• 제목/요약/키워드: micrographs

검색결과 417건 처리시간 0.028초

미세캡슐화를 위한 분무건조 다당류의 특성 (Characteristics of Spray Dried Polysaccharides for Microencapsulation)

  • 이승철;임채환;이상천
    • 한국식품과학회지
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    • 제29권6호
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    • pp.1322-1326
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    • 1997
  • 미세캡슐화를 위한 기초 연구로 다양한 다당류의 점도를 측정하고, 분무건조법을 이용하여 미세캡슐을 제조하여 특성을 비교하였다. 10% maltodexrin의 점도는 2.2 mPa.s, 10% gum arabic은 9.2 mPa.s, 10% dextran은 13.0 mPa.s, 1% gum locust bean은 4660.0 mPa.s, 1% gum karaya는 77.0 mPa.s로 측정되었다. 분무건조기를 이용하여 제조한 각종 다당류의 미세캡슐을 전자현미경으로 관찰한 결과, gum arabic은 20%의 농도에 비하며 30%에서 입자가 크게 형성되었으나 40%에서는 섬유상의 늘어진 형태가 관찰되었다. Maltodextrin 30%메서 고른 분포의 원형 입자가 관찰되었으며, 40%의 농도에서는 다양한 크기의 입자가 뭉쳐서 관찰되었다. Dextran은 20%에서 구형의 캡슐이 골고루 관찰되었으나, 30%이상의 농초에 서는 섬유상의 형태가 관찰되었다. Gum arabic : maltodextrin (1:3, w/w) 경우에서는 20%, 30%, 40%농도에서 구형의 캡슐이 고르게 관찰되었고 농도가 높을수록 입자의 크기가 증가하였다.

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집속 이온빔과 디지털 화상 관련법를 이용한 고 탄소 미세 강선의 잔류 응력 측정 (Measurement of residual stress of steel filaments by using focused ion beam and digital image correlation)

  • 양요셉;배종구;강기주;박찬경
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2007년도 춘계학술대회 논문집
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    • pp.241-245
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    • 2007
  • The residual stress in axial stress in the axial direction of the steel filaments has been measured by using a method based on the combination of the focused ion beam (FIB) and high resolution strain mapping program (VIC-2D). That is, the residual stress was calculated from the measured displacement field before and after the introduction of a slot along the steel filaments. The displacement was obtained by the digital correlation analysis of high-resolution scanning electron micrographs, while the slot was introduced by FIB milling with low energy beam. The present measurement revealed that the residual stress within 8% of the magnitude was persistent in the steel filaments fabricated.

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유구낭모충에 관한 연구 -유구낭모충의 미세구조- (Studies on the Bladder Worm, Cysticercus cellulosae -The Ulrastructure of C. cellulosae-)

  • 이순형
    • Parasites, Hosts and Diseases
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    • 제21권1호
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    • pp.75-82
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    • 1983
  • An electron microscopic study was performed to know the basic tegumental structure of Cysticercus cellulosae. The scolex and bladder portions of cysticerci (human and porcine strains) were prepared for transmission and scanning electron microscopy by conventional procedures. In general, the tegument of C. cellulosae showed the basic ultrastructure of cestode tegument on electron micrographs. The teguments of both scolex and bladder portions consisted of such components, i.e., an outer vesicular layer with numerous microtriches and inner filroug layer. Below the fibrous layer, there were layers of muscle bundles and tegumental cells. The microtriches which covered the surface of cysticercus revealed two distinctly different shapes. The characteristic bladder-like, elongated pyramid shaped "tetrahedrial form" was observed on the surface of the scolex portion, whereas the elongated cylindrical "filamentous form" was distributed on the stirface of bladder portion. In spite of the difference of isolated host and location, the cysticerci showed tole same result. But dimensional variations of the tegument according to topography of the worm were observed. The possibility of application in making differential diagnosis from other larval cestodes and possible functions of this larval tegument were discussed.

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Occurrence of Tomato spotted wilt virus in Chrysanthemum (Dendranthema grandiflorum) in Korea

  • Chung Bong-Nam;Pak Ha-Seung;Jung Jae-A;Kim Jeong-Soo
    • The Plant Pathology Journal
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    • 제22권3호
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    • pp.230-234
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    • 2006
  • Tomato spotted wilt virus (TSWV) has been identified in commercial chrysanthemum cultivars in Korea. Nucleotide sequences of the N gene of TSWV-ch14 isolated from infected chrysanthemum were determined and deposited in GenBank under accession no. DQ453158. The symptoms consisted of dark colored leaf necrosis, black streaks along the stem, wilting of plant parts in 'Sinma'; and chlorotic spots, necrosis of axillary shoots and withering of leaves in 'Hwarang'. Electron micrographs of leaf preparation of Nicotiana rustica infected with TSWV-ch14 contained spherical particles around 85 nm in diameter. TSWV was identified from chrysanthemum by sequence determination of N nucleocapsid protein and virion observation by transmission electron microscope. This is the first reported observation on TSWV in chrysanthemum in Korea.

지류문화재 보존수리에 있어서 한지의 섬유 배향성 분석 연구 (The Study of Hanji and Washi Fiber Orientation using Image analysis)

  • 한윤희;송정주
    • 한국문화재보존과학회:학술대회논문집
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    • 한국문화재보존과학회 2006년도 제24회 학술대회발표 논문집
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    • pp.11-15
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    • 2006
  • This work aims to clarify the character and selection of repair papers, based on fibre orientation information of paper cultural properties under restoration; using nondestructive image analysis applied to micrographs of paper surfaces. Image analysis using fast Fourier transform with suitable modifications was demonstrated to be an effective means to determine angle and intensity of fiber orientation as a nondestructive method. In the case of contemporary repair papers, the Japanese handmade paper exhibited a high anisotropy value, while the Korean handmade papers exhibited low anisotropy values. Korea and Japanese traditional hand making papers were well distinguished. Korea and Japanese papers made in the traditional ways showed its own characteristic orientation behavior in accordance with the motion of a bamboo wire.

