• Title/Summary/Keyword: maximum absorption

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Studies on Separation, Detection and Quantitation of Estriol, Estrone, Estradiol-17 β in Urine of Dairy Cows by Paper, Thin Layer and Column Chromatography (Paper, Thin Layer 및 Column Chromatography에 의한 요중의 Estriol, Estrone, Estadiol-17 β의 분리 정량에 관하여)

  • Yang, Yong Kwan;Han, Soo Nam;Cho, Jong Hoo
    • Korean Journal of Veterinary Research
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    • v.13 no.1
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    • pp.23-30
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    • 1973
  • Thin layer, paper and column chromatography were compared for the separation, detection and quantitation of three kinds of estrogen in urine of dairy cows. While thin layer chromatography utilizing silica gel was better for the detection of estrogens, column chromatography using celite 545 was preferable. Spectrophotometry was compared with fluorometry for determination of estrone, estradiol-17 ${\beta}$ and estriol eluted by paper chromatography and column chromatography. Optical density of three standard estrogens showed almost same curve at maximum absorption wave length of 230 and $282m{\mu}$. However, the former showed a higher peak. In fluorometry, the fluorescence intensity of estrone and estradiol-17 ${\beta}$ were rather strong, when the estrogens were dissolved in sulfuric acid, and showed higher sensitivity than that of the spectrophotometry. However, in the case of estriol was exceptional.

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The Properties of Acoustic in Multi-purpose out-door Stadium II - a case study of seoul world cup stadium measurement - (다목적 야외경기장의 음향특성에 관한 연구 II -서울월드컵 경기장의 전기음향시스템고찰과 음향측정을 중심으로-)

  • 김정중;손장열
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2002.05a
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    • pp.731-739
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    • 2002
  • recently out door stadiums have been built as multi purpose stadium for athletic sports It hold but also various events and huge concerts. in the past, out-door stadium usually was built, but recently the out-door stadium which of the 50 % of roof covered by doom have been built increasingly. as the result, the sound obstacle is becoming very important. but a design of sound has become unplaned except some of the stadium, also rarely been built by sound-absorption material. as the result, the purpose of this study is investigating, analyzing the theory for plan of electric acoustic sound, a drawing of acoustic design and measurement a result value, comparison, evaluating a main sound factor with criteria of the Seoul City design. and reservation time, clearness, sound pressure level suitable for using purpose, so the necessary quantities will be added to financial budget of building acoustic design. and For verification, this contains acoustic analyser measurement and computer simulation and this study will find the solution of helping method.

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An Investigation of Power Flow Mechanism in Beam-plate Built-up Structures with an Energy-absorbing Plate (보-판 결합 구조물에서 에너지 흡수체로 작용하는 판의 특성에 따른 파워 전달 특성에 관한 연구)

  • Yoo, Ji-Woo
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.17 no.1 s.118
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    • pp.55-64
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    • 2007
  • In the built-up structure consisting of a stiff beam and a flexible plate, Grice showed that the plate behaves as an energy absorber in narrow frequency bands(called plate blocking effect). This paper deals with such beam-plate coupled structures, where the plate is an energy absorber and the excited beam is an energy path. It is found that such energy dissipation can occur in the relatively broad bands, if different stiffnesses are used in the rectangular plate. It was experimentally verified by Heckl that the energies in terms of one-third octave band averages transferred to the plate(or dissipated in the plate) increase for increased plate damping. This Paper, however, shows that the energy absorption suddenly reduces at the certain narrow frequency bands where the plate damping effect upon the coupled beam is maximum. Also, in order to minimize energy transfer through the beam in terms of one-third octave band averages, it is advantageous to increase the plate damping closer to the excitation point All these results are based on the wane method.

Experimental and analytical study in determining the seismic performance of the ELBRF-E and ELBRF-B braced frames

  • Jouneghani, Habib Ghasemi;Haghollahi, Abbas
    • Steel and Composite Structures
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    • v.37 no.5
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    • pp.571-587
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    • 2020
  • In this article the seismic demand and performance of two recent braced steel frames named steel moment frames with the elliptic bracing (ELBRFs) are assessed through a laboratory program and numerical analyses of FEM. Here, one of the specimens is without connecting bracket from the corner of the frame to the elliptic brace (ELBRF-E), while the other is with the connecting brackets (ELBRF-B). In both the elliptic braced moment resisting frames (ELBRFs), in addition to not having any opening space problem in the bracing systems when installed in the surrounding frames, they improve structure's behavior. The experimental test is run on ½ scale single-story single-bay ELBRF specimens under cyclic quasi-static loading and compared with X-bracing and SMRF systems in one story base model. This system is of appropriate stiffness and a high ductility, with an increased response modification factor. Moreover, its energy dissipation is high. In the ELBRF bracing systems, there exists a great interval between relative deformation at the yield point and maximum relative deformation after entering the plastic region. In other words, the distance from the first plastic hinge to the collapse of the structure is fairly large. The experimental outcomes here, are in good agreement with the theoretical predictions.

