• Title/Summary/Keyword: mixture experimental design

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Measurement and Calculation of Excess Enthalpies for n-Hexane/Alkane series and NaOH/Water/Ethanol System using Isothermal Microcalorimeter (등온 미세열량계를 이용한 n-Hexane-알칸계 이성분 혼합물 및 NaOH/Water/Ethanol계의 과잉 엔탈피 측정 및 계산)

  • Choi, In Kyu;You, Seong-sik
    • Korean Chemical Engineering Research
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    • v.55 no.5
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    • pp.660-667
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    • 2017
  • Equilibrium data of the mixture is essential in the design and operation of separation equipment such as distillation or extraction in chemical processes. These equilibrium data can be obtained through experiments or by calculations using the known binary parameters and the thermodynamic models. Generally, to obtain these parameters, phase equilibrium experimental data such as gas-liquid and liquid-liquid are used. In this study, the excess enthalpy of the mixture was measured using the flow type microcalorimeter which is a simpler method than phase equilibria experiments, and the parameters of various theories were obtained by using this data. In order to investigate the relationship between carbon chain length, enthalpy and binary parameters in the alkane system, excess enthalpies for the n-hexane + alkane (n-pentane, n-heptane, n-octane and n-dodecane) were measured at 298.15 K and the banary interaction parameters of Wilson, NRTL, and UNIQUAC were obtained from the experimental data. In addition, we wanted to obtain basic information on the interaction and association phenomena of the system including electrolyte applicable to various fields by using the excess enthalpy experimental data and the existing theory. First, we investigated the excess enthalpy for the NaOH / Water / Ethanol system as a basic experiment and examined the applicability using the electrolyte-NRTL (eNRTL) theory.

Basic Study on Quality Evaluation Technique for Peeled Garlics(I) -Rotation sytem for vision-based garlic sorter- (박피 마늘의 품위판정 기술개발에 관한 기초연구(I) -영상식 마늘 선별기용 반전장치 개발-)

  • 이종환;이성범;안청운
    • Journal of Biosystems Engineering
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    • v.26 no.3
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    • pp.271-278
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    • 2001
  • Many workers in the garlic peeling factory are separating the sound peeled garlics from the unpeeled and defective ones in a manual way. In order to reduce the seasonal labor requirement and operating cost, the mechanized garlic sorting system such as the vision-based garlic sorter should be developed. This study was conducted as one of basic studies on developing quality evaluation technique for peeled garlics, especially to developed the system for acquiring the whole surface images of garlics with a CCD camera. The following results were obtained from this study. 1. The belt-type garlic rotation system was devised to apply for the vision-based garlic sorter and was tested to decide the criteria of design and optimum conveying speed. 2. To evaluate the performance of the developed garlic rotation system, feeding rate and rotating rate were measured under the conditions of four experimental factors such as the inclined angle of rotating belt, the inclined angle of feeding belt, the height of plate arrays on feeding belt and the conveying speed of belts. And the capacity of the system according to mixture ratios of peeled garlics and unpeeled garlics was analyzed as a feasibility test. 3. For the inclined angle of rotating belt 20°and height of plate array on feeding belt 22㎜, the maximum rotating rate for garlic samples including unpeeled ones was 81.1% at the conveying speed of 4.2 garlic/sec. And under these condition, the maximum feeding rate was 85% at the inclined angle of feeding belt 6.5°. 4. The capacity of the developed garlic rotation system was almost constant regardless of mixture ratio of peeled garlics and unpeeled garlics and its range was 2.95∼3.92 garlic/sec. At the conveying speed of 4.2 garlic/sec, the capacity of the garlic rotation system was calculated ad 58∼64 kg/hr. 5. To improve performance of the garlic rotation system, it is recommended to develop a device to slide garlics into feeding belt.

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Concrete Optimum Mixture Proportioning Based on a Database Using Convex Hulls (최소 볼록 집합을 이용한 데이터베이스 기반 콘크리트 최적 배합)

  • Lee, Bang-Yeon;Kim, Jae-Hong;Kim, Jin-Keun
    • Journal of the Korea Concrete Institute
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    • v.20 no.5
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    • pp.627-634
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    • 2008
  • This paper presents an optimum mixture design method for proportioning a concrete. In the proposed method, the search space is constrained as the domain defined by the minimal convex region of a database, instead of the available range of each component and the ratio composed of several components. The model for defining the search space which is expressed by the effective region is proposed. The effective region model evaluates whether a mix-proportion is effective on processing for optimization, yielding highly reliable results. Three concepts are adopted to realize the proposed methodology: A genetic algorithm for the optimization; an artificial neural network for predicting material properties; and a convex hull for evaluating the effective region. And then, it was applied to an optimization problem wherein the minimum cost should be obtained under a given strength requirement. Experimental test results show that the mix-proportion obtained from the proposed methodology using convex hulls is found to be more accurate and feasible than that obtained from a general optimum technique that does not consider this aspect.

