• 한국표면공학회지
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• 제54권5호
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• pp.267-277
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• 2021

Nitriding layers developed during gaseous nitriding of AISI4115 steels for the application of steel bushing part were investigated. The compound layer thickness of about 10㎛, 0.3mm of case depth under the same conditions, and conventional nitriding, nitrocarburizing, and controlled nitriding were performed in three methods. In the controlled nitriding, K_N was controlled by measuring the hydrogen partial pressure. The nitrided samples were analyzed by micro Vickers hardness test, optical microscopy and scanning electron microscopy. The phases of compound layer were identified by X-ray diffraction and electron backscatter diffraction. The controlled nitriding specimen indicated the highest surface hardness of about 860 HV_0.1. The compound layer of the conventional nitriding and nitrocarburizing specimen was formed with about 46% porous layer and 𝜺 + 𝜸' phase, and about 13% porous layer and about 80% 𝜸' phase were formed on the controlled nitriding specimen. As a result of the Ball-on-disk wear test, the worn mass loss of ball performed on the surface of the controlled nitriding specimen was the largest. The controlled nitriding specimen had the highest surface hardness due to the lowest porous percentage of compound layer, which improved the wear resistance.

• 한국산학기술학회논문지
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• 제17권11호
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• pp.42-50
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• 2016

오버레이 용접은 희석율에 의해 적층 두께에 따라 화학성분 함량과 용접부의 경도에 영향을 미치며 이는 파이프 제품의 표면성질을 결정한다. 이로 인해 오버레이 용접은 적층의 수를 고려하여야 한다. 본 연구에서는 탄소강 모재에 내부식성 소재인 모넬 소재를 오버레이 용접하여 적층수에 따른 Fe함량, 모재와 모넬 소재와의 용접성, 부위별 경도와 표면 평탄도를 실험적으로 연구하였다. 각각의 평가는 평판의 모재와 파이프 모재에 3개의 층으로 오버레이 용접 후 실시하였다. Fe함량은 각 층별 시료를 채취하여 성분 분석을 통해 평가하였으며, 3Layer에서 만족하는 함량을 나타내었다. 또한 적층별 시편을 밴딩 시험하여 용접성을 평가하였다. 적층별 경도와 비드 평탄도는 Micro Vickers와 3차원 측정을 통해 평가하였다. 경도는 1Layer에서 발생하는 HAZ부에 의해 가장 높은 경도 값을 보였으며, 적층이 증가할수록 경도가 감소하였다. 비드 평탄도의 경우 적층수 증가에 따라 편차가 급격한 차이가 발생하였으며, 이는 경도와 함께 사용 목적의 측면에서 주의 깊게 고려해야 한다. 이러한 실험적 결과는 목적에 따른 용접 파이프 적층수의 결정 방법을 나타내었다.

• 대한금속재료학회지
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• 제49권8호
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• pp.628-634
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• 2011

SA508 Gr.4N Ni-Cr-Mo low alloy steel, in which Ni and Cr contents are higher than in commercial SA508 Gr.3 Mn-Mo-Ni low alloy steels, may be a candidate reactor pressure vessel (RPV) material with higher strength and toughness from its tempered martensitic microstructure. The inner surface of the RPV is weld-cladded with stainless steels to prevent corrosion. The goal of this study is to evaluate the microstructural properties of the clad interface between Ni-Cr-Mo low alloy steel and stainless weldment, and the effects of post weld heat treatment (PWHT) on the properties. The properties of the clad interface were compared with those of commercial Mn-Mo-Ni low alloy steel. Multi-layer welding of model alloys with ER308L and ER309L stainless steel by the SAW method was performed, and then PWHT was conducted at $610^{\circ}C$ for 30 h. The microstructural changes of the clad interface were analyzed using OM, SEM and TEM, and micro-Vickers hardness tests were performed. Before PWHT, the heat affected zone (HAZ) showed higher hardness than base and weld metals due to formation of martensite after welding in both steels. In addition, the hardness of the HAZ in Ni-Cr-Mo low alloy steel was higher than that in Mn-Mo-Ni low alloy steel due to a comparatively high martensite fraction. The hardness of the HAZ decreased after PWHT in both steels, but the dark region was formed near the fusion line in which the hardness was locally high. In the case of Mn-Mo-Ni low alloy steel, formation of fine Cr-carbides in the weld region near the fusion line by diffusion of C from the base metal resulted in locally high hardness in the dark region. However, the precipitates of the region in the Ni-Cr-Mo low alloy steel were similar to that in the base metal, and the hardness in the region was not greatly different from that in the base metal.

