• 제목/요약/키워드: mixed grain

검색결과 453건 처리시간 0.029초

Na0.5Bi0.5TiO3-BaTiO3 계에서 입자성장 및 고상단결정성장에 미치는 Na2CO3 첨가 효과 (Effect of Na2CO3 Addition on Grain Growth Behavior and Solid-state Single Crystal Growth in the Na0.5Bi0.5TiO3-BaTiO3 System)

  • 문경석
    • 한국분말재료학회지
    • /
    • 제25권2호
    • /
    • pp.104-108
    • /
    • 2018
  • Grain-growth behavior in the $95Na_{1/2}Bi_{1/2}TiO_3-5BaTiO_3$ (mole fraction, NBT-5BT) system has been investigated with the addition of $Na_2CO_3$. When $Na_2CO_3$ is added to NBT-5BT, the growth rate is higher than desired and grains are already impinging each other during the initial stage of sintering. The grain size decreases as the sintering temperature increases. With the addition of $Na_2CO_3$, a liquid phase infiltrates the interfaces between grains during sintering. The interface structure can be changed to be more faceted and the interface migration rate can increase due to fast material transport through the liquid phase. As the sintering temperature increases, the impingement of abnormal grains increases because the number of abnormal grains increases. Therefore, the average grain size of abnormal grains can be decreased as the temperature increases. The phenomenon can provide evidence that grain coarsening in NBT-5BT with addition of $Na_2CO_3$ is governed by the growth of facet planes, which would occur via mixed control.

황(黃)라왕재(Shorea spp.)의 모드 I, 모드 II 및 혼합(混合)모드 하중시(荷重時) 파괴기준(破壞基準)에 관(關)한 연구(硏究) (Studies on Fracture Criterion in Yellow Lauan(Shorea spp.) under Mode I, Mode II and Mixed Mode Loading)

  • 심국보;이전제;정희석
    • Journal of the Korean Wood Science and Technology
    • /
    • 제20권2호
    • /
    • pp.61-72
    • /
    • 1992
  • This study was carried out to investigate the fracture behavior and the fracture criterion of yellow lauan(Shorea spp.), when has used for furniture and wood structures, and to offer a reliability for wood structure and basic data for wood fracture criterion in experiments which are fracture tested under mode I, mode II and mixed mode loading condition. The results were summarized as follows; 1. Fractures in specimens which have inclined grain in yellow lauan procedeed from crack tip in the radial direction along the grain. 2. In yellow lauan, $K_{IC}RL$ was 42.1kg/$cm^{3/2}$ and $K_{IIC}RL$ was 15.8kg/$cm^{3/2}$. 3. The fracture criteria of lauan were; ($K_I/K_{IC}$)+($K_{II}/K_{IIC}$)=1 in RL system with inclined grain at $45^{\circ}$, ($K_I/K_{IC}$)+$(K_{II}/K_{IIC})^2$=1 with inclined grain at $15^{\circ}$ and $(K_I/K_{IC})^2$+$(K_{II}/K_{IIC})^2$=1 with inclined grain at $30^{\circ}$, $60^{\circ}$, $75^{\circ}$ and $90^{\circ}$, respectively. 4. The fracture criterion of wood could vary with the species, and the load applying condition. In order to measure the fracture criterion strictly, along with standardization of specimen geometry a large amount of experimental data is needed. 5. $K_{IC}$(critical stress intensity factor) can be predicted by grain angle. As the grain inclined angle increased, $K_{IC}$ and $K_{IIC}$ are increased.

  • PDF

베이나이트강의 미세조직과 저온 충격 인성에 미치는 바나듐과 보론의 영향 (Effect of Vanadium and Boron on Microstructure and Low Temperature Impact Toughness of Bainitic Steels)

  • 황원구;이훈;조성규;서준석;권용재;이정구;신상용
    • 한국재료학회지
    • /
    • 제31권3호
    • /
    • pp.139-149
    • /
    • 2021
  • In this study, three kinds of bainitic steels are fabricated by controlling the contents of vanadium and boron. High vanadium steel has a lot of carbides and nitrides, and so, during the cooling process, acicular ferrite is well formed. Carbides and nitrides develop fine grains by inhibiting grain growth. As a result, the low temperature Charpy absorbed energy of high vanadium steel is higher than that of low vanadium steel. In boron added steel, boron segregates at the prior austenite grain boundary, so that acicular ferrite formation occurs well during the cooling process. However, the granular bainite packet size of the boron added steel is larger than that of high vanadium steel because boron cannot effectively suppress grain growth. Therefore, the low temperature Charpy absorbed energy of the boron added steel is lower than that of the low vanadium steel. HAZ (heat affected zone) microstructure formation affects not only vanadium and boron but also the prior austenite grain size. In the HAZ specimen having large prior austenite grain size, acicular ferrite is formed inside the austenite, and granular bainite, bainitic ferrite, and martensite are also formed in a complex, resulting in a mixed acicular ferrite region with a high volume fraction. On the other hand, in the HAZ specimen having small prior austenite grain size, the volume fraction of the mixed acicular ferrite region is low because granular bainite and bainitic ferrite are coarse due to the large number of prior austenite grain boundaries.

