• Title/Summary/Keyword: mineral analyses

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Determining N value from SPT blows for 30 cm penetration in weathered strata

  • Sun, Chang-Guk;Cho, Hyung-Ik;Kim, Han-Saem;Lee, Moon-Gyo
    • Geomechanics and Engineering
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    • v.28 no.6
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    • pp.625-636
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    • 2022
  • The standard penetration test (SPT) obtaining the N value of the number of blows has been widely used in various subsurface conditions, including in weathered soil and rock on fresh bedrock, in geotechnical studies pertaining to the design of foundations and earth structures. This study examined the applicability of SPTs terminated conventionally after 50 blows for a penetration of less than 30 cm, particularly in weathered strata, at four sites in Korea. The N values obtained during practical SPTs are typically extrapolated linearly at 30 cm penetration, despite the possibility of a nonlinear relationship between blow counts and penetration. Such nonlinearity in weathered strata has been verified by performing special SPTs ensuring 30 cm penetration. To quantify the nonlinearity in dense strata, we conducted statistical regression analyses comparing the differences (DN) between the N values measured by the special SPTs and those extrapolated using the practical approach with the differences (DP) between the 30 cm penetration and the penetration during 50 blows. Bi-linear relationship models between DN and DP were subsequently proposed for determining the N values at 30 cm penetration in weathered strata. The N values reflecting nonlinearity could be determined from the linearly extrapolated N values by adding a modeled DN value.

Environmental Control of Chemical Composition of the Secondary Hydroxyapatite from Japan

  • Kashima, Naruhiko;Tazaki, Kazue;Fyfe, W.S.
    • Journal of the speleological society of Korea
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    • no.8
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    • pp.11-18
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    • 1998
  • The mineral hydroxyapatite is very common species in secondary phosphates originating from guanos(HILL et at., 1997). Several mineralogical analyses of spelean hydroxyapatite exist(e.g., KASHIMA, 1968, 1979 ; MAKI et at., 1977 ; SUH et at., 1978 ; WANG, 1982 a, b), whereas detailedeochemical composition of secondary hydroxy apatites has not been reported in Japan.(omitted)

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A Study on Geology and Clay Minerals of the Landslide Area in the Munhyun-dong, Nam-gu, Pusan (부산시 남구 문현동 산사태 지역의 지질 및 점토광물에 대한 연구)

  • 황진연;김선경;김춘식
    • Journal of the Korean Geotechnical Society
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    • v.15 no.1
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    • pp.113-125
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    • 1999
  • In this study the occurrence and mineralogical characteristics of clay minerals from the Munhyun-dong landslide area in Pusan city were examined by XRD, SEM, and chemical analyses. Several types of clay minerals such as halloysite, vermiculite, mica/vermiculite interstratified mineral, vermiculite/smectite interstratified mineral, kaolinite and illite are found abundantly in the area. The occurrence of clay minerals suggest that they have been formed by weathering of andesite which is the bedrock of the area. It is believed that halloysite was formed in the early stage of weathering, and vermiculite, mica/vermiculite interstratified mineral and mica/vermiculite interstratified mineral were formed in the middle stage, and finally, kaolinite was formed. The clay minerals occurring in the central part of the landsliding area and within the slip surface are dominated by expandable minerals such as halloysite, vermiculite and vermiculite/smectite interstratified mineral. These clay minerals expand by absorbing water and effectively decrease the shear resistance of the rock mass, and therefore, they could be an important factor for the landslide. The analyses of geology and mineralogical characteristics of the area suggest that the landslide was caused by combination of various factors including steep slope, heavy rainfall, abundant joints, alteration of the rocks, and occurrence of expandable clay minerals. The result of this study suggests that the investigation for the prevention of possible landslide must include the examination of clay mineralogy as well as the site geology.

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Trace element concentrations profiles in the hair of normal children living in the northern area of Seoul (서울 북부지역에 거주하는 정상 아동의 모발 미네랄 함량)

  • Kwon, Ji Won;Kim, Byung Eui;Park, Mi Jung;Kim, Sang Woo
    • Clinical and Experimental Pediatrics
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    • v.49 no.1
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    • pp.18-23
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    • 2006
  • Purpose : The reliability of hair mineral analyses regarding nutritional status, environmental exposure or diseases is controversial. The aim of this study was to determine the normal reference range of hair mineral concentration of Korean children. Methods : We examined hair mineral concentrations of 223 children(3-12 yrs old, 110 boys, 113 girls, mean age $8.8{\pm}2.2$ yrs old) living in the northern area of Seoul. The trace elements including six toxic elements(Al, As, Cd, Ba, Hg, Pb) and 11 nutritional elements(Na, Mg, P, K, Ca, Cr, Mn, Fe, Cu, Zn, Se) were analyzed by inductive coupled plasma mass spectrometry(ICP-MS). Results : The mean concentrations of Ca and Mg were higher in girls than in boys. The mean concentrations of Cd, Pb and Cr were higher in boys than girls. The Zn, Ca, Mg, Cu and Hg levels in hair samples were positively correlated with increasing age. The Zn levels of the Korean children's hair samples appear to be lower than that of other countries' reference values. Conclusion : There are considerable differences in hair mineral concentrations by age, sex and race. Additional research is needed to establish Korean reference values, and to evaluate the usefulness of hair mineral analyses as a screening tool for nutrition- and environment-related childhood diseases.

