• 제목/요약/키워드: microwave absorption

검색결과 170건 처리시간 0.025초

Electron Spin Resonance (ESR) and Microwave Absorption Studies of Superparamagnetic Iron Oxide Nanoparticles (SPIONs) for Hyperthermia Applications

  • Choi, Yong-Ho;Yi, Terry;Kim, Do-Kyung
    • 한국세라믹학회지
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    • 제48권6호
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    • pp.577-583
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    • 2011
  • Stabilized biocompatible superparamagnetic iron oxide nanoparticles (SPIONs) were prepared by controlled coprecipitation method for hyperthermia application. ESR measurements determined that all of the interactions in the individual SPIONs (1 nm and 11 nm) were antiferromagnetic in nature because the ions contributed to the magnetization with a range of magnetic moments. In-situ monitoring of the temperature increment was performed, showing that the microwave absorption rate of the SPIONs was dispersed in an appropriate host media (polar or non-polar solvents) during microwave irradiation. Microwave absorption energy rates and heat loss of SPIONs in solvent were calculated by non-linear data fitting with an energy balance equation. The microwave absorption rates of SPIONs dispersed in solvent linearly increases when the concentration of SPIONs increases, implying that the microwave absorption rate can be tunable by changing the concentration of SPIONs.

옻을 지지재로 이용한 복합형 전자파 흡수체의 제작 (Manufacture of Composite Electromagnetic Absorber using Natural Lacquer Binder)

  • 김동일;최동한;김수정;박우근;송재만;김민정
    • 한국전자파학회논문지
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    • 제14권7호
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    • pp.756-761
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    • 2003
  • 고성능 광대역 복합형 전자파 흡수체를 개발하기 위해 지금까지 지지재로 주로 사용되어오던 Silicone과 CPE 그리고 본 연구에서 새롭게 제안하는 전통 옻에서 사용되어 오던 옻에 대한 전자파 흡수능을 조사하였다. 또한 이들과 MnZn 페라이트를 혼합한 전자파 흡수체를 제작하여 이들의 전자파 흡수능을 조사하였다. 옻을 지지재로 한 MnZn 페라이트 복합형 전자파 흡수체는 CPE와 Silicone을 지지재로 한 전자파 흡수체에 비하여 광대역에서 우수한 전파흡수특성을 나타내었다.

Microwave Absorbers Prepared with Alnico Magnets

  • Song Jae Man;Kim Dong Il;Shin Seung Jae;Moon Sang Hyun;Choi Jung- Hyun;Jeung Jae Hyun
    • 한국항해항만학회지
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    • 제29권2호
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    • pp.147-150
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    • 2005
  • We suggest a cast Alnico magnet as a new microwave absorber. The proposed Alnico microwave absorber shows advanced microwave absorption properties of 24 dB at 13.3 GHz for the thicknesses of 1 mm We also investigated the effects of the carbon, which qjfects strongly to microwave absorption in Alnico magnet microwave absorbers. Central frequency shifts toward lower frequency with increasing Alnico content which is related to the frequency to show tan 8 > 1. Also, we investigated the sample thickness dependence on the microwave absorption properties.

Preparation and Microwave Absorption Properties of the Fe/TiO2/Al2O3 Composites

  • Li, Yun;Cheng, Haifeng;Wang, Nannan;Zhou, Shen;Xie, Dongjin;Li, Tingting
    • Nano
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    • 제13권11호
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    • pp.1850125.1-1850125.12
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    • 2018
  • To reduce the imbalance of impedance matching between the magnetic metal nanowires and free space, $Fe/TiO_2$ core/shell nanowire arrays with different diameters were fabricated in the templates of anodic aluminum oxide membranes by electrodeposition. The influences of the microstructure on the microwave absorption properties of the $Fe/TiO_2/Al_2O_3$ composites were studied by the transmission/reflection waveguide method. It was demonstrated experimentally that both the interfacial polarization and the diameter of the $Fe/TiO_2$ core/shell nanowires have critical effects on the microwave absorption properties. We also investigated the angle dependence of the microwave absorption properties. Due to the interfacial polarization and associated relaxation, the $Fe/TiO_2/Al_2O_3$ composites exhibited optimal microwave absorption properties when microwave propagation direction was accordant with the axis of the nanowires. Finally, we managed to obtain an optimal reflection loss of below -10 dB (90% absorption) over 10.2-14.8 GHz, with a thickness of 3.0 mm and the minimum value of -39.4 dB at 11.7 GHz.

