• 제목/요약/키워드: material standardization

검색결과 233건 처리시간 0.027초

Development of Standard Operating Procedures (SOPs), Standardization, TLC and HPTLC Fingerprinting of a Polyherbal Unani Formulation

  • Naaz, Arjumand;Viquar, Uzma;Naikodi, Mohammad Abdul Rasheed;Siddiqui, Javed Inam;Zakir, Mohammad;Kazmi, Munawwar Husain;Minhajuddin, Ahmed
    • 셀메드
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    • 제11권4호
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    • pp.21.1-21.9
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    • 2021
  • Background: Unani System of Medicine (USM) has its origin to Greece. To ensure and develop the quality, authenticity of Unani drugs, standardization on modern analytical parameter is essential requirement for drugs. Objectives: The aimed of the present study was to develop a standard profile of "Qurṣ-e-Mafasil" by systematic study through authenticated ingredients, pharmacognostic identification followed by physicochemical, TLC, HPTLC fingerprinting analysis as per standard protocol. Material and Methods: In this study three batches of "Qurṣ-e-Mafasil" QM were prepared by standard method as per UPI had been followed by organoleptic properties of formulation such as appearance, color, odor, taste. Powder Microscopy and physicochemical studies were carried out such as Uniformity of weight, Friability, Disintegration time, hardness, LOD, ash vales and extractive values in like aqueous, alcohol & hexane. Further qualitative tests such as Thin-Layer Chromatography (TLC), and High-Performance Thin Layer Chromatography (HPTLC) studies were also carried out to develop fingerprint pattern of the alcoholic solvent extract of QM. Phytochemical screening was carried out in different solvent extracts such as alcoholic, aqueous and chloroform extracts to detect the presence phytoconstituents in the formulation QM. Heavy metals, Microbial Load Contamination and pesticidal residues were also determined. Results: Qurṣ-e-Mafasil showed tablet-like appearance, light brown colour, mild pungent odour and acrid taste. Uniformity of weight (mg), friability (rpm), and hardness (kg/cm) and disintegration time was ranged between (500 to 503), (0.0340 to 0.038), (8.40 to 8.67) and (4-5 minutes) respectively for the three batches. Loss in weight on drying at 105℃ was ranged between (8.3425 to 8.7346). Extracted values were calculated in distilled water ranged between (30.9091 to 31.4358), hexane (1.1419 to 1.4281), and alcohol (3.3352 to 3.3962). The ash values recorded were ranged between (3.7336 to 3.8378), and acid insoluble ash (0.5859 to 0.6112).

물류산업의 선진화를 위한 성과지표 분석: IT서비스를 중심으로 (Analysis of Key Performance Index for Advanced Logistics)

  • 장희선
    • 융합보안논문지
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    • 제13권1호
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    • pp.25-30
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    • 2013
  • 본 논문에서는 국내 물류산업의 경쟁력을 높이고 물류 선진화를 도모하기 위한 성과지표를 분석하고 세부적인 IT서비스를 제시한다. 여기서 물류 기업의 성과는 크게 효율성, 지속가능성 및 경제성 측면으로 구분하여 평가지표를 설정하고 IT서비스는 기업 및 공공물류로 분류하여 기업들에게 필요한 IT서비스를 분석한다. 아울러 사례연구로서 평택항 관련 종사자 즉, 물류기업 및 무역업, 공무원, 지역주민 등을 대상으로 실시한 설문조사 결과(SPSS 분석)를 통하여 물류기업의 현황을 진단하고 우선적으로 요구되는 물류 IT서비스의 우선순위를 조사한다. 분석결과, 물류산업의 생산성과 효율성을 높이기 위하여 전문인력의 확보와 표준화가 요구되고 시급한 IT서비스로서 물류자동화 기계화, u-Port 구축, 녹색친환경물류 그리고 물류보안 기술의 구현이 필요함을 알 수 있다.

Built-up H형강의 소재특성 및 용접성능에 관한 연구 (A Study on the Material Properties and Welding Performance of Built-up H-beam)

  • 최영한;김상섭
    • 한국강구조학회 논문집
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    • 제30권1호
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    • pp.13-23
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    • 2018
  • 단면을 자유롭게 제작할 수 있는 Built-up H형강(BH)의 사용이 점점 증대하고 있다. 본 연구는 BH의 규격화를 위한 기초연구로 SM490, SM520 강재의 항복강도, 인장강도, 연신율, 샤르피 흡수에너지 등의 소재특성을 확인하였다. 또한 single-SAW 및 tandem-SAW를 활용하여 6개의 BH 공시체를 제작하였으며, 공시체에서 매크로시험편, T바 인장실험체를 채취하여 용접성능을 확인하였다. 소재특성시험 결과 국내산 SM490, SM520 강재의 특성은 모두 KS를 만족하였으며, 용접성능실험 결과 BH의 용접부는 충분한 용접성능을 갖추었다고 판단할 수 있다. 따라서 본 연구에서 사용된 국내산 SM490, SM520 강재는 BH의 소재로 적합한 것으로 판단되며, single-SAW, tandem-SAW는 충분한 용접성능을 발휘하는 것으로 사료된다.