단어재인에 있어서 처리단위의 적응적 변화 (Adaptive Changes in the Grain-size of Word Recognition)

  • Lee, Chang H.
    • 한국인지과학회:학술대회논문집
    • /
    • 한국인지과학회 2002년도 춘계학술대회
    • /
    • pp.111-116
    • /
    • 2002
  • The regularity effect for printed word recognition and naming depends on ambiguities between single letters (small grain-size) and their phonemic values. As a given word is repeated and becomes more familiar, letter-aggregate size (grain-size) is predicted to increase, thereby decreasing the ambiguity between spelling pattern and phonological representation and, therefore, decreasing the regularity effect. Lexical decision and naming tasks studied the effect of repetition on the regularity effect for words. The familiarity of a word from was manipulated by presenting low and high frequency words as well as by presenting half the stimuli in mixed upper- and lowercase letters (an unfamiliar form) and half in uniform case. In lexical decision, the regularity effect was initially strong for low frequency words but became null after two presentations; in naming it was also initially strong but was merely reduced (although still substantial) after three repetitions. Mixed case words were recognized and named more slowly and tended to show stronger regularity effects. The results were consistent with the primary hypothesis that familiar word forms are read faster because they are processed at a larger grain-size, which requires fewer operations to achieve lexical selection. Results are discussed in terms of a neurobiological model of word recognition based on brain imaging studies.

  • PDF

Effect of Debinding Conditions on the Microstructure of Sintered Pb(Mg1/3Nb2/3)O3-PbTiO3

  • Yun Jung-Yeul;Jeon Jae-Ho;L.Kang Suk-Joong
    • 한국분말재료학회지
    • /
    • 제12권4호
    • /
    • pp.261-265
    • /
    • 2005
  • In order to fabricate complex-shaped polycrystalline ceramics by sintering, organic binders are usually pre-mixed with ceramic powders to enhance the formability during the shape forming process. These organic binders, however, must be eliminated before sintering so as to eliminate the possibilities of poor densification and unusual grain growth during sintering. The present work studies the effect of binder addition on grain growth behavior during sintering of $92(70Pb(Mg_{1/3}Nb_{2/3})O_3-30PbTiO_3))$-8PbO(mol%) piezoelectric ceramics. The microstructures of the sintered samples were examined for various heating profiles and debinding schedules of the binder removal process. Addition of Polyvinyl butyral(PVB) binder promoted abnormal grain growth especially in incompletely debinded regions. Residual carbon appears to change the grain shape from comer-rounded to faceted and enhance abnormal grain growth.

Effect of Residual Binder on Grain Growth during Sintering of $Pb(Mg_{1/3}Nb_{2/3})O_3-PbTiO_3$

  • Yun, Jung-Yeul;Jang, Wook-Kyung;Jeon, Jae-Ho;L.Kang, Suk-Joong
    • 한국분말야금학회:학술대회논문집
    • /
    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
    • /
    • pp.209-210
    • /
    • 2006
  • Organic binders are usually pre-mixed with ceramic powders to enhance the formability during the shape forming process. These binders, however, must be eliminated before sintering in order to avoid pore formation and unusual grain growth during sintering. The present work was performed to investigate the effects of residual binder on grain growth behavior during sintering of $Pb(Mg_{1/3}Nb_{2/3})O_3-PbTiO_3$ piezoelectric ceramics. The microstructures of sintered samples were examined for various thermal processes and atmosphere at debinding. Addition of binder seems to promote abnormal grain growth especially in incompletely debinded regions and to make the grain shape change from corner-rounded to faceted.

  • PDF

CuZn36 합금의 입자 미세화에 미치는 Zr, B, P 첨가의 영향 (Effects of Zr, B and P Additions the Grain Refinement of CuZn36 Alloys.)