Microwave Absorption Study of Carbon Nano Materials Synthesized from Natural Oils

  • Kshirsagar, Dattatray E.;Puri, Vijaya;Sharon, Maheshwar;Sharon, Madhuri
    • Carbon letters
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    • 제7권4호
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    • pp.245-248
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    • 2006
  • Thin films of carbon-nano materials (CNMs) of different morphology have been successfully deposited on ceramic substrate by CVD at temperatures $800^{\circ}C$, $850^{\circ}C$ and $900^{\circ}C$ using plant based oils in the presence of transition metal catalysts (Ni, Co and Ni/Co alloys). Based on the return and insertion loss, microwave absorption properties of thin film of nanocarbon material are measured using passive micro-Strip line components. The result indicates that amongst CNMs synthesized from oil of natural precursors (mustered oil - Brassica napus, Karanja oil - Pongamia glabra, Cotton oil - Gossipium hirsuta and Neem oil - Azadirachta indica) carbon nano fibers obtained from neem's seed oil showed better microwave absorption (~20dB) in the range of 8.0 GHz to 17.90 GHz.

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마이크로파 feedline을 고려한 진행파형 광변조기의 특성 분석 (Microwave characteristics of traveling-wave modulator considering the microwave feedline)

  • 구민주;옥성해;윤영설;문연태;김도균;최영완
    • 대한전자공학회논문지SD
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    • 제41권4호
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    • pp.41-47
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    • 2004
  • 본 논문에서는 마이크로파 feedline을 포함하고, 광도파관과 마이크로파 feedline간의 임피던스 부정합을 고려하여 전계 흡수광변조기(traveling-wave electro-absorption modulator, TW-EAM)의 마이크로파 특성을 분석하였다. Co-planar waveguide(CPW)와 microstrip의 하이브리드 구조를 가지는 광도파관 부분은 등가회로를 통해 모델링 하였으며, 등가회로의 인덕턴스(L)와 커패시턴스 (C)는 3차원 FDTD를 기반으로 한 수식화를 통하여 구하였다. CPW 구조의 마이크로파 feedline은 모멘텀방식을 이용해 분석하였다. 이와 같은 분석을 통해 TW-EAM의 특성을 보다 정확하게 분석 할 수 있음을 제시한다.

Microwave-assisted Solvent-free Synthesis of Some Dimethine Cyanine Dyes, Spectral Properties and TD-DFT/PCM Calculations

  • Zhang, Xiang-Han;Wang, Lan-Ying;Zhai, Gao-Hong;Wen, Zhen-Yi;Zhang, Zu-Xun
    • Bulletin of the Korean Chemical Society
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    • 제28권12호
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    • pp.2382-2388
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    • 2007
  • A series of dimethine cyanine dyes were synthesized in a fast, efficient and high yield by the condensation of quaternary salts with 1H-indole-3-carbaldehyde in the presence of piperidine under solvent-free microwave irradiation. The products were identified by 1H NMR, IR, UV-Vis spectra and elemental analysis. The absorption and fluorescence properties of these dyes were investigated both experimentally and theoretically. Calculations performed at a combination of time-dependent density functional theory (TD-DFT) and the polarizable continuum model (PCM) reproduced the π-π* type absorption bands of the dyes. Regression analysis was used for studying theoretical results of the absorption maxima in different solvents. Compared with experimental counterparts, estimated overall uncertainties in the absorption maxima were about ±2%.

