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TEM Microstructure of Al2O3/Ni Nanocomposites by Electroless Deposition

무전해코팅법으로 제조한 Al2O3/Ni 나노 Composite의 TEM 미세조직

  • 한재길 (공주대학교 공과대학 신소재공학부, 충남나노연구센터) ;
  • 이재영 (공주대학교 공과대학 신소재공학부, 충남나노연구센터) ;
  • 김택수 (공주대학교 공과대학 신소재공학부, 충남나노연구센터) ;
  • 이병택 (공주대학교 공과대학 신소재공학부, 충남나노연구센터)
  • Published : 2003.06.01

Abstract

Ni coated $Al_2O_3$ composite was successfully Prepared by the electroless deposition Process. The average size of Ni particles coated on the $Al_2O_3$ matrix powder was about 20 nm. It was hard to find any reaction compound as an impurity at interface between $Al_2O_3$ and Ni particles after sintering. The characterization of microstructure crystal structure and fracture behavior of the sintered body were investigated using XRD, TEM and Victors hardness tester, and compared with those of the sintered $Al_2O_3$ monolithic body. Many dislocations were observed in the Ni phase due to the difference of thermal expansion coefficient between $Al_2O_3$ and Ni phase, and no observed microcracks at their $Al_2O_3$ and Ni interface. In the $Al_2O_3$/Ni composite, the main fracture mode showed a mixed fracture with intergranular and transgranuluar type having some ,surface roughness. The fracture toughness was slightly increased due to the plastic deformation mechanism of Ni phase in the $Al_2O_3$/Ni composite.

Keywords

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