Dissolution Rate and Bioavailability of Acyclovir, Antiviral Agent, by Cyclodextrin Inclusion Complexation (시클로텍스트린 포접복합체 형성에 의한 항바이러스제 아시클로버의 용출속도 및 생체이용률)

  • Park, Seung-Hyun;Kim, Ha-Hyung;Lee, Kwang-Pyo
    • Journal of Pharmaceutical Investigation
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    • v.28 no.4
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    • pp.257-266
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    • 1998
  • To improve the solubility and dissolution rate of acyclovir (ACV), which is low oral bioavailability due to its properties of slight solubility in water and incomplete gastrointestinal absorption, the solid inclusion complexes of ACV with ${\alpha}CD$, ${\beta}CD$, $DM{\beta}CD$ in molar ratio of 1:1 were prepared by the freeze-drying method. The inclusion complexes were investigated by solubility study, UV, IR and DSC. The dissolution rate of ACV was significantly increased by ACV-CDs inclusion complex formation in artificial intestinal fluid at pH 6.8. The enhanced dissolution rate of ACV could be due to an increase of solubility and the formation of an amorphous structures through inclusion complexation with CDs. Especially, $ACV-DM{\beta}CD$ inclusion complex enhanced the maximum plasma concentration levels and AUC following oral administration compared to those of ACV alone. The present results suggest that $ACV-DM{\beta}CD$ inclusion complex serves as a potential carrier for improving the solubility, the dissolution rate and the bioavailability of ACV.

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The Dyeability of Extract from Opuntia Ficusindica var. Saboten fruits (백년초열매 추출물의 염색성)

  • Kim, In-Young;Lee, So-Hee;Song, Wha-Soon
    • Textile Coloration and Finishing
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    • v.19 no.6
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    • pp.1-6
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    • 2007
  • Opuntia Ficus has been an epiphyte plant since it was introduced in Cheju island as an ornamental plant two hundred years ago. And now it is grown as many as it is designated to local souvenir No.35. The fruit of this plant contains red-purple sap, which is due to be used in coloring clothes. This study aims at confirmation of use possibility as eco-friendly dyeing stuffs on extract from opuntia ficus fruits and contributing to the practical use of natural dyeing. Thus this study was investigated the dyeability of extract from opuntia ficus fruits on the silk fabric. Antioxidants were used ascorbic acid, L-cysteine, prophyl gallete. After dyeing, K/S and dye fastness were measured. The results were as follows; Maximum absorption band of extract from opuntia ficus fruits was 534.5nm. The appropriate dyeing condition was bath ratio 50:1, dyeing temperature $30^{\circ}C$, dyeing concentration 50%, dyeing time 50min, pH 3,concentration of all antioxidants 3%. Addition of antioxidants brought increase of K/S value. And K/S value and dye fastness had the greatest value when ascorbic acid was added

Physicochemical Properties of Rice Extrudate with Added Ginger Powder by the Response Surface Regression Analysis (반응 표면 분석에 의한 생강 분말을 첨가한 쌀 압출 성형물의 이화학적 성질)

  • 고광진
    • The Korean Journal of Food And Nutrition
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    • v.6 no.3
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    • pp.178-188
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    • 1993
  • This research was attempted to investigate changes in physicochemical properties of rice extrudate with added ginger powder extruded by single screw extruder. Graphic three dimensional analysis on response surface regression was used to evaluate effects of extrusion variables on quality factors of the extrudate according to two independent variables, ginger consent 0∼12%, moisture content 14∼26%. The summarized results are as follows : 1) Regarding proximate composition of rice extrudate with added ginger powder, as ginger powder content of raw material Increased, crude tat, crude protein, crude ash and crude fiber increased, while soluble nitrogen free extract decreased. 2) Graphic three dimensional analysis on response surface regression was conducted for each dependent variable which revealed statistically significant relationship with independent variables, 0∼120A ginger and 14∼26% moisture content. Expansion ratio had a critical point as moisture content changed. As ginger and moisture content Increased, bulk density, break strength and water absorption Index Increased, while water solubility Index decreased. The predicted maximum degree of gelatinization in 6.15% ginger and 15.56% moisture content is 88.27%, and lightness decreased as ginger content Increased. According to the microstructure for the cross section of extrudate obsorbed with image analyzer, air cell number and perimeter revealed saddle point, meanwhile total area and fractarea of air cell had critical points as moisture content changed. In view of the results, quality of rice extrudate with added ginger powder was optimum when rice flour was fed to the extruder with 2∼7% singer powder and 15∼20% moisture content.