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전자부품용 메탈라이즈드 알루미나 세라믹스의 미세구조 제어 (Microsturcture Control of Metallized Alumina Ceramics for Electronic Devices)

  • 조범래
    • 한국재료학회지
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    • 제11권12호
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    • pp.1086-1090
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    • 2001
  • Composition effects on microstructure and metallizing properties of the alumina sintered body were evaluated to develop the metallized alumina tubes having superior properties for electronic devices. SEM observation revealed that resultant micrographs and fractographs were varied with composition chance of additives and $SiO_2$-rich specimens showed better microstructural characteristics with uniform distribution of fine and round particles than other CaO-rich or MgO-rich ones. The resultant interfacial microstructure of the $SiO_2$-rich metallized alumina tubes also showed good metallizing properties with no defects between layers and uniform thickness of metallizing layer.

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(Co-Cr)-P-Ni 합금 박막의 자기적 특성 (Magnetic Properties of (Co-Cr)-P-Ni Alloy Thin Film)

  • 박창민;신경호;손홍균;이택동
    • 한국자기학회지
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    • 제5권2호
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    • pp.134-139
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    • 1995
  • DC magnetron 스파터링 방법으로 $(Co_{93}Cr_{7})-P-Ni$ 계 수평 자기 기록용 박막을 제조하였다. $(Co_{93}Cr_{7})-P-Ni$ 의사 삼원계(pseudo-ternary) 박막의 Ni 및 P의 함량 변황 따른 자기적 특성의 변화를 조사하였다. 박막의 조성을 조절함으로써 최대 1500 Oe의 보자력을 얻을 수 있었다. P 첨가에 따른 보자력 향상의 원인으로는 면내 이방성(in-plane anisotropy) 향상, 입자 크기의 변화, P 성분의 입계편석에 따른 입자간의 decoupling 등을 들 수 있다. 또한 TEM으로 미세 구조를 관찰한 결과 P 가 첨가되면 입자의 크기가 작아지면서 입자간의 자기적 decoupling이 일어남을 알 수 있었다.

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미끄럼 마찰하에서의 베어링간의 마모 diagram과 마모기구 (Wear diagram and Wear Mechanisms of Bearing Steel in Frictional Sliding)

  • 임대순;박성길;조성재;방건웅;문한규
    • Tribology and Lubricants
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    • 제6권1호
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    • pp.108-115
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    • 1990
  • Wear diagrams, which are the three dimensional representations of the dependence of the wear rate on the applied pressure and the sliding speed, were constructed with the pin on ring type wear test results using 52100 wear couples. The pressure and speed ranges from 0.45 MPa to 45.30 MPa and from 0.012 m/sec to 0.12 (0.120)m/sec, respectively. The results show the mild to severe transition, which suggests the change of the wear mechanisms as a function of the pressure and sliding speed. The SEM micrographs of the corresponding worn area shows clearly that different wear mechanisms dominate.

구상흑연주철재의 마멸-부식특성에 미치는 pH의 영향 (The Effect on the Wear-Corrosion Behavior of Ductile Cast Iron in the Various pH Environments)

  • 임우조;박동기
    • Tribology and Lubricants
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    • 제19권1호
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    • pp.31-35
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    • 2003
  • This paper reports the studies on the wear-corrosion behavior of ductile cast iron in the various pH environments. In the variety of pH solutions, corrosion and wear-corrosion loss of GCD 600 were investigated. Also, the anodic polarization test of GCD 600 using potentiostat/galvanostat was carried out. And rubbed surface of GCD 60 using scanning electron micrographs after immersion and wear-corrosion test was examined in the environment of various pH values. The main results are as following In alkali zone, the wear-corrosion loss of GCD 600 increases, but corrosion loss decreases. The unevenness and crack of wear-corrosion surface in neutral zone becomes duller than that in alkali zone. As the corrosive environment is acidified, wear-corrosion behavior of GCD 600 with passing immersion time becomes sensitive.

Preparation of Silver Nanoparticles in Ultrasonic Vibration-Induced Nanodroplets of Isopropyl Alcohol in Combination with Ionic Liquids

  • Shin, Ueon-Sang;Hong, Hyun-Ki;Kim, Hae-Won;Gong, Myoung-Seon
    • Bulletin of the Korean Chemical Society
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    • 제32권5호
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    • pp.1583-1586
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    • 2011
  • Silver nanoparticles (<10 nm) were prepared in ultrasonic vibration-induced nanodroplets of isopropyl alcohol (IPA) in combination with hydrophobic room temperature ionic liquids (RTILs). The Ag-precursor used were silver (I) complex, Ag$_2$(ehac)$_2$(eha)$_2$ (ehac = 2-ethylhexylammonium carbamate; eha = 2-ethylhexylamine), in IPA, while 1-butyl-3-methylimidazolium-based ionic liquids bearing $SbF_6^-$, $PF_6^-$ and $NTf_2^-$ as counter anions were used as RTILs. During sonication for 10-90 min at room temperature, uniform silver nanoparticles with mean sizes of 2 to 8 nm were rapidly synthesized. Transmission electron micrographs also confirmed that silver nanoparticles have a spherical shape and diverse sizes depending on the reaction time (10-90 min).