Mineralogy and Chemical Properties according to Particle Size Separation of Hwangto (Reddish Residual Soil) used in Feeding of Cattle (한우 사육에 이웅한 황토(풍화토)의 입도분리에 따른 광물성분 및 화학적 특성)

  • 황진연;박현진;양경희;이효민
    • Journal of the Mineralogical Society of Korea
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    • v.15 no.1
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    • pp.33-43
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    • 2002
  • Mineral composition and chemical properties of Hwangto (reddish residual soil) that used in feeding of cattles at Iksan, Jeollabuk-do, Korea were examined according to particle size separation such as gravel, sand, silt, coarse clay and fine clay. Mineral composition analyses reveal that gravel and sand are mainly composed of quartz and feldspars and that kaolin mineral and illite are dominant in clay and silt. Iron oxides are mainly included in fine clay. According to chemical analyses of major elements, Al, Fe and $H_2O$ contents are increased with decreasing of particle size. This trend well agrees with increase of clay minerals in smaller particles, Chemical analyses of trace elements indicate that contents of Zn, Rb, Sr, Ba, Pb significantly differ with particle sizes. Ba and Sr are included in feldspars since these elements are abundant in sand containing abundant feldspars. Pb and Sm are abundant in sample before particle size separation, but the contents are significantly decreased after separation. Therefore, most of these elements appear to be existed as removable phase. Nb, La, Th, Ce are more abundant in silt. The contents of all the other trace elements tend to be increased in smaller particles containing more clay minerals. The contents of changeable cations and teachable elements in acid and alkali solutions are high in clay samples. All the above results indicate that using the portion of smaller particle of Hwangto for livestock feed rather than bulk Hwangto can improve cation exchangeable capacity, ion leaching capacity and sorption properties.

Association of Calcium Intake and Bone Mineral Density by Vitamin D Receptor Genotype among Elderly Women Living in Rural a Area (노년기 농촌여성의 비타민 D 수용체 유전자형에 따른 칼슘 섭취량과 골밀도와의 관계)

  • Kim Ji-Sun;Kim Hee-Seon
    • Korean Journal of Community Nutrition
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    • v.11 no.4
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    • pp.534-540
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    • 2006
  • Recent studies have shown that environmental, biochemical, nutritional or genetic factors affect bone mineral density (BMD). The purpose of the present study was to investigate the effect of vitamin D receptor (VDR) gentotype and nutritional status on BMD of elderly women living in a rural area. Three hundred thirty five elderly women over 65 years in Asan participated the study. Data for demographic and nutrient intakes were obtained by survey with a two day 24 hr recall method. BMD was measured by broadband ultrasound attenuation (BUA) using quantitative ultrasound (QUS). VDR genotypes of the subjects analyzed with Bsm I restriction enzyme were bb (92%), Bb (7%) and BB (1%). No differences were found between genotypes bb and Bb/BB in age, menopausal age, body mass index and body fat. BUA of bb genotype was higher (62.5 $\pm$ 15.6 dB/MHz) than Bb/BB genotype (56.1 $\pm$ 17.6 dB/MHz) by Student's t-tests. Correlation analyses showed strong negative correlation of BMD and age, but positive correlation with BMI, energy and calcium intake. When subgroup analyses were conducted after stratification by the median calcium intake level (412.9 mg/d), the above median calcium intake group showed significant difference in BUA by VDR genotype while the lower median calcium intake group did not show significant difference. The current study confirmed interaction of calcium intake and VDR genotype in association with BMD. Further nutritional intervention will be needed to improve calcium status of the elderly women living in rural areas.

Mineralogical Properties of Asian Dust in April 6 and 15, 2018, Korea (2018년 4월 6일과 15일 황사의 광물학적 특성)

  • Jeong, Gi Young
    • Journal of the Mineralogical Society of Korea
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    • v.31 no.2
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    • pp.103-111
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    • 2018
  • Mineralogical properties of two Asian dust (Hwangsa) samples collected during dust events in April 6 and 15, 2018 were examined by X-ray diffraction (XRD) and scanning electron microscopy (SEM). XRD analyses showed that Asian dusts were dominated by phyllosilicates (62 wt%) comprising illite-smectite series clay minerals (ISCMs) (55%), chlorite (3%) and kaolinite (4%). Nonphyllosilicate minerals were quartz (18%), plagioclase (9%), K-feldspar (3%), calcite (3%), and gypsum (2-4%). Mineral compositions determined by SEM chemical analyses were consistent with XRD data. ISCMs occur as submicron grains forming aggregate particles or coating coarse mineral grains such as quartz, plagioclase, K-feldspar, chlorite, and calcite. The ISCMs are often associated with calcite nanofibers and gypsum blades. Mineralogical properties of 2018 dusts were similar to those of previous dusts although clay contents were higher than that of coarse 2012 dust.