Evaluation of DNA Damage Using Microwave Dielectric Absorption Spectroscopy

  • Hirayama, Makoto;Matuo, Youichirou;Sunagawa, Takeyoshi;Izumi, Yoshinobu
    • Journal of Radiation Protection and Research
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    • 제41권4호
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    • pp.339-343
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    • 2016
  • Background: Evaluation of deoxyribonucleic acid (DNA)-strand break is important to elucidate the biological effect of ionizing radiations. The conventional methods for DNA-strand break evaluation have been achieved by Agarose gel electrophoresis and others using an electrical property of DNAs. Such kinds of DNA-strand break evaluation systems can estimate DNA-strand break, according to a molecular weight of DNAs. However, the conventional method needs pretreatment of the sample and a relatively long period for analysis. They do not have enough sensitivity to detect the strand break products in the low-dose region. Materials and Methods: The sample is water, methanol and plasmid DNA solution. The plasmid DNA pUC118 was multiplied by using Escherichia coli JM109 competent cells. The resonance frequency and Q-value were measured by means of microwave dielectric absorption spectroscopy. When a sample is located at a center of the electric field, resonance curve of the frequency that existed as a standing wave is disturbed. As a result, the perturbation effect to perform a resonance with different frequency is adopted. Results and Discussion: The resonance frequency shifted to higher frequency with an increase in a concentration of methanol as the model of the biological material, and the Q-value decreased. The absorption peak in microwave power spectrum of the double-strand break plasmid DNA shifted from the non-damaged plasmid DNA. Moreover, the sharpness of absorption peak changed resulting in change in Q-value. We confirmed that a resonance frequency shifted to higher frequency with an increase in concentration of the plasmid DNA. Conclusion: We developed a new technique for an evaluation of DNA damage. In this paper, we report the evaluation method of DNA damage using microwave dielectric absorption spectroscopy.

도금공정 크롬시료 분석을 위한 Microwave Oven Digestion/Atomic Absorption Spectrophotometry 방법의 정확도 및 정밀도 평가 (Accuracy and Precision of Microwave Oven Digestion/Atomic Absorption Spectrophotometry for Analyzing Airborne Chromium Collected on MCE Filter in Plating Operation)

  • 이병규;이지태;신용철
    • 한국산업보건학회지
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    • 제11권1호
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    • pp.48-55
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    • 2001
  • The purpose of this study was to evaluate the analytical accuracy and precision of microwave oven digestion/atomi absorption spectrophotometry (AAS) for analyzing airborne chromium collected on mixed cellulose ester membrane (M filter from the work environment, and to compare the accuracy and the precision with those of the National Institute for Occupational Safety and Health (NIOSH) Method #7024 hot plate digestion/AAS method. For this study, field air sample pairs were collected from a electroplating process, and spiked samples in a laboratory were prepared and using these samples. Two digestion methods were comp; and evaluated in terms of recovery rate and bias as indices of accuracy and coefficient of variation as a index of precision. The results and conclusions are as follows. In spiked samples, the accuracies (% mean recoveries) of hot plate/AAS and microwave oven/AAS method were 97.19%, 97.1%, respectively, and the precisions (pooled respectively, and the precisions (pooled coefficient of variance, $CV_{pooled}$) 6.93% and 3.88%, respectively. The biases of hot plate ani microwave oven methods were 4.56 - 14.7% and 2.22 - 7.42% respectively. There was no statistically significant difference between hot plate and microwave oven methods recovery rates of spiked samples (p>0,05). Also, no statistically significant difference was shown among the concentrations of air samples determined by two method (p>0.05). In conclusion, microwave oven/AAS method h excellent accuracy and precision, and advantages such as time-saving and simple procedure in comparison with the classical NIOSH method. Therefore, this method can be use widely to analyze airborne chromium collected on MCE filter from the work environments.

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마이크로파 feed line을 고려한 진행파형 광 변조기의 특성 분석 (Microwave characteristics of traveling-wave modulator considering the microwave feed-line)

  • 구민주;옥성해;최영완
    • 한국정보통신설비학회:학술대회논문집
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    • 한국정보통신설비학회 2003년도 하계학술대회
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    • pp.172-174
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    • 2003
  • In this paper, we analyze the traveling-wave electro-absorption modulator (TW-EAM) in consideration of the microwave feed-line. The TW-EAM is analyzed by using the equivalent circuit model. The microwave feed-line isanalyzed by momentum method. In a view point of microwave characteristics, we present the effect of the structure and the length of microwave feed-line.

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