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Effectiveness of some conventional seismic retrofitting techniques for bare and infilled R/C frames

  • Kakaletsis, D.J.;David, K.N.;Karayannis, C.G.
    • Structural Engineering and Mechanics
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    • v.39 no.4
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    • pp.499-520
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    • 2011
  • The effectiveness of a technique for the repair of reinforced concrete members in combination with a technique for the repair of masonry walls of infilled frames, damaged due to cyclic loading, is experimentally investigated. Three single - story, one - bay, 1/3 - scale frame specimens are tested under cyclic horizontal loading, up to a drift level of 4%. One bare frame and two infilled frames with weak and strong infills, respectively, have been tasted. Specimens have spirals as shear reinforcement. The applied repair technique is mainly based on the use of thin epoxy resin infused under pressure into the crack system of the damaged RC joint bodies, the use of a polymer modified cement mortar with or without a fiberglass reinforcing mesh for the damaged infill masonry walls and the use of CFRP plates to the surfaces of the damaged structural RC members, as external reinforcement. Specimens after repair, were retested in the same way. Conclusions concerning the effectiveness of the applied repair technique, based on maximum cycles load, loading stiffness, and hysteretic energy absorption capabilities of the tested specimens, are drawn and commented upon.

Electrochromism of Various Conducting Polymers with Enhanced Functionality (기능성을 향상시킨 다양한 전도성 고분자의 전기 변색 현상)

  • Ko Heung-Cho;Moon Bong-Jin;Lee Hoo-Sung
    • Polymer(Korea)
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    • v.30 no.5
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    • pp.367-372
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    • 2006
  • Electrochromic materials based on conducting polymers with pendant chromophores as well as their electrochromic properties are described. The conducting polymers described aye polypyrrole, polythiophene, poly(3,4-ethylenedioxythiophene), poly (cyclopentadithiophene), and poly (1,4-bis [2- (3,4-ethylenedioxy) thienyl] benzene). The chromophores described are viologen and perylenetetra-carboxylic diimide. When the wavelength ranges of absorption of the conducting polymer and the chromophore aye not overlapping, multiple electrochromism was achieved. When the wavelength ranges are largely overlapping, higher contrast was achieved. An easy method for prediction of the film thickness for maximum contrast of a given electrochromic material is also described.

Carotenoid, Color value, UV Spectrum, Organic Acid and Free Sugar Contents of Citrus Varieties Produced in Cheju (제주산 감귤 품종별 carotenoid, 색도, UV 스펙트럼, 유기산 및 유리당 함량)

  • 김병주;김효선
    • Food Science and Preservation
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    • v.3 no.1
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    • pp.23-32
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    • 1996
  • Total carotenoid contents, color values and spectrum characterization in the range of UV of fruit juice and organic acid and free sugar contents determined by HPLC were investigated on 10 varieties of Cheju citrus fruits. Carotenoid contents of juice were 0.47-9.20$\mu\textrm{g}$/ml which showed higher with Dangyooja while showed lowest content with Meiwa Kumquat. Lightness (L) of juice was highest in Meiwa Kumquat, and in the order of Sankyool, Navel orange and Hungjin. Redness(a) and yellowness(b) were in the order of Dangyooja, Natsudaidai, Sambokam and Kinkoji. The maximum absorption wavelengths if citrus Juices were variable at 269.5-285.5nm according to varieties and it was observed that were changed by mixing with Juices of other varieties. Major organic acids of citrus juice were citric and malic acid, and citric acid was 64.4-95.1% of total organic acids. Ascorbic acid was high in Navel orange, Sudachi and Dangyooja, and low in Meiwa Kumquat and Hungjin. Major free sugars were sucrose, glucose and fructose. Sucrose was 49.2-75.2% of total free sugars, and high in Sankyool and Meiwa Kumquat. Glucose and fructose were high in Meiwa Kumquat and Navel Orange.

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