• Fire Science and Engineering
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• v.32 no.4
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• pp.1-6
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• 2018

As a preliminary study to quantify the measurement uncertainty of the Schmidt-Boelter type heat flux gauge, the present study has been conducted to evaluate the measurement error due to the calibration constant supported by manufacturer. Calibrations of heat flux gauges are performed at NIST Fire Research Division using a calibration facility with heat source of a 2000 W halogen-tungsten filament lamp and the calibration constant is obtained by comparing the response of the reference and a standard heat flux gauge at the same irradiance conditions. Calibration for heat flux gauges made by three different manufacturers is compared with their factory calibration constant. Relative error due to fluctuation of output signal from heat flux gauges does not exceed 1% of the mean value and the relative error between calibration of this study and factory calibration constant ranged from 1.5% to 14.3%. The present study shows that a continuous and periodic calibration is necessary for accurate heat flux measurement.

• Journal of the Korean Society of Surveying, Geodesy, Photogrammetry and Cartography
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• v.32 no.3
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• pp.191-204
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• 2014

In recent years, multi-camera systems have been recognized as an affordable alternative for the collection of 3D spatial data from physical surfaces. The collected data can be applied for different mapping(e.g., mobile mapping and mapping inaccessible locations)or metrology applications (e.g., industrial, biomedical, and architectural). In order to fully exploit the potential accuracy of these systems and ensure successful manipulation of the involved cameras, a careful system calibration should be performed prior to the data collection procedure. The calibration of a multi-camera system is accomplished when the individual cameras are calibrated and the geometric relationships among the different system components are defined. In this paper, a new single-step approach is introduced for the calibration of a multi-camera system (i.e., individual camera calibration and estimation of the lever-arm and boresight angles among the system components). In this approach, one of the cameras is set as the reference camera and the system mounting parameters are defined relative to that reference camera. The proposed approach is easy to implement and computationally efficient. The major advantage of this method, when compared to available multi-camera system calibration approaches, is the flexibility of being applied for either directly or indirectly geo-referenced multi-camera systems. The feasibility of the proposed approach is verified through experimental results using real data collected by a newly-developed indirectly geo-referenced multi-camera system.

• Mass Spectrometry Letters
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• v.8 no.3
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• pp.59-64
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• 2017

In clinical diagnosis, it's well known that the abnormal level of uric acid (UA) in human body is implicated in diverse human diseases, for instance, chronic heart failure, gouty arthritis, diabetes, and so on. As a primary method, an isotope dilution mass spectrometry (IDMS) has been used to obtain the accurate quantity of UA in blood or serum and also develop the certificated reference material (CRM) so as to provide a SI-traceability to clinical laboratories. Due to the low solubility of UA in water, an ammonium hydroxide ($NH_4OH$) has been considered as a promising solvent to increase the solubility of UA that enables the preparation of both UA and its isotope standard solution for next IDMS-based absolute quantification. But, because of using this $NH_4OH$ solvent, it gives rise to the unwanted degradation of UA. In this study, we sought to optimize condition for the stability of UA in $NH_4OH$ solution by varying the mole ratios of UA to $NH_4OH$, followed by ID-LC-MRM analysis. In addition, we also inspected minutely the effect of the storage temperatures. Additionally, we also performed the quantitative analysis of UA in the KRISS serum certificated reference material (CRM, 111-01-02A) with diverse mixing ratios of UA to $NH_4OH$ and then compared those values to its certification value. Based on our experiments, adjusting the mole ratio of 1/2 ($UA/NH_4OH$) with the storage temperature of $-20^{\circ}C$ is an effective way to secure both the solubility and stability of UA in $NH_4OH$ solution for next IDMS-based quantification of UA in serum.

• Analytical Science and Technology
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• v.30 no.5
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• pp.226-233
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• 2017

In general, quantitative chemical analysis in various areas including food, the environment, in vitro diagnostics, etc., requires traceability in order to increase the reliability of the measurements. Measurement traceability is a property of an unbroken chain of comparisons relating an instrument's measurements to SI units. Purity analysis is the first process for establishing traceability to SI units in chemical measurements. The purpose of this study is to develop and validate a method of purity assignment for establishing the traceability of $17{\beta}$-estradiol measurements in an in vitro diagnostics field. The establishment of this method is very important as it can be applied to the development of CRM and to the analysis of the purity of other hormones. The method of assignment of the purity of $17{\beta}$-estradiol was developed using the mass balance method and was validated through participation in an International comparison. In the mass balance method, impurities are categorized into four classes as follows: total related structure impurities, water, residual organic solvents, and nonvolatiles/inorganics. In this study, total related structure impurities were characterized by a gas chromatography-flame ionization detector (GC-FID) and a high-performance liquid chromatography-ultraviolet (HPLC-UV) detector, water content was determined by a Karl-Fisher coulometer, and total residual solvents and nonvolatiles/inorganics were checked simultaneously by thermogravimetric analysis (TGA). The purity of the $17{\beta}$-estradiol was 985.6 mg/g and the expanded uncertainty was 2.1 mg/g at 95% confidence. The developed method can be applied to the development of certified reference materials, which play a critical role in traceability.