  • 김정근;이동우
    • 한국주조공학회지
    • /
    • 제13권2호
    • /
    • pp.168-174
    • /
    • 1993
  • It has been known that the grain refinement of Cu base alloys greatly improved mechanical properties, castability, workability and hot shortness resistance etc. In this study CuZr50, CuP7, CuFe7, CuMg10 binary alloys were added as grain refiners in CuZn36 alloy. The alloys melted in vacuum and controlled in mixed gas conditions and casted at $1050^{\circ}C$. Zr-P-X compound has significantly grain refined but oxygen has been found detrimental to grain refinement. In the case of Zr /B ratio below 4, B acted as grain growth element in this alloy.

  • PDF

전라북도 지역 당뇨환자의 잡곡밥 섭취 실태 및 혼합비를 달리한 잡곡밥의 관능검사 (Status of Mixed Grain Diet by People with Diabetes in Jeollabuk-do and Sensory Evaluation of Different Composition of Mixed Grains)

  • 정은순;신동화;두재균;채수완;김영수;박영민
    • 한국식품영양과학회지
    • /
    • 제39권7호
    • /
    • pp.1049-1055
    • /
    • 2010
  • 본 연구에서는 전라북도 지역에 거주하는 68명의 당뇨환자들을 대상으로 잡곡밥 섭취 실태를 조사하였고 이를 바탕으로 관능성을 개선하기 위하여 잡곡의 혼합비를 달리한 잡곡밥을 대상으로 관능검사를 실시하였다. 조사대상자의 BMI를 측정한 결과 전체 대상자 중 61.7%가 과체중 이상이었다. 잡곡밥 섭취실태를 조사한 결과 94.1%가 잡곡밥을 섭취하였고, 성별에 따른 섭취율은 여성이 남성에 비해 더 자주 섭취하였으며(p<0.05), 섭취이유에 대해서 알아본 결과 남녀 모두 건강에 좋아서 섭취한다고 응답한 대상자가 가장 많았다. 잡곡밥에 혼합하는 잡곡의 수는 여성이 남성에 비하여 더 많은 잡곡을 혼합하였으며(p<0.01), 지속적인 섭취 여부를 알아본 결과 '지속적으로 먹겠다'라고 응답한 여성이(47.1%) 남성(36.8%)보다 많았다(p<0.05). 잡곡밥 섭취 기간은 3년 이상 섭취 59%, 잡곡의 구입 장소는 집주변 소형마트 46.0%로 가장 많았으며, 흰밥에 가장 많이 혼합하는 잡곡은 검정콩(76.5%)으로 조사되었다. 멥쌀을 제외하고 보리, 현미 등 6가지 잡곡의 혼합비율을 50%로 만든 RMGD-50과 40%로 만든 RMGD-40의 비교 관능검사 결과 겉모양과 색깔에 있어 잡곡의 함량이 많은 RMGD-50이 상대적으로 잡곡의 함량이 적은 RMGD-40보다 낮은 점수를 받았으며($3.33{\pm}0.68$, $3.50{\pm}0.81$), 당뇨환자들은 잡곡의 혼합비율이 보다 낮은 잡곡밥을 더 선호하는 것으로 나타났다. RMGD-40과 찰성 곡물 함량이 많은 Control 1, 백미인 Control 2를 비교 평가한 결과 Control 1에 비해 RMGD-40은 겉모양, 냄새, 색깔에서는 낮은 점수를 받았으나 유의적인 차이는 나타나지 않았다. 잡곡밥에 익숙한 입맛을 가진 당뇨환자들에게 백미는 질기, 씹힘성, 맛 항목에서 가장 낮은 점수를 보였으며($3.26{\pm}0.82$, $3.48{\pm}0.85$, $3.19{\pm}0.70$), 이는 RMGD-40 및 Control 1과 유의적인 차이를 나타냈다(p<0.01). 결론적으로 당뇨환자들은 잡곡의 비율이 보다 낮고 찰성 곡물의 함량이 많은 잡곡밥을 선호하였다. 따라서 바람직한 혈당 관리를 위하여 당뇨환자들에게 곡류의 섭취에 대한 교육이 반드시 필요하며 당뇨환자들을 위하여 혈당관리에 도움이 되는 잡곡밥의 개발에 대한 연구가 지속적으로 이루어져야 할 것이다.

