• Title/Summary/Keyword: mechanical and thermal properties

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Thermo-Mechanical Properties of Al2TiO5 Ceramics Stabilized with MgO and ZrO2 Additives (MgO와 ZrO2가 첨가된 Al2TiO5 세라믹의 열·기계적 물성)

  • Kim, Da-Mi;Kim, Hyung-Tae;Kim, Hyeong-Jun;Kim, Ik-Jin;Choi, Seong-Cheol;Kim, Yong-Chan;NamKung, Jung;Ryu, Sung-Soo
    • Journal of Powder Materials
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    • v.19 no.4
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    • pp.253-258
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    • 2012
  • The characteristics of $Al_2TiO_5$ ceramics were influenced by the additives and the heat treatment that controls the microcrack behavior at grain boundaries. The effect of additives on $Al_2TiO_5$ ceramics were investigated in terms of mechanical properties and thermal expansion at high temperature. The $Al_2TiO_5$ were synthesized at $1500^{\circ}C$, $1550^{\circ}C$ and $1600^{\circ}C$ for 2h by reaction sintering. The formation of $Al_2TiO_5$ phase was increased by additives that enhanced the volume of the microcrack that can lead to low thermal expansion. The mechanical properties of the stabilized $Al_2TiO_5$ ceramics were increased remarkably at $1100^{\circ}C$, $1200^{\circ}C$ and $1300^{\circ}C$ due to the oneset of mechanical healing of grain-bondary microcracks at a high temperature. The amount of microcrack was decreased at lower sintering temperature that causes the increase of mechanical properties at high temperature.

The Properties of DSC and DMA for Epoxy Nano-and-Micro Mixture Composites

  • Lee, Chang-Hoon;Park, Jae-Jun
    • Transactions on Electrical and Electronic Materials
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    • v.11 no.2
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    • pp.69-72
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    • 2010
  • This study investigates the thermal and mechanical properties of insulation elements through the mixing of epoxy based micro and nano particles. Regarding their thermal properties, differential scanning calorimeter and dynamic mechanical analyser were used to calculate the cross-linking densities for various types of insulation elements. The mechanical properties of the bending strength, the shape and scale parameters, were obtained using the Weibull plot. This study obtained the best results in the scale parameters, at 0.5 phr, for the bending strength of the epoxy nano-and-micro mixture composites.

Physical and Chemical Properties of Silk Fiber Treated with Calcium Nitrate (질산칼슘 처리농도에 따른 수축견사의 이화학적 특성)

  • 이광길;이용우
    • Journal of Sericultural and Entomological Science
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    • v.40 no.1
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    • pp.70-77
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    • 1998
  • This study was carried out in order to find out the relationship between physical and chemical properties of silk fiber treated by concentrated calcium nitrate solution. The tensile, thermal and dynamic mechanical properties are also examined on Ca(NO3)2 treated silk fibers. The tensile properties of silk fibers treated by calcium nitrate changed with a concentration. The thermal behavior were also affected by the concentration of calcium nitrate. The degradation temperature (endotherms) and glass transition temperature shifted to lower temperature as the treated concentration increased. It is thought that the physical properties are strongly related to the structure and morphology of Ca(NO3)2 treated silk fibers. As a result, these give property changes with a concentration dependence.

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Effect of $TiO_2$ Nanoparticle on the Mechanical and Thermal Properties of Epoxy Resin Composites (에폭시수지 복합재료의 기계적.열적 성질에 대한 $TiO_2$ 나노입자의 영향)

  • Moon, Y.J.;Choi, J.Y.;Kim, B.A.;Moon, C.K.
    • Journal of Power System Engineering
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    • v.14 no.4
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    • pp.68-75
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    • 2010
  • The effect of dispersion agent, the content and size of nanoparticle on the mechanical and thermal properties has been investigated in $TiO_2$ nanoparticle/epoxy resin composites(nanocomposites). The weight fraction of fabricated nanocomposites were 0, 1, 3, 5%, respectively. The glass transition temperature was lower than pure epoxy resin and decreased with the increasing of nanopaticle content. This is considered that the cross link of epoxy resin during solidification was hindered by the presence of nanoparticles. Nanocomposites of 3wt% content with dispersion agent showed the best tensile strength. The tensile strength of 20㎚ $TiO_2$ nanocomposites were higher than one of 200nm $TiO_2$ nanocomposites.

