• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2007년도 추계학술대회 논문집
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• pp.322-325
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• 2007

Precipitation characteristics of the Fe-36Ni based high strength Invar alloy for power transmission wire was investigated in this study. High strength can be obtained in this alloy through solution hardening, precipitation hardening and strain hardening by cold working. In the present study, ingots of Fe-36Ni based Invar alloys with the contents of C, Mo and V varied. Microstructure observations by OM, SEM, and TEM were carried out to validate the simulation results. BCC phase and $FeNi_3$ phase are also expected at lower temperatures below $500^{\circ}C$. Aging treatments were carried out at temperatures ranging from 400 to $900^{\circ}C$ for time intervals from 3 min to 100hrs. Peak aging condition was obtained as $400^{\circ}C$ and 1 hr. With temperature increased, peak strength was decreased abruptly. Microstructure observation was conducted by optical microscopy, scanning electron microscopy, and transmission electron microscopy.

• 한국재료학회지
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• 제27권9호
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• pp.507-511
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• 2017

An optimum route to fabricate oxide dispersion strengthened ferritic superalloy with desired microstructure was investigated. Two methods of high energy ball milling or polymeric additive solution route for developing a uniform dispersion of $Y_2O_3$ particles in Fe-Cr-Al-Ti alloy powders were compared on the basis of the resulting microstructures. Microstructural observation revealed that the crystalline size of Fe decreased with increases in milling time, to values of about 15-20 nm, and that an FeCr alloy phase was formed. SEM and TEM analyses of the alloy powders fabricated by solution route using yttrium nitrate and polyvinyl alcohol showed that the nano-sized Y-oxide particles were well distributed in the Fe based alloy powders. The prepared powders were sintered at 1000 and $1100^{\circ}C$ for 30 min in vacuum. The sintered specimen with heat treatment before spark plasma sintering at $1100^{\circ}C$ showed a more homogeneous microstructure. In the case of sintering at $1100^{\circ}C$, the alloys exhibited densified microstructure and the formation of large reaction phases due to oxidation of Al.

• 열처리공학회지
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• 제37권1호
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• pp.9-15
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• 2024

Nd-Fe-B permanent magnets have been utilized on various industrial fields such as electric vehicles, generator, robots with actuator, etc, due to their outstanding magnetic properties even 10 times better than conventional magnets. Recently, there are many researches that report magnetic properties improved by controlling microstructure through adjusting alloying elements or conducting various processing. Especially, post-sintering annealing (PSA) can significantly improve the coercivity by modifying the distribution and morphology of Nd-rich phase which formed at grain boundaries. In this study, Nd-Fe-B sintered magnets were subjected to primary heat treatment followed by secondary heat treatment at 460℃, 500℃, and 540℃ to investigate the changes in microstructure and magnetic properties with the secondary heat treatment temperature. EBSD analysis was conducted to compare anisotropic characteristics. Through the SEM and TEM observation for analyzing the morphology and distribution of Nd-rich phase, we investigated the relationship between microstructure and magnetic properties of sintered Nd-Fe-B magnets.

• 대한기계학회논문집A
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• 제24권8호
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• pp.1910-1916
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• 2000

The five classes of the thermally aged CF8M specimen are prepared using an artificially accelerated aging method. Namely, after the specimens are held for 100, 300, 900, 1800, and 3600hrs at 430$^{\circ}C$ respectively, the specimens are water-cooled to room temperature. The impact energy variations are measures for both the aged and virgin specimens through the Charpy impact tests in addition to the microstructure observation, tensile, hardness and fatigue crack growth tests. From the present investigation the following results are obtained : 1) The difference among the thermally degraded specimens can be distinguished through their microstructures, 2) Hardness and tensile strength are increased to 300hrs, degradation specimen, while elongation and reduction area are decreased to 3600hrs degradation specimen, and impact energy is decreased to 1800hrs degradation specimen, 3) The FCG rates for thermally degraded specimens are larger than that of the virgin specimen.

• 대한치과기공학회지
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• 제27권1호
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• pp.57-63
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• 2005

Experimental Ti-13%Zr and Ti-13%Zr-5%Cu alloys were made in an argon-arc melting furnace. The grade 2 CP Ti was used to control. To investigate the surface reaction layers produced by the reaction with mold materials and the influence of the reaction layers on the hardness of castings, A phosphate bonded $SiO_2$ base investment was used as mold material, and microstructure observation and hardness test were performed. The surface reaction layers of Ti-13%Zr and Ti-13%Zr-5%Cu alloys were thinner than that of CP Ti had a clearly multiple structure. A difference of the hardness between surface and inner of the Ti-13%Zr and Ti-13%Zr-5%Cu alloys became less than that of CP Ti. From the results, it was found that the Ti-Zr-(Cu) based alloys were possible to cast with $SiO_2$ base investment without the great changes of mechanical properties of the castings.