상황버섯 및 카레를 첨가한 잡곡밥 추출물의 LLC-PK1 세포에서의 산화적 스트레스 보호 효과 (Protective Effects of Phellinus linteus and Curry-Added Cooked Mixed Grain Rice Extracts on Oxidative Stress-Induced LLC-PK1 Cell Damage)

  • 이정숙;송가락;길정하;정병진;정종성;허태곤;박건영
    • 한국식품영양과학회지
    • /
    • 제43권11호
    • /
    • pp.1674-1680
    • /
    • 2014
  • 잡곡밥 메탄올 추출물이 가지는 산화적 스트레스 개선 효과를 확인하기 위하여 $H_2O_2$로 유도된 산화적 스트레스에 대한 LLC-PK1 세포의 보호 효과를 조사하였다. $250{\mu}M$$H_2O_2$에 의한 산화적 스트레스가 유발된 LLC-PK1 세포에 시료추출물을 처리한 결과, WR, TMR, GR 순으로 $H_2O_2$ 처리군에 비해 세포 생존율이 증가하였다(P<0.05). 특히 GRS와 GRK에서 정상군에 가까운 세포 생존율을 나타내어 $H_2O_2$에 의한 산화적 스트레스로 유발된 세포 손상에 대한 잡곡밥 추출물의 보호 효과를 확인할 수 있었다. 세포 내 활성산소(ROS)의 수준과 세포 내 지질과산화물질(MDA)의 생성 억제 효과 역시 WR, TMR, GR, GRK, GRS 순으로 증가하는 것을 관찰하였다. $H_2O_2$로 인하여 세포 내 항산화 효소인 SOD, CAT와 GSH-px 등의 활성이 감소된 LLC-PK1 세포에 잡곡밥 추출물을 처리했을 때 이들 효소의 활성이 증가했으며 특히 GRK, GRS군에서 현저하게 증가되었다. LLC-PK1 세포에서 $H_2O_2$에 의해 발생하는 산화적 스트레스에 대한 보호 효과를 측정한 결과 잡곡밥 추출물은 세포 손상을 억제하고 세포 내 활성산소(ROS)의 수준과 지질과산화물질(MDA)의 생성을 억제하며, 세포 내 항산화 효소의 활성을 증가시키는 효과를 가지는 것으로 보인다. 또한 항산화 효소유전자 발현에서도 위와 비슷한 효과를 나타내었다. 이상의 결과로 잡곡밥 메탄올 추출물, 특히 기능성 물질인 카레가루와 상황버섯 추출물이 첨가된 잡곡밥은 LLC-PK1 세포에 대한 보호 작용과 in vitro에서의 항산화 효과가 높은 것으로 확인되었다.

Fe-20Mn-12Cr-1Cu 제진합금의 고온가스 질화처리 (High Temperature Gas Nitriding of Fe-20Mn-12Cr-1Cu Damping Alloy)

  • 성지현;김영희;성장현;강창룡
    • 열처리공학회지
    • /
    • 제26권3호
    • /
    • pp.105-112
    • /
    • 2013
  • The microstructural changes of Fe-20Mn-12Cr-1Cu alloy have been studied during high temperature gas nitriding (HTGN) at the range of $1000^{\circ}C{\sim}1150^{\circ}C$ in an atmosphere of nitrogen gas. The mixed microstructure of austenite and ${\varepsilon}$-martensite of as-received alloy was changed to austenite single phase after HTGN treatment at the nitrogen-permeated surface layer, however the interior region that was not affected nitrogen permeation remained the structure of austenite and ${\varepsilon}$-martensite. With raising the HTGN treatment temperature, the concentration and permeation depth of nitrogen, which is known as the austenite stabilizing element, were increased. Accordingly, the depth of austenite single phase region was increased. The outmost surface of HTGN treated alloy at $1000^{\circ}C$ appeared Cr nitride. And this was in good agreement with the thermodynamically calculated phase diagram. The grain growth was delayed after HTGN treatment temperature ranges of $1000^{\circ}C{\sim}1100^{\circ}C$ due to the grain boundary precipitates. For the HTGN treatment temperature of $1150^{\circ}C$, the fine grain region was shown at the near surface due to the grain boundary precipitates, however, owing to the depletion of grain boundary precipitates, coarse grain was appeared at the depth far from the surface. This depletion may come from the strong affinity between nitrogen and substitutional element of Al and Ti leading the diffusion of these elements from interior to surface. Because of the nitrogen dissolution at the nitrogen-permeated surface layer by HTGN treatment, the surface hardness was increased above 150 Hv compared to the interior region that was consisted with the mixed microstructure of austenite and ${\varepsilon}$-martensite.