• 열처리공학회지
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• 제26권6호
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• pp.306-316
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• 2013

Microstructure and fracture behavior of a multi-phase low-density steel were investigated. After hot-rolling and heat treatment, the microstructure of low-density steel was composed of coarse ferrite grains and elongated bands which include second phases such as austenite, martensite and ${\kappa}$-carbide depending on holding time during isothermal heat treatment. After tensile test, microcracks were observed at martensite or ${\kappa}$-carbide interface in the elongated bands. Coarse ferrite grains showed cleavage fracture behavior regardless of second phase. The cleavage fracture of ferrite could be attributed to their coarse grain size and solute atoms that increase ductile-to-brittle transition temperature of ferrite. Despite of the tendency of cleavage fracture in coarse ferrite grains, a specimen having coarse spheroidized ${\kappa}$-carbide particles in the elongated bands showed high total elongation of 30%. Thus, the easiness of plastic deformation in the elongated band seems to play an important role in retardation of cleavage crack formation in coarse ferrite grains.

• 지질공학
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• 제4권2호
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• pp.231-243
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• 1994

응력하에서 암석 및 암반의 변형특성의 원인이되는 손상발달에 대한 이해는 지질공학 및 토목공학에 있어서 매우 중요하다. 지금까지의 연구에서 본면 실험전과 후의 관찰로서 응력하의 미소손상발달에 대한 연구는 아직 미미한 실절이다. 그러므로 응력하에서 손상과 정을 직접 관찰하는 것은 매우 중요하다. 본 연구에서는 응력하 중립질 화강암의 미소손상에 대한 보다 정확한 이해를 위해 미소손상집중, 발생 및 진전등에 석영과 장석의 접촉면에서 새로이 개발한 실험장치에의해 상세히 관찰되었다. 그 결과 두입자의 elastic mismatch 와 Hertzian fracture mechanice에 의해 잘 설명된다.

• 지질공학
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• 제4권2호
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• pp.139-151
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• 1994

암반은 서로 다른 입자 및 미소크랙과 같은 미소구조의 개별요소로 구성되어 있다. 이러한 미소구조에 대한 연구는 대심도 지하공간개발과 관련된 지질공학 및 토목공학분야등에 있어서의 관심이 증대되고 있다. 따라서, 단순한 연속체역학에 의한 접근보다는 구성입자들에 대한 역학적성질 및 개별구조요소등이 고려되어야 할 것이다. 그러나, 단순한 유크리드 공간에서 아들 구조를 표현하기는 매우 어렵다. 그래서 Mandelbrot에 의해 자연에 있어서 규칙성이 거의 없는 물체를 정량적으로 표현하기위한 Fractal이론이 개발되었다. 본 연구에는, 크랙의 진전과 응력의 관계를 평가하기위해 미소구조의 기하학적 성질이 Fractal차원에 의해 계산되었다. 암반의 역학적 성질을 평가함에 있어 그 구조의 복잡성을 Fractal이론에 의해 단순화 및 수치화시켜 균질화이론에 적용시키므로서 그 평가를 보다 용이하고 효과적으로 할 수 있다.

• 한국세라믹학회지
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• 제31권9호
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• pp.1037-1043
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• 1994

The effects of annealing atmosphere and temperature on piezoelectricity (k33) and the mechanical strength of machined PZT was studied. Morphotropic Nb-doped PZT was sintered, machined to a rod and then annealed between 80$0^{\circ}C$ and 100$0^{\circ}C$ in air, PbZrO3, and CuO atmospheres respectively. In air or PbZrO3 atmosphere, the compressive strength of Nb-doped PZT increased by 12% with little change in k33 irrespective of annealing temperature. In CuO atmosphere, on the other hand, the compressive strength increased by 20% with little change in k33 at 80$0^{\circ}C$ but both turned to significant decrease above 90$0^{\circ}C$. The examination of the phase distribution and microstructure beneath the surface of CuO-treated PZT revealed that the changes in compressive strength and k33 are closely related to the reaction between PZT and vaporized CuO:liquid PbO precipitated in shallow surface region by the substitution of Cu to Pb sites enhances the decrease in microcracks and the surface roughness at 80$0^{\circ}C$ ; rapid evaporation of precipitated PbO expands a porous region of changed composition into the bulk above 90$0^{\circ}C$.

• Journal of Electrical Engineering and information Science
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• 제2권3호
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• pp.71-76
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• 1997

A lot of experiments and analyses have been done to determine the aging mechanism of mica-epoxy composite material used for large generator stator windings in order to estimate remaining life of the generator for last decades. After degrading artificially the mica-epoxy composite material, the surface analysis is performed to analyze breakdown mechanism of insulation in air and hydrogen atmosphere; i) In the case of air atmosphere, it is observed that an aging propagation from conductor to core by partial discharge effect and the formation of cracks between layers is widely carbonized surface. ii) In case of hydrogen atmosphere, the partial discharge effect is reduced by the hydrogen pressure (4kg/$\textrm{cm}^2$). Potassium ions forming a sheet of mica is replaced by hydrogen ions, which can lead to microcracks. It is confirmed that the sizes of crack by SEM analysis are 10∼20[$\mu\textrm{m}$] in length under air, and 1∼5[$\mu\textrm{m}$] in diameter, 10∼50[$\mu\textrm{m}$] in length under hydrogen atmosphere respectively. The breakdown mechanism of sttor winding insulation materials which are composed of mica-epoxy is analyzed by the component of materials with EDS, SEM techniques. We concluded that the postassium ions of mica components are replaced by H\ulcorner, H$_3$O\ulcorner at boundary area of mica-epoxy and/or mica-mica. It is proposed that through these phenomena, the conductive layers of potassium enable creation of voids and cracks due to thermal, mechanical, electrical and environmental stresses.

