• Title/Summary/Keyword: measurement uncertainty

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Development of a Model System of Uncertainty Evaluations for Multiple Measurements by Isotope Dilution Mass Spectrometry: Determination of Folic Acid in Infant Formula

  • Kim, Byung-Joo;Hwang, Eui-Jin;So, Hun-Young;Son, Eun-Kyung;Kim, Yong-Seong
    • Bulletin of the Korean Chemical Society
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    • v.31 no.11
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    • pp.3139-3144
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    • 2010
  • A model system has been established for the evaluation of the uncertainty of the value from measurements of multiple subsamples by isotope dilution mass spectrometry (IDMS). In this report, we apply this model system for the evaluation of measurement uncertainty in determination of folic acid in infant formula. Five subsamples were analyzed by IDMS. The mean of the measurement results of the five subsamples was assigned as the final measurement value. The standard deviation (s) of the results from five subsamples was attributable to repeatability of the measurement. The uncertainty components in the IDMS measurement methods were categorized into two groups. Group I includes uncertainty components which give common systematic effects to all subsamples and do not contribute to the variation among multiple measurements (repeatability). Group II includes uncertainty components that give random effects on the measurement results, and are related with the measurement repeatability. These random effects are attributed to s. Therefore, the uncertainty of the final value was calculated by combining the standard deviation of the mean of multiple measurements, $s/{\surd}n$ (where n = 5), and the measurement uncertainty associated with the uncertainty components that give systematic effects.

Uncertainty Analysis and Improvement of an Altitude TestFacility for Small Jet Engines

  • Jun, Yong-Min;Yang, In-Young;Kim, Chun-Taek;Yang, Soo-Seok;Lee, Dae-Sung
    • International Journal of Aeronautical and Space Sciences
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    • v.5 no.1
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    • pp.46-56
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    • 2004
  • The verification and improvement of the measurement uncertainty have beenperformed in the altitude test facility for small gas turbine engines, which was built atthe Korea Aerospace Research Institute (KARI) in October 1999. This test is performedwith a single spool turbojet engine at several flight conditions. This paper discussesthe evaluation and validation process for the measurement uncertainty improvements usedin the altitude test facility. The evaluation process, defined as tests before the facilitymodification, shows that the major contnbutors to the measurement uncertainty are theflow meter discharge coefficient, the inlet static and total pressures, the cell pressureand the fuel flow rate. The measurement uncertainty is focused on the primary parametersof the engine performance such as airflow rate, thrust and specific fuel consumption (SFC).The validation process, defined as tests after the facility modification, shows that themeasurement uncertainty, in seal level condition, is tmproved to the acceptable level throughthe facility modification. In altitude test conditions, the measurement uncertainties arenot improved as much as the uncertainty in sea level condition.

Uncertainty Evaluation of Nicotine in Cigarette Mainstream Smoke Using Two Point Re-calibration Method (두 점 교정법을 이용한 담배 연기 성분 중 니코틴 분석 결과에 대한 불확도 평가)

  • Kim Mi-Ju;Ji Sang-Un;Hwang Keon-Joong;Lee Moon-Soo;Cho Sung-Eel
    • Journal of the Korean Society of Tobacco Science
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    • v.26 no.2 s.52
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    • pp.168-178
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    • 2004
  • Uncertainty of final measurement results considering main uncertainty sources being in nicotine of mainstream smoke was estimated. This study was accomplished by using the ISO 'The Guide to the Expression of Uncertainty in Measurement'. Using the two point re-calibration method, uncertainty for nicotine concentration was calculated considering the uncertainty sources of each step. The concentration and uncertainty of nicotine in mainstream smoke was estimated as $153.95{\pm}17.84\;{\mu}g/mL\;(0.77\pm0.089 mg/cig)$. The expanded uncertainty was $17.84 {\mu}g/mL(\pm0.089 mg/cig).$ The reported expanded uncertainty of the measurement is stated as the standard uncertainty of measurement multiplied by a coverage factor of 2, which for a normal distribution corresponds to a coverage probability of approximately $95\%$ The former expression indicates the conversion concentration into the sample.

An Evaluation of the Uncertainty of Pressure Measurement Systems (압력 측정 시스템의 불확도 평가)

  • 최주호;홍성수
    • Journal of the Korea Institute of Military Science and Technology
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    • v.5 no.1
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    • pp.15-23
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    • 2002
  • Uncertainty components and evaluation of the system of pressure measurement are presented in this paper. Since early in 1980s, measurement uncertainty is getting more important due to ISO/IEC 17025, which is established for international test and calibration laboratories. Up to now it is true that accuracy, precision, error and etc. have been commonly used in industry to define the amount of error to the products and equipment, but these terms ought to be united into uncertainity in the future. This paper describes how to indicate measurement uncertainty and types of measurement errors, and then shows the evaluation result of measurement system using piezoelectric pressure transducers.

