest in the wet side rather than in soil with the optimum moisture content. As the soil becomes coarse grain, the ratio of specific surface area increased due to increased crushability, and the increasing ratio of the specific surface area decreased as the compaction energy was increased. The highest ratio of grain crushability was attained in the wet side rather than in the soil with the optimum moisture content. Such tendency was transforming to the dry side as the compaction energy was increased. The effect of water on the grain crushability of soil was high in the coarse grained soil. The specific surface area of WK soil sample, when compacted under the condition of air dried and under the optimum moisture content, was constant regardless of the compaction energy. When the weathered granite soil and river sand with the same grain size were compacted with low compaction energy, the weathered granite soil with crushability had higher dry density than river sand. However, when the compaction energy reached to certain point over limitation, the river sand had higher dry density than the weathered granite soil. The coefficient of permeability was lowest in the wet side rather than in the optimum moisture content, when the soil was compacted by adjusting soil water content. The reduction of permeability of soil due to the compaction was more apparent in the weathered granite soil than in the river sand. The highly significant correlation coefficient was obtained between the amount of particle breakage and dry density of the compacted soil.

• 한국식품저장유통학회지
• /
• 제19권5호
• /
• pp.688-695
• /
• 2012

대두분말을 떡볶이 떡에 첨가하여 수분, 색도, 조리특성, 기계적 조직감 및 관능적 품질특성을 살펴보았다. 대두분말 첨가 떡볶이 떡의 수분함량은 모든 저장기간에서 대두분말 함량이 증가할수록 높은 경향을 나타내었다. 대두분말 15% 첨가군인 SF15는 저장 0, 1, 2일째에 각각 46.30, 46.30, 45.00%로 전 처리군 중에서 가장 높은 수분함량을 보였다. 대두분말을 첨가한 처리군이 첨가하지 않은 처리군보다 L값은 낮았고 첨가한 처리군들간에는 대두분말이 증가할수록 L값은 감소하였고 a, b 값은 증가하는 경향을 보였다. 저장 1일째까지는 색을 유지하였다가 저장 2일째에는 유의적으로 변화하였다. 조리특성 결과, 대두분말함량이 증가할수록 수분 흡수율은 감소하였고 고형물 용출량은 증가하였다. 기계적 조직감 특성결과, 떡볶이 떡의 경도, 씹힘성, 응집성은 대두분말을 첨가한 처리군이 대조군에 비해 낮은 값을 보였으나 대두분말 첨가량에 따른 유의적인 차이는 보이지 않았다. 탄력성은 전처리구간에서 유의적인 차이가 없었으며 부착성은 증가하는 경향을 보였다. 대두분말 첨가 떡볶이 떡의 관능적 특성 결과 맛, 향, 색, 경도, 탄력성 및 전반적인 기호도에서 저장기간 0, 1, 2 일째 모두에서 대두분말 5% 첨가한 떡볶이 떡의 품질이 가장 우수한 점수를 보였다. 이상의 연구결과들을 토대로 떡볶이 떡에 식이섬유와 단백질 급원인 대두분말을 첨가하였을 시 떡의 수분을 유지시켜 조직감 및 관능적 특성에 긍정적인 영향을 주었으며 5% 첨가군이 맛과 향, 조직감 및 전반적인 기호도가 가장 우수하여 제조 시 적합할 것으로 판단되며 향후 기능성과 품질이 우수한 떡볶이 떡을 제조할 수 있을 것으로 기대되었다.

• 한국지반공학회지:지반
• /
• 제2권1호
• /
• pp.7-14
• /
• 1986

The structure of the collapsible soils, such as decomposed granite soil and loess, were examined by the odeometer test, SEM & XES analysis and static & cyclic triaxial test, and hove this structure have influences upon the collapsible behaviour under static and cyclic load was investigated. The study results obtained are as follows; 1. The macropores space of decomposed granite soil (rd=1.50g/cm3) and loess (rd=1.43g/cm3) used in this test were well developed, and showed the behaviour of collapsible soil. 2. Collapsible soil has high resistance on the strain under natural moisture content, however, the resistance on the strain was sharply decreased by the absorption and increasing load since its special structure was destructed. 3. Under the static load, the strain of collapsible soil was high by the viscous flow of the cyclic bonds with time lapse, but Infer the cyclic load, the strain of collapsible soil was low since the tinge needed to destruct the bonding force of clay was not enough. 4. The understanding about the cyclic behaviour of collapsible soil may be helpful to predict the elastic & residual strain of the foundations by the earthquake together with the damage by the additional failure.