Structure -Properties Relations of Polypropylene/ Liquid Crystalline Polymer Blends

  • Sahoo, N.G.;Das, C.K.;Jeong, Hye-Won;Ha, Chang-Sik
    • Macromolecular Research
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    • v.11 no.4
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    • pp.224-230
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    • 2003
  • The blends of polypropylene (PP) with glass filled thermotropic liquid crystalline polymer (LCP-g) have been prepared by melt mixing techniques at different blend ratios. The thermal, dynamic mechanical, crystalline and morphological characteristics of these blends were investigated. Higher percent crystallinity was observed for 10% level of LCP-g in the blend in comparison to that of other blend ratios. The thermal stability increased with LCP-g concentration in the blend with PP. The variation of storage modulus, stiffness and loss modulus as a function of blend ratios suggested the phase inversion at the 50% level of LCP-g in the blend. The scanning electron microscopy (SEM) photographs showed the creation of voids and destruction of the fiber structures during the dynamic mechanical measurements. Processing behavior of the blends depended on the fiber forming characteristics of LCP-g, which again varied with the molding temperatures.

The Thermal Stability and Elevated Temperature Mechanical Properties of Spray-Deposited $SiC_P$/Al-11.7Fe-1.3V-1.7Si Composite

  • Hao, L.;He, Y.Q.;Wang, Na;Chen, Z.H.;Chen, Z.G.;Yan, H.G.;Xu, Z.K.
    • Advanced Composite Materials
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    • v.18 no.4
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    • pp.351-364
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    • 2009
  • The thermal stability and elevated temperature mechanical properties of $SiC_P$/Al-11.7Fe-1.3V-1.7Si (Al-11.7Fe-1.3V-1.7Si reinforced with SiC particulates) composites sheets prepared by spray deposition (SD) $\rightarrow$ hot pressing $\rightarrow$ rolling process were investigated. The experimental results showed that the composite possessed high ${\sigma}_b$ (elevated temperature tensile strength), for instance, ${\sigma}_b$ was 315.8 MPa, which was tested at $315^{\circ}C$, meanwhile the figure was 232.6 MPa tested at $400^{\circ}C$, and the elongations were 2.5% and 1.4%, respectively. Furthermore, the composite sheets exhibited excellent thermal stability: the hardness showed no significant decline after annealing at $550^{\circ}C$ for 200 h or at $600^{\circ}C$ for 10 h. The good elevated temperature mechanical properties and excellent thermal stability should mainly be attributed to the formation of spherical ${\alpha}-Al_{12}(Fe,\;V)_3Si$ dispersed phase particulates in the aluminum matrix. Furthermore, the addition of SiC particles into the alloy is another important factor, which the following properties are responsible for. The resultant Si of the reaction between Al matrix and SiC particles diffused into Al matrix can stabilize ${\alpha}-Al_{12}(Fe,\;V)_3Si$ dispersed phase; in addition, the interface (Si layer) improved the wettability of Al/$SiC_P$, hence, elevated the bonding between them. Furthermore, the fine $Al_4C_3$ phase also strengthened the matrix as a dispersion-strengthened phase. Meanwhile, load is transferred from Al matrix to SiC particles, which increased the cooling rate of the melt droplets and improved the solution strengthening and dispersion strengthening.

Reliability Properties of Carbon Nanotube-filled Solderable Anisotropic Conductive Adhesives (탄소 나노튜브 함유 Solderable 이방성 도전성 접착제의 신뢰성 특성에 관한 연구)

