• 한국정밀공학회지
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• 제23권8호
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• pp.100-107
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• 2006

The objective of this research is to investigate the electromagnetic interference(EMI) shielding characteristics of fiber reinforced composites. We fabricated glass and carbon fiber reinforced composites filled with metal powder and nano carbon black. The measurements of shielding effectiveness(SE) were carried out frequency range 300MHz - 1GHz for commercial purposes such as electric or telecommunication devices. The return loss and loss due to absorption were also measured as a function of frequency in the micro wave(300MHz-1GHz) region. It is observed that the SE of the composites is the frequency dependent, increase with the increases in filler loading. The Mg metal powder filled composite showed higher SE compared to that of carbon black. The Mg metal powder/epoxy composite was shown to exhibit up to 40dB of SE. The results indicates that the composite having higher filler loading can be used for the purpose of EMI shielding as well as for some microwave applications.

• 한국결정성장학회지
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• 제16권6호
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• pp.235-239
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• 2006

Micro-pulling down$({\mu}-PD)$법을 이용하여 직경 $0.8{\sim}1.0mm$, 길이 $30{\sim}35mm$의 ZnO가 첨가된 near-stoichiometric $LiNbO_3$, 단결정을 성장하였다. 성장된 결정의 결정구조를 powder x-tay diffraction(XRD) patterns으로 확인하였고, electron probe micro analysis(EPMA)를 이용하여 결정내 Zn 이온들이 균일하게 분포되었음을 확인하였다. 또한 2 mol% 이상의 ZnO 첨가시 $OH^-$ 흡수밴드의 특성이 크게 변화함을 관찰함으로써 ZnO 첨가량에 일치한 역치(threshold)가 존재함을 확인하였다.

• 한국건축시공학회지
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• 제17권1호
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• pp.111-117
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• 2017

Stone powder sludge is a byproduct of the crushed aggregate industry, and most of it is dumped with soil in landfills. The disposal of stone powder sludge presents a major environmental problem. This paper investigates the effects of stone powder sludge on the fluidity, density, strength and micro-structure properties of AAC(autoclaved aerated concrete) samples. Stone powder sludge was obtained from a crushed aggregate factory in order to investigate its applicability as a substitute for quartz sand in AAC. To determine the properties of the AAC samples produced with stone powder sludge, specimens containing different foam ratios were produced. Flow value, density, compressive strength, tensile strength and flexural strength of the samples were tested, and X-ray diffraction (XRD) was performed. The test results indicated that the compressive strength of AAC specimens (F120) with stone powder sludge was higher than that of AAC specimens (Q120) with quartz sand for same foam ratio of 120%. For all XRD diagrams, a higher number of tobermorite peaks was shown for the F120 sample than for the Q120 sample, which may explain the slightly higher strength gain in the F120 sample.

• 한국정밀공학회지
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• 제21권6호
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• pp.28-34
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• 2004

The old technique of sandblasting which has been used for decoration of glass surface has recently been developed into a powder blasting technique for brittle materials such as glass, silicon and ceramics, capable of producing micro structures larger than 100${\mu}{\textrm}{m}$. In this study, we introduced oblique powder blasting, and investigated the effect of the impacting angle of particles, the scanning times and the stand-off distance on the surface roughness and the weight-loss rate of samples with no mask, and the wall profile and overetching of samples with different mask pattern in powder blasting of soda-lime glass. The varying parameters were the different impact angles between 50$^{\circ}$ and 90$^{\circ}$, scanning times of nozzle up to 40 and the stand-off distances 70mm and 100mm. The widths of mask pattern were 0.2mm, 0.5mm and 1mm. The powder was alumina sharp particles, WA #600. The mass flow rate of powder during the erosion test was fixed constant at 175g/min and the blasting pressure of powder at 0.2Mpa.