• 한국농공학회지
• /
• 제20권1호
• /
• pp.4575-4591
• /
• 1978

In order to investigate the effects of grain size distribution, cement content, and molding pressure on the strength and durability of soil-cement mixtures, a laboratory test of soil cement mixtures was performed at four levels of cement content, five levels of molding pressure, and four levels of normal curing periods. The results are summarized as follows: 1. Optimum moisture contents in loam soil and maximum dry density in sand soil increased with the increase of cement content, but in others, both optimum moisture contents and maximum dry density were changed ununiformly. 2. When the specimens were molded with molding pressure, 50kg/$\textrm{cm}^2$, strength of soil cement mixture with cement content, 2 and 4 per cent, was lower than the strength of soil cement mixture without cement content by more than 40 to 50 per cent. 3. The strength of soil-cement molded with molding pressure, 100kg/$\textrm{cm}^2$, was higher than the strength of soil-cement molded with M.D.D. obtained from standard compaction test more than 40 per cent in sand loam cement and 50 per cent in loamy cement. 4. There was highly significant positive correlation among molding pressure, cement content and unconfined compressive strentgh and so the following multiple regression equations were obtained. Loam: fc=1.9693C+0.197P-0.84 Sandy loam: fc=2.9065C+0.235P-0.77 5. When the specimens were molded with molding pressure, 20 to 100kg/$\textrm{cm}^2$, the regression equation between the 28-day and 7-day strenght was obtained as follows. Loam : q28=1.1050q7+7.59(r=0.9147) Sandy loam : q28=1.3905q7+3.17 (r=0.9801) 6. At the cement contents of above 50 per cent, the weight losses by freeeze-thaw test were negligible. At the cement content of below 8 per cent the weight losses were singnificantly high under low molding pressure and remarkably decreased with the increase of molding pressure up to 80kg/$\textrm{cm}^2$. 7. Resistance to damage from water and to absorption of water were not improved by molding pressure alone, but when the soil was mixtured with cement above 6 per cent, damage seldoms occurred and absorbed less than 5 per cent of water. 8. There was highly significant inverse-corelationship between the compressive strength of soil cement mixtures and their freeze-thaw loss as well as water absorption. By the regression equation methods, the relationships between them were expessed as followed fc=-7.3206Wa+115.6(r=0.9871) log fc=-0.0174L+1.59(r=0.7709) where fc=unconfined compressive stregth after 28-days curing. kg/$\textrm{cm}^2$ Wa=water absorption, % L : freeze-thaw loss rate, %

• 대한기계학회논문집A
• /
• 제40권2호
• /
• pp.139-145
• /
• 2016

본 연구에서는 나노클레이 함량에 따른 나노클레이-에폭시 나노복합재료의 흡습 특성 및 기계적 특성을 실험을 통해 분석하였다. 나노복합재료의 흡습 시험, 인장시험 및 접착조인트를 나노클레이 함량에 따라 구성하였으며 이를 통해 수분 포화도, 수분 확산 계수, 인장 강도 및 접착 강도와 같은 특성을 파악 할 수 있었다. 또한 나노클레이 및 에폭시 재료를 분자단위로 모델링하여 재료의 흡습 특성변화의 매커니즘을 분석할 수 있는 분자동역학 시뮬레이션을 수행하였으며 그 결과를 실험결과와 비교하여 고찰하였다. 본 연구에서 제안된 분자동역학 시뮬레이션 기법은 흡습특성의 변화를 성공적으로 예측할 수 있었으며, 추후 다른 나노-복합재료의 연구에도 널리 활용될 것이라 기대된다.