고온초전도 coated conductor의 임계전류 측정 표준화 연구 I (A study of standardizing Critical-Current Measurements for coated conductor I)

  • 오상수;이남진;김호섭;염도준
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2009년도 하계학술대회 논문집
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    • pp.363-364
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    • 2009
  • 본 연구는 IEC/TC 90 규격을 참조하여 Cu stabilizer/Ag/$LaMnO_3$/IBAD-MgO/$Y_2O_3$/$Al_2O_3$/Hastelloy C276/Cu stabilizer의 구조를 가지는 coated conductor의 DC 임계 전류의 결정에 대한 사전 연구를 위해 (1) 시편의 냉각시간, (2) 전류 선의 용량을 변화하여 임계 전류의 변화를 관찰하여 다음과 같은 결과를 얻었다. (1) 5분 이상의 시편 냉각시간은 COV가 약 0.4% 정도로 거의 임계 전류 결정에 영향을 주지 않았으며, 냉각 시간이 길면 길수록 임께 전류 이하에서 전압의 기저면이 낮아지는 경향을 보였다. (2) 전류 선의 용량이 클수록 임계 전류 이하에 전압의 기저면이 낮아지는 경향을 보였다.

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Cold Room을 이용한 얼음 및 동토의 재료특성 계측 실험기법의 표준화 (Standardization of Ice Mechanics Experimental Procedures in a Cold Room)

  • 김정현;최경식;서영교
    • 한국해양공학회지
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    • 제21권2호
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    • pp.60-66
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    • 2007
  • The first Korean cold room facility for ice mechanics experiments was assembled in 2004. Since then, the $4m{\times}6m$ cold room facility has been used, extensively under various environmental and loading conditions. After reviewing published references on cold room testing methods and also by trial and error, the standard procedures for testing and preparing laboratory ice material were established for the measurement of basic ice properties. In this paper, laboratory experimental techniques with the cold room facility and standard procedures established for ice material properties are introduced. Test specimens include laboratory-grown fresh water ice and frozen soils. Tests are carried out for unconfined compressive strength. Preparation and dimension of the specimen are the most important issues arising in cold room tests. The details of specimen preparation, testing procedure and strength test results are also discussed.

극후판 Box-Column의 Lamellar 균열 감수성 평가 (Sensitivity Appraisal for Lamellar Tearing of Box-Column of Ultra Thick Plate)

  • 노찬승;박창수;김흥주;방한서;이창우
    • 한국해양공학회지
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    • 제17권4호
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    • pp.31-36
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    • 2003
  • In case of this thick rolling-steel for a multistory building, a large oil-drilling structure, a large vessel, a bridge and so on, Lamella Tearing around the welded joint zone is the most serious problems. In order to prevent Lamella Tearing, not only is choice of material important, but also the comprehensive investigation for the structural design and the construction. The Lamella Tearing that is a staircase-shape occurs due to the contraction stress to the thickness direction of the plate and has the character that the cracks progress along the elongated inclusion by rolling. In general, because cracks occur at the heat affected zone and around HAZ, it is necessary to establish the safety and the confidence of the welded structure to restrain the welding defect such as Lamella Tearing. The mechanical approaches are the easier and more economical than the approaches of the material and the construction method. In addition, the appropriate welding profile and the optimum welding condition contribute toward the improvement of the productivity and influence on the standardization of the manufacturing technology.