• Journal of Sensor Science and Technology
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• v.11 no.3
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• pp.145-154
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• 2002

NiCr-heaters with three different thicknesses ranging from 400 nm to 800 nm were fabricated and their characteristics were compared for the purpose of developing a chromel-alumel multijunction thermal converter for low input voltage with low frequency. The thermoelectric effect-induced AC-DC voltage transfer difference of the thermal converter with a built-in NiCr-heater of 400 nm-thickness was ${\pm}0.51{\sim}1.69\;ppm$ in the DC reversing frequency of $40\;Hz{\sim}10\;kHz$ with appling $0.5\;V_{rms}$ and the difference was increased to ${\pm}40{\sim}{\pm}115\;ppm$ in the frequency of $40\;Hz{\sim}1\;MHz$, when both thermoelectric effects and frequency effects were considered, showing the thermal converter would be suitable for the low input voltage application with low frequency.

• Journal of Sensor Science and Technology
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• v.7 no.2
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• pp.90-96
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• 1998

Non-contacting capacitive sensors, based on principle of the cross capacitor, for measuring small displacement less than $1.95{\pm}0.5\;mm$ have been fabricated and characterized. To overcome disadvantages of the existed capacitive sensors with 2-electrodes and 3-electrodes, the new sensor is consisted of 4-electrodes which are formed two electrode(high, low) and 2 guard electrodes on a sapphire plate with diameter 17 mm and thickness 0.7 mm, and are symmetrically situated with a constant gap of 0.2 mm between the electrodes. This sensor can be used for measuring both metallic and non-metallic target without ground connection, and is evaluated to the correlation coefficient of 0.9987 for the range of $1.95{\pm}0.5\;mm$ and that of 0.9995 for $1.95{\pm}0.25\;mm$ range.

• Aerospace Engineering and Technology
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• v.3 no.1
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• pp.126-133
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• 2004

Photogrammetry, as its name implies, is a 3-dimensional coordinate measuring technique that uses photographs as the fundamental medium for metrology. In the last few years the accuracy of photogrammetry has increased dramatically thanks to the rapid advance of digital camera manufacturing technique. This paper discusses photogrammetric measurement of the interface surface of MSC(Multi-Spectral Camera), which is a main payload of KOMPSAT-2. Total 24 paper targets on the objective surfaces and two scale bars calibrated with high accuracy were used for measurement, and multiple images were taken from 11 different camera angles by using a spacecraft rotation dolly. As a result of analysis, 3D coordinates of each targeted point were obtained and the flatness value based on the selected reference plane was calculated and compared with the pre-determined requirement. The technique acquired by this study is expected to be used for the 3D precise measurement of ultra-light weight and inflatable space structures such as a satellite antenna and a solar array.

• The Journal of the Acoustical Society of Korea
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• v.24 no.4
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• pp.194-201
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• 2005

Since the necessity for the accurate measurement in the field of acoustics, vibration, and ultrasound was internationally increased, CCAUV (Consultative Committee for Acoustics , Ultrasound and Vibration) was created by the CIPM (International Committee for Weights and Measures) in 1998. One of the first activities of CCAUV is the key comparison on 1' standard microphones. The key comparison was done from April. 1999 to April. 2001 and 12 NMIs(National Metrology Institutes) including KRISS (Korea Research Institute of Standards and Science) were participated. The pilot laboratory was the National Physical Laboratory(NPL). The traveling standards were two LSIP(Laboratory Standard 1' Pressure Type) microphones specified in IEC 61094-1 and the calibration frequency ranges covers from 63Hz to 8kHz. In this paper, the analyzed results in the final report were summarized.

• Bulletin of the Korean Chemical Society
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• v.33 no.1
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• pp.143-148
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• 2012

The photodissociation dynamics of cyclopropyl bromide ($C_3H_5Br$) and cyclobutyl bromide ($C_4H_7Br$) at 234 nm was investigated. A two-dimensional photofragment ion-imaging technique coupled with a [2+1] resonanceenhanced multiphoton ionization scheme was utilized to obtain speed and angular distributions of the nascent $Br(^2P_{3/2})$ and $Br^*(^2P_{1/2})$ atoms. The recoil anisotropies for the Br and $Br^*$ channels were measured to be ${\beta}_{Br}=0.92{\pm}0.03$ and ${\beta}_{Br^*}=1.52{\pm}0.04$ for $C_3H_5Br$ and ${\beta}_{Br}=1.10{\pm}0.03$ and ${\beta}_{Br^*}=1.49{\pm}0.05$ for $C_4H_7Br$. The relative quantum yield for Br was found to be ${\Phi}_{Br}=0.13{\pm}0.03$ and for $C_3H_5Br$ and $C_4H_7Br$, respectively. The soft radical limit of the impulsive model adequately modeled the related energy partitioning. The nonadiabatic transition probability from the 3A' and 4A' potential energy surfaces was estimated and discussed.

• The Journal of the Acoustical Society of Korea
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• v.24 no.8
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• pp.431-440
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• 2005

The precise measurement of ultrasonic power is important to the qualify assurance and the safety of medical ultrasonic equipments In the Present work, a brier theory was introduced to determine the ultrasonic Power from the time valving balance-indication due to the radiation force acting on an absorbing target and/or other causes such as buoyancy during the repetition of on/off behavior of ultrasonic irradiation. The developed automated system measuring the ultrasonic power was described in detail with the precise mechanical alignment tool , the electric signal generation network, the control and measurement network and the appropriate procedure. The ultrasonic power measured by the developed system was compared to the reference data calibrated by the other national metrology institute at 1 MHz, 5 MHz, 10 MHz, and 15 MHz over the range 10 mW to 10 W. Their relative differences are within $5\%$.