An Experimental Study on the Performance of Cooling Tower Unit for Mechanical Draft (기계통풍식 냉각탑 유닛의 성능에 관한 실험적 연구)

  • JEONG, SOON YOUNG
    • Transactions of the Korean hydrogen and new energy society
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    • v.32 no.6
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    • pp.642-648
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    • 2021
  • In this paper, an experimental study was conducted on the performance of the cooling tower. In order to improve reliability in the cooling tower performance test, the measurement uncertainty of the instrument was estimated. Measurement uncertainty refers to the uncertainty of a measurement, estimates the range in which the expected value of the measurement can be within a certain confidence level, and suggests a range in which the measured representative value is incorrect. Therefore, the measurement result of the performance experiment is not an actual value, but a reasonable estimated value. The measurement uncertainty for the test was calculated and the measured results were presented.

Measurement Uncertainty Analysis of Positioning Accuracy for High Precision Feed Mechanism (고정밀 이송기구의 위치결정정밀도에 대한 측정불확도 요소 분석)

  • Lee, Jung-Hoon;Yoon, Sang-Hwan;Park, Min-Won
    • Journal of the Korean Society for Precision Engineering
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    • v.29 no.5
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    • pp.494-499
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    • 2012
  • Reliable results can't be derived without the notion of measurement uncertainty. The reason is that the measured value includes a lot of uncertain factors. Finding the factor that affect the measurement of parameter is important for estimation of measurement uncertainty. In this paper, the evaluation of uncertainty analysis about positioning accuracy measurements of high precision feed mechanism is presented to evaluate the important factors of uncertainty.

A Study on the Measurement Method and Uncertainty Factors for Precision Inspection to Feed Unit of High Precision Machine Tool (고정밀 공작기계 이송장치의 정밀도 측정방법 및 불확도 요인에 관한 연구)

  • Kim, Sang-Hwa;Kim, Byung-Ha;Choi, Woo-Gak
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.11 no.4
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    • pp.55-61
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    • 2012
  • Very important content in performance evaluation of machine tool is positioning accuracy and repeatability precision measurements of feed mechanism. A study analyses the measurement method and uncertainty factors by ISO-based test method. Reliable results can't be derived without the notion of measurement uncertainty. The reason is that the measured value includes a lot of uncertain factors. Finding the factor that affects the measurement of parameter is important for estimation of measurement precision. In this paper, the evaluation of uncertainty analysis about positioning accuracy and repeatability precision measurements of high precision feed mechanism is presented to evaluate the important factors of uncertainty.

Uncertainty Evaluation of Viscosity Measurement Standards (점도 측정표준 불확도 평가)

  • Choi, H.M.;Yoon, B.R.;Lee, Y.B.;Choi, Y.M.;Lee, S.H.
    • 유체기계공업학회:학술대회논문집
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    • 2005.12a
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    • pp.295-301
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    • 2005
  • Viscosity measurement standards were evaluated according to ISO/IEC 17025. The step-up procedure was employed to calibrate a series of capillary type master viscometers. Uncertainty was calculated with evaluation of various uncertainty factors affected in viscosity measurement. The maximum expanded uncertainty(U) of the master viscometer was $3.0{\times}10^{-3}$(at the confidence level of 95 %). This evaluation example will be useful in viscosity measurement uncertainty determination of other standard measurement.

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Estimation of Uncertainty in Vibration Measurement of Shipboard Equipment (함정탑재장비 진동 측정불확도 추정)

  • Park, Sungho;Lee, KyungHyun;Han, HyungSuk
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.24 no.7
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    • pp.509-516
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    • 2014
  • This paper proposes estimation model of uncertainty in vibration measurement of shipboard equipment and analyzes the result of uncertainty estimation. Vibration of shipboard equipments affects underwater radiated noise that is important performance related to stealth of the naval vessel. Acceptance testing for shipboard equipment is required to guarantee the stealth performance of naval vessel. In measuring, detailed uncertainty estimation is essential to improve measuring reliability. Acceptance testing result of structure-borne noise and vibration is used to analyze uncertainty in vibration measurement of shipboard equipment.

Measurement uncertainty in heavy-weight floor impact sounds (측정 불확도에 따른 중량충격음 측정편차에 관한 연구)

  • Yoo, Seung-Yup;Kim, Yong-Hee;Sim, Myoung-Hee;Jeon, Jin-Yong
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2008.04a
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    • pp.826-829
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    • 2008
  • In a field measurement, measurement errors are produced by measuring environments and systematic errors in the measurement procedure. Measurement errors can be expressed as a measurement uncertainty. In this study, the measurement uncertainty and various measuring factors are investigated in heavy-weight impact sounds. According to KS 2810-2, the model functions, which is the estimation of the maximum SPL measurement in each octave band frequency, are determined. From this estimation model, 3.53dB is shown in 63Hz. This level is caused by the sound field of the receiving room, which does not meet the diffusing field.

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