• Journal of Korea Technical Association of The Pulp and Paper Industry
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• v.37 no.3
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• pp.1-8
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• 2005

Increase in the utilization rate of recycled paper and closing level of papermaking system increased the problem associated with stickies that include decrease in process runnability and product quality. It is required to establish a process for removing the micro stickies to solve the problems associated with stickies. In this study, the application of flotation process as a method to remove micro stickies was examined. Model micro stickies (MMS) were prepared using microcrystalline cellulose (MCC) and pressure sensitive adhesives (PSA), and the influence of three nonionic surfactants on the removal efficiency of MMS from flotation process was examined. Also the effect of surfactants on the deposition of micro stickies that remaining in the papermaking wet end onto wire was examined. Removal efficiency of MMS by flotation was increased when the proportion of nonionic surfactant with propylene oxide (PO) type hydrophilic tail was increased and stock pH was 7. It was suggested that this nonionic surfactant minimized the increase of surface energy of hydrophobic MMS. The MMS with high hydrophobicity remaining in the papermaking system, however, would cause more serious deposition problems on papermaking wet end. Therefore, it is of great importance to increase the removal efficiency of MMS in flotation process for the prevention of papermaking system contamination caused by stickies deposition.

• Journal of Korea Technical Association of The Pulp and Paper Industry
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• v.41 no.5
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• pp.26-32
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• 2009

As a part of utilizing the nanocellulose (NC) from lignocellulosic components of wood biomass, this paper reports preliminary results on the products of sulfuric acid hydrolysis. The purpose of this study was to investigate the morphology of both NC and micro-sized cellulose fiber (MCF) isolated by acid hydrolysis from commercial microcrystalline cellulose (MCC). Field emission.scanning electron microscopy (FE-SEM) and transmission electron microscopy (TEM) were employed to observe the acid hydrolysis suspension, NC, and MCF. The electron microscopy observations showed that the acid hydrolysis suspension, before separation into NC and MCF by centrifugation, was composed of nano-sized NCs and micro-sized MCFs. The morphology of isolated NCs was a whisker form of rod-like NCs. Measurements of individual NCs using TEM indicated dimensions of 6.96$\pm$0.87 nm wide by 178$\pm$55 nm long. Observations of the MCFs showed that most of the MCC particles had de-fibered into relatively long fibers with a diameter of 3-9 ${\mu}m$, depending on the degree of acid hydrolysis. These results suggest that proper technologies are required to effectively realize the potentials of both NCs and MCFs.

• Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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• 2007.11a
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• pp.21-33
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• 2007

CPAM has been applied to the paper industry for the purpose of wet-end improvement for a long time. And molecular weight and charge density have been managed most important quality factors to make CPAM for this application. Recently branched CPAM was developed to improve retention and drainage characteristics and we considered branch degree of CPAM as important factor as molecular weight and charge density. In this experiment, we tried to investigate physical and chemical properties to determine branch degree and flocculation efficiency using Arbocell pulp which was recently developed micro size pulp and finally we applied retention and drainage test under the ONP stock condition.

• Journal of Korea Technical Association of The Pulp and Paper Industry
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• v.47 no.6
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• pp.57-65
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• 2015

Microfibrillated cellulose (MFC) or Nanofibrillated cellulose (NFC) has been used to reduce the use of raw pulp and to improve paper strength. The problem of MFC preparation is high manufacturing cost. In this study, it was carried out to prepare MFC after enzyme beating and estimated properties of MFC. Endo-D was the best beating efficiency among three type of endo-glucanase. As the grinder pass number increased, the viscosity and the fines of MFC suspension increased while the crystallinity and the porosity of MFC sheet decreased. Also enzyme beating MFC was higher value in the crystallinity and lower value in the viscosity than non-enzyme MFC. In addition, the aspect ratio of MFC was the highest at 5 pass. MFC addition improved the handsheet strength and the air permeability but worsened the drainage.

• Journal of Korea Technical Association of The Pulp and Paper Industry
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• v.48 no.1
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• pp.5-18
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• 2016

Electron microscopy is an important investigation and analytical method for the morphological characterization of various cellulosic materials, such as micro-crystalline cellulose (MCC), microfibrillated cellulose (MFC), nanofibrillated cellulose (NFC), and cellulose nanocrystals (CNC). However, more accurate morphological analysis requires high-quality micrographs acquired from the proper use of an electron microscope and associated sample preparation methods. Understanding the interaction of electron and matter as well as the importance of sample preparation methods, including drying and staining methods, enables the production of high quality images with adequate information on the nanocellulosic materials. This paper provides a brief overview of the micro and nano structural analysis of cellulose, as investigated using transmission and scanning electron microscopy.

• Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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• 2002.05a
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• pp.34-45
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• 2002

The new measuring method of micro-stickies considering both the effects of charge neutralization and evaporation of process water was developed by KRICT PPRC. By the new KRICT method, the contamination of metal dryer surface and other machine clothes could be estimated quickly and simultaneously. According to this study, it could be confirmed that the novel method is a useful one for the evaluation of several treatments regarding the reduction of stickies troubles.

• Journal of Korea Technical Association of The Pulp and Paper Industry
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• v.44 no.6
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• pp.79-86
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• 2012

The aim of this general remarks is to introduce the results concerning the thermo physical, charging, developing and fusing characteristics of micro-encapsulated (MC) model toners in order to apply to the toner of electrophotographic system at the condition of a low temperature. In order to clarify the fusing mechanism of MC toner, rheological analysis of the toner was chosen. It was suggested that MC toner had a different fusing mechanism compared with non-MC toner. Some kinds of MC model toners showed a good result on adhesion test as well as cohesion test. Also, it was possible to get the good charging and development characteristic of MC toner for printing test with laser printer.

• Journal of Korea Technical Association of The Pulp and Paper Industry
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• v.34 no.2
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• pp.73-83
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• 2002

Gloss is very important optical property influencing the perceived quality of the paper surface as well as the surface after printing. Although the average gloss level of paper products or printed images is important to meet end use specifications, the occurrence of gloss mottle, or non-uniformity of gloss, is often of greater concern for meeting quality requirements, especially for the high gloss paper. Gloss variation originates from the irregularities of paper surface, especially surface roughness of paper. Roughness of paper can be divided into micro-roughness (under $1\mu m$ scale in variation) and macro-roughness (over $1\mu m$ scale in variation) depending on the scale of the irregularities. A clearer understanding of the gloss variation of paper can be achieved by separating the contributions of these two scales of roughness, and characterizing them independently. In order to do this, a novel gloss measuring method was introduced. This can detect local gloss with very high resolution. The effect of macro-roughness on gloss variation, which was identified by the measurable surface topography, was separated from the total gloss variation by using this method. The effect of micro-roughness was then estimated indirectly. The local gloss variations of various paper samples were then evaluated to demonstrate the utility of this approach.

• Journal of Korea Technical Association of The Pulp and Paper Industry
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• v.44 no.4
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• pp.99-107
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• 2012

In this study, the lumen loading technology for preparing magnetic papers were evaluated. The rice husk fiber, softwood kraft pulp, hardwood kraft pulp were applied and the morphological properties of pits on the those fibers were investigated with SEM. The softwood kraft pulp had the bigger size of pits, $3{\sim}5{\mu}m$ in diameter, which resulted in higher loading amount. The comparison of two methods for lumen loading such as the low concentration method with the disintegrator and the high concentration method with the Hobart mixer showed the Hobart mixer could resulted in the higher efficiency. The conditions of lumen loading process such loading time, addition amount of metal particles and addition of PEI were also evaluated. The magnetic hysteresis loop of handsheet samples made of lumen loaded fiber with $Fe_3O_4$ and $Fe_2O_3$ were examined. The differences in magnetic properties could be found according to the ferrite types.

• Restorative Dentistry and Endodontics
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• v.46 no.2
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• pp.17.1-17.9
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• 2021

Objectives: In recent in vitro study, it was reported that osteostatin (OST) has an odontogenic effect and synergistic effect with mineral trioxide aggregate (MTA) in human dental pulp cells. Therefore, the aim of this study was to evaluate whether OST has a synergistic effect with MTA on hard tissue formation in vivo. Materials and Methods: Thirty-two maxillary molars of Spraque-Dawley rats were used in this study. An occlusal cavity was prepared and the exposed pulps were randomly divided into 3 groups: group 1 (control; ProRoot MTA), group 2 (OST 100 μM + ProRoot MTA), group 3 (OST 10 mM + ProRoot MTA). Exposed pulps were capped with each material and cavities were restored with resin modified glass ionomer. The animals were sacrificed after 4 weeks. All harvested teeth were scanned with micro-computed tomography (CT). The samples were prepared and hard tissue formation was evaluated histologically. For immunohistochemical analysis, the specimens were sectioned and incubated with primary antibodies against dentin sialoprotein (DSP). Results: In the micro-CT analysis, it is revealed that OST with ProRoot MTA groups showed more mineralized bridge than the control (p < 0.05). In the H&E staining, it is showed that more quantity of the mineralized dentin bridge was formed in the OST with ProRoot MTA group compared to the control (p < 0.05). In all groups, DSP was expressed in newly formed reparative dentin area. Conclusions: OST can be a supplementary pulp capping material when used with MTA to make synergistic effect in hard tissue formation.