  • Yim, Byung-Seung;Lee, Jeong Il;Kim, Jong-Min
    • Journal of Welding and Joining
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    • v.35 no.3
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    • pp.15-20
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    • 2017
  • In this paper, two types of assemblies using CNT-filled SACAs (with 0.03 wt% CNTs and without CNT) were prepared to investigate the influence of carbon nanotubes (CNTs) on the reliability properties of solderable anisotropic conductive adhesives (SACAs) with a low-melting-point alloy (LMPA). Two types of reliability test including thermal shock (TS: -55 to $125^{\circ}C$, 1000 cycles) and high-temperature and high-humidity (HTHH: $85^{\circ}C$, 85% RH, 1000 h) tests were conducted. The SACA assemblies with and without CNTs showed stable electrical reliability properties due to the formation of wide and stable metallurgical interconnection between corresponding metallizations by the molten LMPA fillers. Although the mechanical pull strength of CNT-filled SACA assemblies was decreased after thermal aging (because of the excessive layer growth and planarization of the IMCs), the CNT-filled SACA with 0.03wt% CNTs showed enhanced mechanical reliability properties compared with the SACA assemblies no CNTs. This enhancement in mechanical performance was due to the reinforcement effect of the CNTs. These results demonstrate that CNTs within the CNT-filled SACAs can improve the reliability properties of CNT-filled SACAs joints due to their superior physical properties.

Effect of Heat Treatment on the Physical Properties of LM PET Jacquard Fabrics (저융점 폴리에스터 자카드직물의 물성에 대한 열처리 효과)

  • Lee, Sun Young;Kim, Jeong Hwa;Kim, Eui Hwa;Lee, Jung Soon;Lee, Seung Goo
    • Textile Coloration and Finishing
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    • v.25 no.3
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    • pp.206-214
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    • 2013
  • There has been an increasing demand for high performance and energy-saving of blind. In order to develop the eco-friendly blind textiles, heat treatment process has been utilized for LM(Low Melting) polyester fabrics and the changes of the physical properties of the treated fabrics were examined according to temperature of heat treatment. Morphology, surface reflectance, contact angle, luster, thermal property and mechanical property of heat treated LM polyester fabrics were investigated. As results, morphology analysis of thermal treated fabrics confirmed that degree of fusion of LM polyester yarns improved with increase of temperature. Surface reflectance of thermal treated fabrics decreased with increase of temperature. Luster and contact angle of a water droplet on thermal treated fabrics increased slightly with increase of temperature. The mechanical properties of the fabrics by KES-FB system were found to be temperature-dependent and especially, bending and shear properties among them were highly related to temperature.

Fracture Characteristics of Flame Thermal Shock in PSZ/NiCrAlY FGM (세라믹(PSZ)/금속(NiCrAlY) 경사기능성 복합재료의 화염 열충격 파괴특성)

  • Song, Jun-Hee;Mun, Sang-Don
    • Korean Journal of Metals and Materials
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    • v.48 no.8
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    • pp.775-779
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    • 2010
  • Functionally graded materials (FGM) of PSZ/NiCrAlY on Inconel substrate were fabricated by detonation gun spraying method. A thick ceramic layer generally has a high thermal barrier effect however, because failure often occurs, the use of an FGM layer gives an advantage in thermal property. During the thermal shock test, micro fracture processes were detected by the AE method. Also, the thermal shock test was performed for NFGM, FGM and the changed FGM in the layered composition profile. It was found through AE testing and the observation of fracture surface that FGM was superior to NFGM in thermal shock properties. The linear or metal-rich type FGM in composition profile had the best resisting property among the FGM. It was found that the controlled composition profile of the graded layers had better thermal properties.

The Sense of Touch of Man-made Leather (인조피혁의 촉감평가)

  • 이정순;신혜원
    • Journal of the Korean Society of Clothing and Textiles
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    • v.24 no.2
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    • pp.277-285
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    • 2000
  • The purpose of this study was to quantify the relationship between the sense of touch and mechanical properties of man-made leather. The first was to develop the five conversion equations which convert mechanical properties of man-made leather into five factor scores, which express five factors of the sense of touch(surface property, stretchiness, thickness & weight, thermal property(warmth & coolness), and moisture property(sticky & clingy)). The second was to develop the conversion equation which converts five factor scores into score of the sense of touch. Five factor scores were predicted by the following mechanical properties; surface property factor by log2HB and (log2HB)2, stretchiness factor by logEM, thickness & weight factor by logT, log2HB, logW, thermal property factor by logT, logHB, logSMd, and moisture property factor by logMMD, RC, RC2, (logEM)2, RT2. Subsequently, these five factor scores were converted into score of the sense of touch. The predictive abilities of the developed equations were satisfied.

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