국제적(國際的) 건축(建築) 전문교육(專門敎育) 인증기준(認證基準)에서 본 한국(韓國) 건축교육(建築敎育)의 현황분석(現況分析) (A Critical Analysis on the Architectural Education in Korea from the view of International Accrediting Criteria)

  • 류전희;이선영
    • 건축역사연구
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    • 제8권3호
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    • pp.75-89
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    • 1999
  • Under the WTO system, global standardization of professionalism in architecture practice calls for transformation of curriculum in architectural education in Korea. This paper compares the curriculum standards of international accrediting authorities such as NAAB and RIBA based on UIA accord which defines fundamental knowledge and abilities of an architect. As a result this paper extracts 51 achievement oriented criteria of architectural education in Korea. It can be categorized as communication, design, cultural context(history and theory, human behavior and social aspects), technical systems(structural systems, environmental control systems, construction material and assemblies) and practice(project process, project economics and business management, laws and regulations). Based on this recommended Korean curriculum standards, current curriculum is analyzed focusing on the 5 architectural programs in Seoul. Through this analysis, it became clear that some area - social and economic aspects in architecture, sustainability in architecture, understanding and selection of construction material, assemblies and environmental control system, recycling of existing building, professional liability, professional rules of conduct, project economics and project management - need to be covered and emphasized to meet the international standards in professional education in architecture. The result in this paper will be used as a basic data in the process of finding the direction of restructuring curriculum for professional architectural education in Korea.

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154 kV XLPE 전력케이블의 부분방전 측정을 위한 FSA의 적용 및 표준화 연구 (A Study on FSA Application and Standardization for Partial Discharge Measurement of 154 kV XLPE Cable)

  • 신동훈;;양종석;황두현;임종천;박노준;박대희
    • 한국전기전자재료학회논문지
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    • 제20권5호
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    • pp.462-466
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    • 2007
  • The measuring system of the Partial discharge(PD) is very essential to investigate the hazard defects in the insulation systems of the high voltage engineering. We will discussed this research which has included two parts. The proposed method of Foil Sensor Array(FSA) and the normally used method in the practice. Firstly, it will be shown the improved sensitivity of a FSA sensor, which is our aim, compare with the existing normal foil sensor. And then, the linearity of detecting sensitivities of various kinds of FSA sensors was shown. According to our experiments, we can see that FSA sensor is more sensitivity than normal foil sensor and the linear increment property of FSA sensitivities.

BIM 템플릿 개발을 위한 템플릿 구성요소 분석에 관한 연구 (A Study on Analysis of the Template Component for the Development of BIM Template)

  • 이상헌;김미경;최현아;전한종
    • KIEAE Journal
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    • 제11권2호
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    • pp.123-130
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    • 2011
  • BIM based design methodology requires more information than traditional design methodology in order to insure efficiency throughout the project. BIM based design not only requires all building data in the form of 3D shapes, but also all other relevant data regarding building components. Information is typically grouped in a standard classification system such as by standardized material names. The development of a domestic BIM based standard classification system is yet to be created and deployed in the industry. Each designer is specifying their own building information classification systems which is causing inconsistency in the industry. Therefore BIM based designs, are causing confusion in the industry as each designer follow no guidelines for material standardization classification. The lack of information regarding this in the BIM template will continue to cause confusion about a projects building information data consistently. This study is that of preliminary research to develop a BIM template. First, overseas BIM templates were analyzed regarding BIM standards and documentation. Examination then followed regarding the element and characteristics needed for the development of a BIM template, a suggested hierarchy of elements required for a BIM template were then made. The result of this research is that it will be used to develop a "BIM template prototype", to support the generation of building information data regarding neighborhood facilities.

GIS 공간 분석기법을 통한 철도사고위험물질별 피해규모 자동추출방안 (A Method to Measure Damage Areas by the types of Railroad Hazardous Material through GIS Spatial Analysis)

  • 김상균;김시곤;이원태
    • 한국철도학회:학술대회논문집
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    • 한국철도학회 2009년도 춘계학술대회 논문집
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    • pp.1769-1778
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    • 2009
  • 산업의 발달 및 도시화의 증가로 인해 위험물질을 포함한 물류 수송량은 날로 증가하는 추세이고 위험물질 수송차량들의 사고발생 위험도 따라서 증대되고 있다. 본 연구에서는 위험물 운송이 점차 증가하고 있는 철도수송에 있어 기존 선행 연구의 피해규모 분석모형을 적용하고, 위험물 물류 표준화 연구에서 정의된 물질별 사고노출량을 기준으로 하여 위험물 물질별 인구 및 환경 노출규모를 GIS(Geographic Information System)의 버퍼링 분석 기 법을 통하여 일반적으로 분석이 어려운 피해규모산정을 자동으로 도출하는 방안을 제시하였다. 각 링크별 인구 및 노출규모 산출 모형을 적용하기 위해서는 Network(철도망), Zone(행정구역), 철도사고 Data, 철도화물 통행량, 하천 및 강 등을 GIS Database로 구축하였고, 최종적으로 Buffering 분석과 함께, 중첩분석의 Clip 기법과 Special Join 기법을 함께 사용하여 본연구의 제시한 위험물 물질별 피해규모 자동 추출 방안을 제시해 보았다.

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