• 열처리공학회지
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• 제18권2호
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• pp.83-90
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• 2005

Failure cause of the fractured engine parts was analyzed by microstructural observation. These parts were failed far earlier than the expected service life. By the stereoscope and SEM examinations of the fractured surface, the fracture modes have been identified as wear and fatigue failure. From the observation of microstructure and microhardness measurements of the failed gears, the probable cause for failures are internal oxidation during using and retained austenite and carbide networks due to heat-treatment, respectively. These defected structures at near surface contributed to the wear and fatigue failure.

• 열처리공학회지
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• 제27권4호
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• pp.191-201
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• 2014

The gear was made of SNC815 case-carburized, quench hardened and tempered steel. The gears were failed far earlier than the expected service life used in the industrial site. Causes of the failed gear were analyzed by microstructure observation. By the SEM and micro structure examinations, the damaged surfaces had been weared and failed by fatigue. Through microscope observation on the damaged surface, it was found that the cause of failure was determined by external overloading and the initial stage of the damage was closely related to complex contact fatigue failure. The overload and contact fatigue contributed to the early failure cause.

• 한국세라믹학회지
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• 제46권1호
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• pp.116-121
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• 2009

The constituent phases in Ti($C_{0.7}N_{0.3}$)-xWC-20Ni (wt%, x=5, 15, 25) cermets were characterized using nanoindentation in conjunction with observation of microstructure. The microstructure of cermet is composed of hard phase and binder phase, which gave rise to a wide range of hardness distribution when nanoindentation was carried out on the polished surface of cermets. Because of the inhomogeneous nature of cermet microstructure, observation of indented surface was indispensable in order to separate the hardness of each constituent phase. The measured values of hardness using nanoindentation were ${\sim}14\;GPa$ for the binder phase and ${\sim}24$ to 28 GPa for the hard phase, of which nanoindentation hardness was decreased with the addition of WC into Ti($C_{0.7}N_{0.3}$)-Ni system. In addition, the nanoindentation hardness of Ni binder phase was much higher than reported Vickers hardness, which could result from confined deformation of binder phase due to the surrounding hard phase particles.

• 한국표면공학회지
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• 제51권4호
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• pp.191-196
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• 2018

The self-annealing which leads evolution of microstructure in copper electroplating layers at room temperature occurs after forming deposition layer. During the process, crystal orientation, size and sheet resistance of plating layer change. Lastly, it causes the change of physical and mechanical characteristics such as a tensile strength of plating layer. In this study, the variation of incorporated impurities, microstructure and sheet resistance of copper plating layer formed by electroplating are measured with and without inorganic additives during the self-annealing. In case of absence of inorganic additives, the copper layer presents strong total intensity of incorporated impurities. During the self-annealing, such width of reduction was significant. Moreover, microstructure and crystal size are increased while the tensile strength is decreased noticeably. On the other hand, in the presence of inorganic additives, there is no observable distinction in the copper plating layer. According to the observation on movements of the incorporated impurities in electrodeposition copper layer, within 12 hours the impurities are continuously shifted from inside of the plating layer to its surface after as-deposited electroplating. Within 24 hours, except for the small portion of surface layer, it is considered that most of the microstructure is transformed.

• Journal of Periodontal and Implant Science
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• 제37권2호
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• pp.251-263
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• 2007

The present study was performed to evaluate the effects of Tetracycline-HCI on the microstructure change of SLA implant surface according to application time. In the Tetracycline-HCI group, 6 implants were rubbed with sponges soaked $50mg/m{\ell}$ Tetracycline-HCI solution for O.5min., lmin., 1. 5min., 2min., 2.5min. and 3min. In the saline group. another 6 implants conditioned with sponges soaked saline using same methods. One implant wasn't conditioned anything. Then, the changes of surface roughness values were evaluated by optical interferometer & specimens were processed for scanning electron microscopic observation. The results of this study were as follows: 1. In both Tetracycline-HCI group & saline group, there are no significant differences between surface roughness values before & after surface detoxification. And in scanning electron microscopic observation. there are slightly changes of implant surface structures but this changes were not significant by comparison with no treatment implant surface. 2. In the changes of surface roughness values & the scanning electron microscopic observation, there were no significant differences between saline & Tetracycline-HCI groups. In conclusion, the detoxification with $50mg/m{\ell}$ Tetracycline-HCI within 3 minutes can be applied for treatment of peri-implantitis in SLA surface implants. without surface microstructure changes.