• 동력기계공학회지
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• 제4권4호
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• pp.48-53
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• 2000

This study was aimed at observing the influence of laser irradiation on a $ZrO_2-8%Y_2O_3$ ceramic coating layer fabricated by plasma spraying. The $ZrO_2-8%Y_2O_3$ ceramic powder was plasma sprayed onto SS400 carbon steel substrate and laser irradiated on the coating layer under various conditions of laser power and beam diameters. As to the as-sprayed specimen and laser-treated specimen, a hardness test and a microstructure analysis were performed. Hardness was measured by a microhardness tester; microstructure was observed by an optical microscope and a scanning electron microscope. The result was that the microstructure of the laser-irradiated coating layer was dense; porosities almost disappeared and hardness increased. It was also observed that microcracks occured in the laser-irradiated coating layer.

• 한국재료학회지
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• 제13권4호
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• pp.213-218
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• 2003

Fibrous monolithic control of$ Al_2$$O_3$ -$ZrO_2$composite was investigated by multi-pass extrusion process. To obtain sound $Al_2$$O_3$-X $O_2$sintered bodies, burning out and sintering process were carefully carried out. The sintered bodies showed continuous, fibrous monolithic microstructure without any swelling. Many microcracks were observed at the $Al_2$$O_3$-$ZrO_2$interfaces due to the mismatching of thermal expansion coefficient between $Al_2$$O_3$ and $ZrO_2$phase. Most of m- $ZrO_2$grains included twin defects such as (001), (010) and (011) type to accommodate the phase transformation induced stress.

• 한국재료학회지
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• 제23권10호
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• pp.574-579
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• 2013

The milling and particulate characteristics of Al alloy-$Al_2O_3$ powder mixtures for a reaction-bonded $Al_2O_3$ (RBAO) process were studied. A commercially available prealloyed Al powder with Zn, Mg, Cu and Cr alloying elements (7475 series) was mixed with a calcined sinter-active $Al_2O_3$ powder and then milled in centrifugal milling equipment for ~48 hrs. The Al alloy-$Al_2O_3$ powder mixtures after milling were characterized and evaluated in various ways to reveal their particulate characteristics during milling. The milling efficiency of the Al alloy increased with a longer milling time. Comminution of the Al alloy particles started with its elongation, showing a high aspect ratio. With a longer milling time, the elongated Al alloy particle changed in terms of its shape and size, becoming equiaxially fine particles. Regardless of the milling efficiency of the Al alloy particles, all of the Al alloy particles repeatedly experienced strong plastic deformation during milling, giving rise to higher density of surface defects, such as microcracks, and leading to higher residual microstress within the Al alloy particles. The chemical reactions, oxidation behavior and hydration behavior of the Al alloy particles and the hydrolysis characteristics of their reaction with the environment were also observed during the milling process and during the subsequent powder handling steps.

• 한국분말재료학회지
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• 제10권3호
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• pp.195-200
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• 2003

Ni coated $Al_2O_3$ composite was successfully Prepared by the electroless deposition Process. The average size of Ni particles coated on the $Al_2O_3$ matrix powder was about 20 nm. It was hard to find any reaction compound as an impurity at interface between $Al_2O_3$ and Ni particles after sintering. The characterization of microstructure crystal structure and fracture behavior of the sintered body were investigated using XRD, TEM and Victors hardness tester, and compared with those of the sintered $Al_2O_3$ monolithic body. Many dislocations were observed in the Ni phase due to the difference of thermal expansion coefficient between $Al_2O_3$ and Ni phase, and no observed microcracks at their $Al_2O_3$ and Ni interface. In the $Al_2O_3$/Ni composite, the main fracture mode showed a mixed fracture with intergranular and transgranuluar type having some ,surface roughness. The fracture toughness was slightly increased due to the plastic deformation mechanism of Ni phase in the $Al_2O_3$/Ni composite.

• 산업기술연구
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• 제20권B호
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• pp.87-94
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• 2000

A study has been made on the behavior of microscopic fatigue crack growth at the stress level of the fatigue limit with ferrite-martensitic structures. For the above purpose, two types of the microstructures were prepared ; one is the microstructure having the ferrite encapsulating the islands of second phase martensite(FEM), the other is the microstructure with the martensite encapsulating the islands of ferrite(MEF). It has been pointed out that the fatigue limits of these microstructures are related to the critical stress at which the microcrack in the ferrite proceeds to the martensite. The high fatigue limit might be excepted for the MEF microstructure in which the critical crack length would be restricted within the second phase spacing in contrast with the FEM microstruture. However, the fatigue tests shows that no appreciable difference of the fatigue limits among them were recognized. Also, it turned out from the metallographic observations that the micro crack path is very much affected by the microstructures, so that the microcracks grow according to the 3-dimentional situation of its microstructures.