• Advances in concrete construction
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• 제13권3호
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• pp.215-221
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• 2022

Considering their similar mass densities, an attempt was made to optimize the mix design of micro-concrete that used barite sand as an aggregate by substituting marble powder (5%, 10%, 20%, 30%, 40%, 50%, 70%), clay brick powder (30%, 50%, 70%), and fly ash (30%, 50%, 70%) for the concrete (by mass) to form specimens for shaking table tests. The test results showed that for these three groups of materials, the substitutions had little effect on the density. The barite sand played a decisive role in the density, and the overall density of the specimens reached approximately 2.9 g/cm³. The compressive strength and elastic modulus decreased with an increase in the substitution rates for the three types of materials. Among them, the 28 day compressive strength values of the 40% and 50% marble powder groups were 11.73 MPa and 8.33 MPa, respectively, which were 58.7% and 70.7% lower than the control group, respectively. Their elastic modulus values were 1.33×10⁴ MPa and 1.42×10⁴ MPa, respectively, which were 39.1% and 35% lower than those of the control group, respectively. The 28 day compressive strength values of the 50% and 70% clay brick powder groups were 13.13 MPa and 5.8 MPa, respectively, which were 53.8% and 79.6% lower than the control group, respectively. Their elastic modulus values were 1.54×10⁴ MPa and 1.19×10⁴ MPa, respectively, which were 29.7% and 45.4% lower than those of the control group, respectively. The 28 day compressive strength values of the 50% and 70% fly ash groups were 13.5 MPa and 7.1 MPa, respectively, which were 52.5% and 75% lower than those of the control group, respectively. Their elastic modulus values were 1.36×10⁴ MPa and 0.95×10⁴ MPa, respectively, which were 37.9% and 56.6% lower than those of the control group, respectively. There was a linear relationship between the 28 day compressive strength and elastic modulus, with the correlation coefficient reaching a value higher than 0.88. The test results showed that the model materials met the high density, low compressive strength, and low elastic modulus requirements for shaking table tests, and the test data of the three groups of different alternative materials were compared and analyzed to provide references and assistance for relevant model testers.

• 한국분말재료학회지
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• 제22권3호
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• pp.163-168
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• 2015

Ti alloys are extensively used in high-technology application because of their strength, oxidation resistance at high temperature. However, Ti alloys tend to be classified very difficult to cut material. In this paper, The powder synthesis, spark plasma sintering (SPS), bulk material properties such as electrical conductivity and thermal conductivity are systematically examined on $Ti_2AlN$ and $Ti_2AlC$ materials having most light-weight and oxidation resistance among the MAX phases. The bulk samples mainly consisted of $Ti_2AlN$ and $Ti_2AlC$ materials with density close to theoretical value were synthesized by a SPS method. Machining characteristics such as machining time, surface quality are analyzed with measurement of voltage and current waveform according to machining condition of micro-electrical discharge machining with micro-channel shape.

• 한국분말재료학회지
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• 제14권6호
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• pp.354-361
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• 2007

The bi-materials with Al-Mg alloy and its composites reinforced with SiC and $Al_2O_3$ particles were prepared by conventional powder metallurgy method. The A1-5 wt%Mg and composite mixtures were compacted under $150{\sim}450\;MPa$, and then the mixtures compacted under 400 MPa were sintered at $773{\sim}1173K$ for 5h. The obtained bi-materials with Al-Mg/SiCp composite showed the higher relative density than those with $Al-Mg/Al_2O_3$ composite after compaction and sintering. Based on the results, the bi-materials compacted under 400 MPa and sintered at 873K for 5h were used for mechanical tests. In the composite side of bi-materials, the SiC particles were densely distributed compared to the $Al_2O_3$ particles. The bi-materials with Al-Mg/SiC composite showed the higher micro-hardness than those with $Al-Mg/Al_2O_3$ composite. The mechanical properties were evaluated by the compressive test. The bi-materials revealed almost the same value of 0.2% proof stress with Al-Mg alloy. Their compressive strength was lower than that of Al-Mg alloy. Moreover, impact absorbed energy of bi-materials was smaller than that of composite. However, the bi-materials with Al-Mg/SiCp composite particularly showed almost similar impact absorbed energy to $Al-Mg/Al_2O_3$ composite. From the observation of microstructure, it was deduced that the bi-materials was preferentially fractured through micro-interface between matrix and composite in the vicinity of macro-interface.