Petrochemical Study on the Micrographic Granite in the Wando Area (완도지역(莞島地域)에 분포하는 미문상화강암(微文象花崗岩)에 대한 암석화학적(岩石化學的) 연구(硏究))

  • Shin, In-Hyun;Nam, Ki-Sang;Kim, Hee-Nam;Park, Young-Seog;Ahn, Kun-Sang
    • Economic and Environmental Geology
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    • v.27 no.2
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    • pp.181-190
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    • 1994
  • Petrochemical study on the micrographic granite distributed in the Wando area, the southernmost part of the Yeongdong-Kwangju depression is performed to investigate the petrogenesis and differentiation processes of the granitic magma. Polarized light microscopy for modal analyses, electron probe microanalyses of feldspars and biotite, inductively coupled plasma analyses for major and trace element contents were adopted in the study. The lithology of the study area consists of Precambrian metasediments, Mesozoic volcanic and sedimentary rocks, and micrographic granite which intrude into the former. The micrographic granite in the Wando area are distributed in the shape of a cauldron. Modal and nonnative mineral analyses of the micrographic granite fall in the area of granite and granodiorite. The chemical composition indicates that the micrographic granite is I-type and magnetite series. The micrographic granite is characterized by more than 90% of micrographic texture in volume percent. Feldspars in the micrographic granite is alkali feldspars (Or, 45~93) and plagioclases (albite to oligoclase). The biotite has a intermediate composition between phlogopite and annite solid solution. The results of the petrochemical studies indicate that the granitic magma of calc-alkaline source materials reactivated in a compressional environment at the continental margin, and then was differentiated by fractional crystallization. The micrographic granite intruded into a shallow level of the crust (5~7 km) in the late Cretaceous.

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Damage of Minerals in the Preparation of Thin Slice Using Focused Ion Beam for Transmission Electron Microscopy (투과전자현미경분석용 박편 제작 시 집속이온빔에 의한 광물 손상)

  • Jeong, Gi Young
    • Journal of the Mineralogical Society of Korea
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    • v.28 no.4
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    • pp.293-297
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    • 2015
  • Focused ion beam (FIB) technique is widely used in the precise preparation of thin slices for the transmission electron microscopic (TEM) observation of target area of the minerals and geological materials. However, structural damages and artifacts by the Ga ion beam as well as electron beam damage are major difficulties in the TEM analyses. TEM analyses of the mineral samples showed the amorphization of quartz and feldspar, curtain effect, and Ga contamination, particularly near the grain edges and relatively thin regions. Although the ion beam damage could be much reduced by the improved procedures including the adjustment of the acceleration voltage and current, the ion beam damage and contamination are likely inevitable, thus requiring careful interpretation of the micro-structural and micro-chemical features observed by TEM analyses.

Evaluation of regeneration after the application of 2 types of deproteinized bovine bone mineral to alveolar bone defects in adult dogs

  • Lee, Dajung;Lee, Yoonsub;Kim, Sungtae;Lee, Jung-Tae;Ahn, Jin-soo
    • Journal of Periodontal and Implant Science
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    • v.52 no.5
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    • pp.370-382
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    • 2022
  • Purpose: The aim of this study was to evaluate the preclinical results of 2 types of commercially available deproteinized bovine bone mineral (DBBM) when applied to alveolar bone defects in dogs. Methods: This study was conducted using 6 beagles. Alveolar defects in the mandible were formed and filled with 2 DBBMs produced by a similar procedure. Defects were randomly assigned to be filled using DBBM 1 or 2. All defects were covered with a collagen membrane and had a healing period of 12 weeks. After the dogs were sacrificed, histological, histomorphometric, and linear/volumetric analyses were performed. Results: Both DBBM groups showed similar histological findings, demonstrating that bone remodeling had occurred and new bone had formed. The residual bone particles were surrounded by newly formed vital bone. In the histomorphometric analysis, the ratio of the area of vital bone and residual bone substitute in DBBM 2 (38.18% and 3.47%, respectively) was higher than that of DBBM 1 (33.74% and 3.41%, respectively), although the difference was not statistically significant. There were also no statistically significant differences between both groups in linear and volumetric analyses using micro-computed tomography scans and digitized images of dental casts. Conclusions: In the present study, DBBM 1and 2, which were produced by similar processes, showed similar results in histological, histomorphometric, and volumetric analyses. Further studies are needed to identify more specific differences between the 2 DBBMs.