Study on Combustion Gas Properties of a Fuel-Rich Gas Generator (연료 과농 가스발생기의 연소 가스 물성치에 관한 연구)

  • 서성현;최환석;한영민;김성구
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.34 no.10
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    • pp.56-60
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    • 2006
  • It is essential to predict thermodynamic properties of combustion gas with respect to a propellant mixture ratio for the development of a gas generator for a liquid rocket engine. The present study shows the temperature measurement of exit combustion gas as a function of a mixture ratio through the series of combustion tests of a fuel-rich gas generator with liquid oxygen and Jet A-1. The measurements of dynamic and static pressures, and combustion gas temperatures allowed the estimation of thermodynamic properties like a specific heat ratio, a gas constant, and a constant pressure specific heat of the combustion gas. The comparison of the experimental results with predictions made by interpolation parameters obtained from the modification of the chemical equilibrium code indicates that the interpolation method calibrated using the temperature measurements can be utilized as an effective tool for the initial design of a fuel-rich gas generator.

Effects of momentum ratio and mixture ratio on combustion efficiency in liquid rocket engine (액체로켓에서의 운동량비와 혼합비가 연소성능에 미치는 영향)

  • Han, J.S.;Kim, S.J.;Kim, S.G.;Kim, Y.
    • Journal of the Korean Society of Propulsion Engineers
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    • v.3 no.4
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    • pp.38-43
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    • 1999
  • An experimental study was carried out, in order to set up the procedure for evaluation of hot fire test, to investigate the effect of mixture on combustion performance and combustion stability , and to determine the optimum design condition for designing the liquid rocket engine. $HNO_3$/Kerosene uni-element liquid rocket engine(thrust 24 $\iota{b}_f$, chamber pressure 200 psia) using impinging streams doublet injector was designed, and ground hot-fire test was carried out. To prevent or reduce the hard start during ignition period, two step ignition method was used. This was accomplished by maintaining about 25% of the designed operating pressure doting transient period, then chamber pressure was built up to the designed operating pressure. Maximum combustion efficiency was at O/F ratio 3.6, and combustion efficiency is decreased with increasing momentum ratio.

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Measurement of Radiative Heat Flux of Nozzle Exit (노즐 후방부의 Radiative Heat Flux 측정)

  • An, Won Geun;Park, Hui Ho;Hwang, Su Gwon;Kim, Yu
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.31 no.5
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    • pp.87-92
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    • 2003
  • In rocket systems, somtimes special devices or equipments are installed near the nozzle exit area where high temperature and pressure combustion gas flows. To pretect these subsystems from severe thermal environment, it is necessary to have accurate thermal data measured from the experimental liquid rocket firing test. Test variables were combustion pressure (200, 300, 400 psi) and mixture ratio (1.5, 2.0, 2.5) and quartz was used as a heat probe. Measurement technique used in this research can be also applied to measure the radiative heat flux inside the combustion chamber which is important imput data for the liquid rocket regenerative cooling system design.

Experimental Study on Fire Resistant Capacity and Thermal Conduction of Construction Material Using the Circulation Resources (폐콘크리트 순환자원을 이용한 건설재료의 화재내력 및 단열성에 관한 실험적 연구)

  • Choi, Jea-Nam;Hong, Se-Hwa;Son, Ki-Sang
    • Journal of the Korea Safety Management & Science
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    • v.12 no.3
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    • pp.121-128
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    • 2010
  • This is to show some basic data for introducing both circulated aggregate and recycled powder producing waste concrete. Standard-mixing design for 24MPa has been basically used and added and replaced normal aggregate with recycled powder made of waste concrete. In addition, polycarboxylate high-range water reducing agent has been used because recycled powder is missing adhesive strength and it is not compare with cement's adhesive strength. Compressive strength with powder mixture of 2%, 4%, 6%, 8%, and 10% has been decreased down to 80% of normal concrete material strength without recycled powder mixture. $200^{\circ}C$, $400^{\circ}C$ and $600^{\circ}C$ heated concrete were compressively tested in order to find out concrete strength resistant to high temperature. heat capacity was also tested, based on the expectancy of its low conductivity. In addition, thermal conduction test was tested in order to find out concrete insulation. According to this test, when concrete was tested by fire resistance, it using the circulation aggregate was same resulted by concrete using the natural aggregate. also, recycle powder was not effecting insulation performance. but it is fit to standard on concrete insulation of building law.

