• 제목/요약/키워드: material softening

검색결과 284건 처리시간 0.03초

PDP의 격벽 형성 공정인 감광성 공법에서 $B_2O_3-Al_2O_3-SiO_2$계 유리 조성의 열적 특성과 굴절률 변화 (Thermal Properties and Refractive Index of $B_2O_3-Al_2O_3-SiO_2$ Glasses for Photolithographic Process of Barrier Ribs in PDP)

  • 황성진;원주연;김형순
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2008년도 추계학술대회 논문집 Vol.21
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    • pp.321-321
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    • 2008
  • To obtaingood resolution in PDP, one of the important factors is to achieve the accuracy of barrier ribs. The photolithographic process can be used to form patterns of barrier rib with high accuracy and a high aspect ratio. The composition for photolithography is based on the $B_2O_3-SiO_2-Al_2O_3$ glass system including additives such as alkali oxides and alkali earth oxides. The refractive index and thermal properties in glass system are changed by amount of alkali oxides and alkali earth oxides. Therefore, it is important that additives are controlled to have proper refractive index and thermal properties. The additives are contributed to non-bridging oxygen within the glass network, causing a change of density. In addition to a change of the structural cross-link density, the refractive index, dielectric and thermal properties glass are correlated with ionic radius and polarizability of cations. In this study, we investigated the refractive index and the thermal properties such as glass transition temperature, glass softening temperature and coefficient of thermal expansion by changing composition in the $B_2O_3-SiO_2-Al_2O_3$ glass system.

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SHPB 기법을 사용한 고온에서의 Al 7075-T6 의 동적 변형 거동 (Characterization of Dynamic Deformation Behavior of Al 7075-T6 at High Temperature by Using SHPB Technique)

  • 이억섭;박진수;최혜빈;김홍민
    • 대한기계학회논문집A
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    • 제34권8호
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    • pp.981-987
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    • 2010
  • Split Hopkinson Pressure Bar(SHPB) 실험기법은 고변형률 하중 조건하에서 변형하는 여러 가지 공업 재료의 변형 거동 특성을 규명하는데 가장 널리 사용되는 실험 방법 중의 하나이다. 본 논문에서는 봉을 통하여 전파하는 응력파의 모양과 라이징 시간을 제어할 수 있는 pulse shaper를 사용하는 수정 SHPB 실험기법을 이용하였다. 수정 SHPB 실험 장치에 고온 장치를 부착하고 알루미늄 합금 7075-T6의 고변형률 하에서의 고온 변형거동에 대한 연구를 수행하였다. 고온 수정 SHPB 실험 장치를 이용하여 알루미늄 합금 7075-T6의 온도와 변형률속도에 따른 기계적 특성을 규명하고, 실험적으로 얻어진 데이터를 Johnson-Cook 구성방정식을 적용하여 알루미늄 합금 7075-T6의 동적 거동을 모델 하는 변수를 결정하였다.

PAAS LB 박막의 열자격 변위 전류에 관한 연구 (A study on the thermally-stimulated displacement current(TSDC) of the PAAS Langmuir-B1odgett(LB) films)

  • 이호식;김상걸;송민종;최명규;이원재;김태완;강도열
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2000년도 제2회 학술대회 논문집 일렉트렛트 및 응용기술전문연구회
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    • pp.11-14
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    • 2000
  • This paper describes a thennally stimulated displacement current(TSDC) of polyamic acid alkylamine salts(PAAS) Langmuir-Blodgett(LB) films, which is a precursor of polyimide(PI). The TSDC measurements of PAAS LB film were performed from room temperature to about $250^{\circ}C$ and the temperature was increased at a rate of $0.2^{\circ}C/s$. This show that this is TSDC peaks at about $70^{\circ}C$ in the arachidic acid LB films, and at about $70^{\circ}C$ and $160^{\circ}C$ in the PAAS LB films. Results of this measurements indicate that one small peak at $70^{\circ}C$ is resulted from a softening of the alkyl group and the large peak at $160^{\circ}C$ is possibly due to dipole moment of C-O group in the PAAS molecule. We have calculated the vertical component of dipole moment of the P AAS LB film out of the TSDC curves. It shows that the dipole moment of PAAS LB film is about -40mD at $70^{\circ}C$ and about 200mD at $160^{\circ}C$ in the first measurement of TSDC. In the second measurement of TSDC of PAAS LB film after cooling down to room temperature, the TSDC peaks are almost disappeared.