• 한국구조물진단유지관리공학회 논문집
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• 제19권3호
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• pp.22-29
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• 2015

본 연구에서는 압축강도 24MPa 이상 열전도율이 기존 콘크리트보다 2배 감소된 구조용 단열성능 향상 콘크리트를 개발하고 현장적용하기 위한 실험을 진행하였다. 슬럼프 및 공기량 시험결과 Plain과 규조토 미분말을 사용한 배합은 경과시간에 따라 슬럼프와 공기량 저하가 나타났으며, 마이크로기포제를 사용한 배합은 슬럼프와 공기량 저하가 나타나지 않았다. 또한 단열성능 향상 재료를 사용한 배합의 단위용적질량은 Plain 대비 감소하였다. 압축강도는 단열성능 향상 콘크리트가 Plain보다 감소한 결과를 나타내었으나 목표강도 24MPa를 만족하였으며, 열전도율은 Plain보다 감소하는 경향을 보였다. 단열성능 향상 콘크리트의 동결융해 저항성은 Plain과 유사하였고, 중성화 저항성은 규조토 미분말을 사용한 배합이 재령 4주에 Plain과 유사했으며, 마이크로기포제를 사용한 배합은 Plain보다 중성화 저항성이 저하되었고, 길이변화율은 Plain보다 전체적으로 증가되었다.

• 한국분말재료학회지
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• 제24권3호
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• pp.223-228
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• 2017

Nanopowders provide better details for micro features and surface finish in powder injection molding processes. However, the small size of such powders induces processing challenges, such as low solid loading, high feedstock viscosity, difficulty in debinding, and distinctive sintering behavior. Therefore, the optimization of process conditions for nanopowder injection molding is essential, and it should be carefully performed. In this study, the powder injection molding process for Fe nanopowder has been optimized. The feedstock has been formulated using commercially available Fe nanopowder and a wax-based binder system. The optimal solid loading has been determined from the critical solid loading, measured by a torque rheometer. The homogeneously mixed feedstock is injected as a cylindrical green body, and solvent and thermal debinding conditions are determined by observing the weight change of the sample. The influence of the sintering temperature and holding time on the density has also been investigated. Thereafter, the Vickers hardness and grain size of the sintered samples have been measured to optimize the sintering conditions.

• 한국분말재료학회지
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• 제6권1호
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• pp.88-95
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• 1999

The purpose of this study is to investigate the manufacturing feasibility of WC-Co milling inserts via Powder Injection Molding (PIM) process. WC-Co is used in a wide variety of cutting tools due to its high hardness, stiffness, compressive strength and wear resistance properties. WC-Co parts for a high stress application were conventionally produced by the press and sinter method, which were Iimited to 2 dimensional shapes. Manufacturing WC-Co parts for a high stress application by PIM implies that tool efficiency can be highly improved due to increased freedom is design. P30 grade WC powder (WC-Co-TiC-TaC system) was mixed with RIST-5B133 binder and injection molded into milling inserts (Taegu Tech. Model WCMX 06T 308). The mean grain size of the powder was about 0.8$\mu$m. Injection molded specimens were debound by solvent extraction and thermal degradation method at various conditions. The specimens were sintered at 140$0^{\circ}C$ for 1 hr in vacuum. Carbon content, weight loss, dimensional change, and macro defects of the specimen were carefully monitored at each stage of the PIM process. PIMed WC-Co milling inserts reached 100% full density after sinteing. Its mechanical properties and micro-structures were comparable with the press and sintered milling insert. Carbon content of the sintered WC-Co insert was mainly determained by the atmosphere of thermal debinding. By controlling powder loading and injection molding condition, dimensional accuracy could be obtained within 0.4%. We confirm that PIM can not only be an alternative manufacturing method for WC-Co parts economically but also provide a design freedom for more effieient cutting tools.