Effect of Sowing Season on the Growth and Dry Matter Yield Legumes in Different Legume-Grass Mixtures according to Altitude (표고별 파종시기가 서로다른 두과 - 화본과 혼파초지에서 두과목초의 생육 및 건물수량에 미치는 영향)

  • 정의수;김현섭
    • Journal of The Korean Society of Grassland and Forage Science
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    • v.12 no.3
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    • pp.153-160
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    • 1992
  • This experiment was conducted to investigate the adaptability of legume in different legume-grass mixtures according to altitude(600, 800, lOOOm a.s.1.) in the alpine area. The experimental plot was allocated as a split plot design with three replications. The main plots were sowing season(spring and fall) and subplots legume-grass mixture(alfa1fa-grass, red clover-grass and white clover-grass mixture). The results obtained are summarized as follows: 1. At 600m, in case of sowing alfalfa, red clover and white clover in fall. each legume of legume-grass mixtures was consistuted about 30% without between-year variation and then all legumes at fall sowing could grow. 2. At 800m, in case of sowing white clover in spring this species was consistuted about 14.7 % at the last cutting without severe between-year variation. 3. At 1000m, only white clover sown in spring like at 800m was somewhat maintained without severe between-year variation. 4. Percentage and DM yield of legume considerably decreased with the rise of altitude and alfalfa couldn't grow more than 800m.

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Target Speech Detection Using Gaussian Mixture Model of Frequency Bandwise Power Ratio for GSC-Based Beamforming (GSC 기반 빔포밍을 위한 주파수 밴드별 전력비 분포의 혼합 가우시안 모델을 이용한 목표 음성신호의 검출)

  • Chang, Hyungwook;Kim, Youngil;Jeong, Sangbae
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.19 no.1
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    • pp.61-68
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    • 2015
  • Noise reduction is necessary to compensate for the degradation of recognition performance by various types of noises. Among many noise reduction techniques using microphone array, generalized sidelobe canceller (GSC) has been widely applied to reduce nonstationary noises. The performance of GSC is directly affected by its adaptation mode controller (AMC). That is, accurate target speech detection is essential to guarantee the sufficient noise reduction in pure noise intervals and the less distortion in target speech intervals. Thus, this paper proposes an improved AMC design technique in which the power ratio of the output of fixed beamforming to that of blocking matrix is calculated frequency bandwise and probabilistically modeled by mixture Gaussians for each class. Experimental results show that the proposed algorithm outperforms conventional AMCs in receiver operating curves (ROC) and output SNRs.

Study of hydrodynamics and iodine removal by self-priming venturi scrubber

  • Jawaria Ahad;Talha Rizwan ;Amjad Farooq ;Khalid Waheed ;Masroor Ahmad ;Kamran Rasheed Qureshi ;Waseem Siddique ;Naseem Irfan
    • Nuclear Engineering and Technology
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    • v.55 no.1
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    • pp.169-179
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    • 2023
  • Filtered containment system is a passive safety system that controls the over-pressurization of containment in case of a design-based accidents by venting high pressure gaseous mixture, consisting of air, steam and radioactive particulate and gases like iodine, via a scrubbing system. An indigenous lab scale facility was developed for research on iodine removal by venturi scrubber by simulating the accidental scenario. A mixture of 0.2 % sodium thiosulphate and 0.5 % sodium hydroxide, was used in scrubbing column. A modified mathematical model was presented for iodine removal in venturi scrubber. Improvement in model was made by addition of important parameters like jet penetration length, bubble rise velocity and gas holdup which were not considered previously. Experiments were performed by varying hydrodynamic parameters like liquid level height and gas flow rates to see their effect on removal efficiency of iodine. Gas holdup was also measured for various liquid level heights and gas flowrates. Removal efficiency increased with increase in liquid level height and gas flowrate up to an optimum point beyond that efficiency was decreased. Experimental results of removal efficiency were compared with the predicted results, and they were found to be in good agreement. Maximum removal efficiency of 99.8% was obtained.