• 대한치과기공학회지
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• 제39권2호
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• pp.75-82
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• 2017

Purpose: This study provided the basic data for selection the zirconia block and CAM by means of marginal fitness observations, flexural strength test and hardness test. Methods: Three dental zirconia blocks(ABCera, NaturaZ, ST98) and two dental milling machines(CAD/CAM MS, DWX-50) were used in this study. Metal abutment(diameter 10 mm, height 5 mm, inclined angle $3^{\circ}$ taper, 1 mm chamfer margin) was fabricated by Ti customized abutment, and then zirconia copings were fabricated for each ten specimens. Silicone replica technique was used to observe the marginal fitness of cross-sections with a stereomicroscope at ${\times}50$ magnification. The dental zirconia blocks was cut into 10 pieces each having a size of $25mm{\times}5mm{\times}1mm$, and fabricated according to the manufacturer's instructions, and flexural strength was measured using a universal testing machine. For hardness test, a micro Vickers hardness tester was used as it was in the flexural strength test. Statistical analysis was performed by one way ANOVA and post-test was performed by Scheffe test. Results: For marginal fitness of bucco-lingual axial, ZU group($59.7{\pm}10.3{\mu}m$) was the lowest, followed by RA, ZA, ZD, RD, RU. For marginal fitness of mesio-distal axial, ZU group($59.3{\pm}10.2{\mu}m$) was the lowest, followed by RA, ZA, RD, ZD, RU. One-way ANOVA showed statistically significant difference between groups(p<0.05). For flexural strength, ABCera block($718.0{\pm}57.2MPa$) was the highest, followed by NaturaZ, ST98. For hardness, ABCera block($1550.3{\pm}19.8Hv$) was the highest, followed by ST98, NaturaZ. There was no significant difference in flexural strength and hardness between blocks(p>0.05). Conclusion: Based on the results of this study, the type of dental zirconia block did influence the marginal fitness, and all dental zirconia blocks are expected to be suitable for clinical application. The highest flexural strength and hardness were ABCera block, and no statistically significant difference was observed.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2007년도 춘계학술대회 논문집
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• pp.421-424
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• 2007

Dry sliding wear behavior of ultra-fine grained (UFG) plain low carbon dual phase steel, of which microstructure consists of hard martensite in a ductile ferrite matrix, has been investigated. The wear characteristics of the UFG dual phase steel was compared with that of a coarse grained dual phase steel under various applied load conditions. Dry sliding wear test were carried out using a pin-on-disk type tester at various loads of 1N to 100N under a constant sliding speed condition of 0.20m/s against an AISI 52100 bearing steel ball at room temperature. The sliding distance was fixed as 1000m for all wear tests. The wear rate was calculated by dividing the weight loss, measured to the accuracy of 10-5g by the specific gravity and sliding distance. The worn surfaces and wear debris were analyzed by SEM, EDS and profilometer. Micro-vickers hardness of the cross section of worn surfaces were conducted to analyze strain hardening underneath the contact surfaces. The wear mechanism of the UFG dual phase steel was investigated with emphasis on the unstable nature of the grain boundaries of the UFG microstructure.

• 한국주조공학회지
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• 제36권3호
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• pp.88-94
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• 2016

We investigated the effect of heat treatment on an ADC12 alloy produced using diecasting. The heat treatment used in this study was a typical T6 process: a solid solution treatment followed by an artificial aging treatment. As-cast specimens were solid-solution-treated at $500^{\circ}C$ and $530^{\circ}C$ for 1-16 hr, and aged at $160^{\circ}C$ and $180^{\circ}C$ for 1-8 hr. Microstructural changes in the alloy during the heat treatment were observed. Changes in mechanical properties of the alloy were measured using a micro-Vickers hardness tester. Finally, we determined the optimal heat treatment conditions for the diecast ADC12 alloy.

• 한국재료학회지
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• 제19권2호
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• pp.85-89
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• 2009

Nano-crystalline hydroxyapatite (HAp) films were formed at the Ti surface by a single-step microarc oxidation (MAO), and HAp-zirconia composite (HZC) films were obtained by subsequent chemical vapor deposition (CVD) of zirconia onto the HAp. Through the CVD process, zero- and one-dimensional zirconia nanostructures having tetragonal crystallinity (t-ZrO2) were uniformly distributed and well incorporated into the HAp crystal matrix to form nanoscale composites. In particular, (t-$ZrO_2$) was synthesized at a very low temperature. The HZC films did not show secondary phases such as tricalcium phosphate (TCP) and tetracalcium phosphate (TTCP) at relatively high temperatures. The most likely mechanism for the formation of the t-$ZrO_2$ and the pure HAp at the low processing temperature was proposed to be the diffusion of $Ca^{2+}$ ions. The HZC films showed increasing micro-Vickers hardness values with increases in the t-$ZrO_2$ content. The morphological features and phase compositions of the HZC films showed strong dependence on the time and temperature of the CVD process. Furthermore, they showed enhanced cell proliferation compared to the $TiO_2$ and HAp films most likely due to the surface structure change.

• 소성∙가공
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• 제17권7호
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• pp.523-527
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• 2008

In this study, mechanical properties of Alloy 718 welded after forgings for jet propulsion component was investigated. Hot-forged and machined work-pieces($230mm\times70mm\times15mm$) which have different grain sizes are welded by electron beam welding technique. After welding, the components were solution heat-treated and aged. Samples were sectioned to analyze the microstructural evolution and formation of micro-crack. It was found that HAZ grain boundary liquation crack generally initiates in the coarse grains rather than the fine grains. Needle-like phases with high Nb contents were found at the outer part near the base metal. Vickers hardness and tensile tests were carried out at room temperature and at $649^{\circ}C$. The tensile properties of electron beam welding specimens exhibited around 100MPa and 10% decrease in strength and elongation, respectively.

• 한국분말재료학회지
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• 제24권3호
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• pp.223-228
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• 2017

Nanopowders provide better details for micro features and surface finish in powder injection molding processes. However, the small size of such powders induces processing challenges, such as low solid loading, high feedstock viscosity, difficulty in debinding, and distinctive sintering behavior. Therefore, the optimization of process conditions for nanopowder injection molding is essential, and it should be carefully performed. In this study, the powder injection molding process for Fe nanopowder has been optimized. The feedstock has been formulated using commercially available Fe nanopowder and a wax-based binder system. The optimal solid loading has been determined from the critical solid loading, measured by a torque rheometer. The homogeneously mixed feedstock is injected as a cylindrical green body, and solvent and thermal debinding conditions are determined by observing the weight change of the sample. The influence of the sintering temperature and holding time on the density has also been investigated. Thereafter, the Vickers hardness and grain size of the sintered samples have been measured to optimize the sintering conditions.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2006년도 춘계학술대회 논문집
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• pp.149-152
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• 2006

Dry sliding wear behavior of low carbon dual phase steel, of which microstructure consists of hard martensite in a ductile ferrite matrix, has been investigated. The wear characteristics of the dual phase steel was compared with that of a plain carbon steel which was normalized at $950^{\circ}C$ for 30min and then air-cooled. Dry sliding wear tests were carried out using a pin-on-disk type tester at various loads of 1N to 10N under a constant sliding speed condition of 0.2m/sec against an AISI 52100 bearing steel ball at room temperature. The sliding distance was fixed as 1000m for all wear tests. The wear rate was calculated by dividing the weight loss measured to the accuracy of $10^{-5}g$ by the specific gravity and sliding distance. The worn surfaces and wear debris were analyzed by SEM, EDS and a profilomter. Micro vickers hardness values of the cross section of worn surface were measured to analyze strain hardening behavior underneath the wearing surfaces. The were rate of the dual phase steel was lower than the plain carbon steel. Oxidation on the sliding surface and strain hardening were attributed for the higher wear resistance of the dual phase steel.