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$CO_2$가스 배관용접부의 파괴인성평가에 관한 연구 (Study on the Evaluation of Fracture Toughness at Welded Zone for the Pipe Steel by $CO_2$ Gas Welding)

  • 나의균;유효선;오석형
    • 대한기계학회논문집A
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    • 제24권7호
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    • pp.1817-1825
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    • 2000
  • The purpose of this study is to examine the fracture toughness of the welded pipe from the viewpoint of FATT for the S38 and S42 steels used widely as the pipe material. Post weld heat treatment(PW HT) was carried out like following conditions: temperature of 67$0^{\circ}C$, I hour of holding time and cooling in furnace. Fracture toughness was obtained by measuring the crack opening displacement(COD) of the notched specimens over the range of temperature from -14$0^{\circ}C$ to -$25^{\circ}C$. Hardness values at fusion line near around were the highest and the microstructures at welded zone were coarsened. Regardless of the pipe materials, COD and temperature curves of the as-welds were moved toward higher temperature compared with those of the parents. However, COD and temperature curves of the PWHT specimens were positioned at lower temperature compared with those of the as-welds. The more heat input causes to decrease the COD values at the constant temperature. It was verified through the recrystallization treatment that PWHT was attributed to move toward lower temperature region considerably due to the improved plastic deformation at the same applied COD value of 0.3mm and softening effect. In case of the weldment of S38 steel, cleavage fracture was observed at -105$^{\circ}C$ unlike the structural steels, in which brittle fracture mode was generally shown at - 196$^{\circ}C$.

개량형 9Cr-1Mo 강의 열화도 평가를 위한 기계적 성질 및 초음파 특성 분석 (Analysis of Mechanical and Ultrasonic Properties for the Evaluation of Material Degradation in Modified 9Cr-1Mo Steel)

  • 현양기;원순호;이상훈;손영호;이재훈;김인배
    • 열처리공학회지
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    • 제23권4호
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    • pp.198-204
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    • 2010
  • Modified 9Cr-1Mo steels possess excellent high-temperature mechanical properties and are widely used in energy conversion industries. However, in-service materials degradation, such as softening, carbide-induced embrittlement, temper embrittlement, etc., can take place during long-term operation. Evolution of microstructure due to service exposure to high temperature has a strong effect on the performance of heat resistant steels. In case of modified 9Cr-1Mo steels, precipitation of $Fe_2Mo$-type laves phases and coarsening of $M_{23}C_6$-type carbides are the primary cause of degradation of mechanical properties such as toughness, hardness, tensile strength and creep resistance. This study was aimed at finding reliable parameter for assessing the integrity of modified 9Cr-1Mo steels. Characteristic parameters were attained between mechanical and ultrasonic properties.

콘크리트 손상 모델을 적용한 콘크리트 구조물 구조내력 해석 (Numerical Analysis of Load Carrying Capacity of RC Structures Based on Concrete Damage Model)

  • 우상균;이윤;이성태
    • 한국구조물진단유지관리공학회 논문집
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    • 제16권5호
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    • pp.121-128
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    • 2012
  • 이 논문에서는 대표적 수치해석에의 균열처리 방법으로 손상모델 기반의 분산균열모델을 체택하여 구조내력을 산정하였다. 또한 전력구 구조물의 실구조 모델링을 위해 3차원 해석방법을 택하였으며 3차원 콘크리트 구성모델로는 현재 3차원 모델중 콘크리트의 다축압축, 인장균열을 효과적으로 모사하는 미소면 모델(Microplane model)을 재료모델로 사용하여 비선형 유한요소해석을 수행하였다. SFRC의 인장연화곡선을 얻기 위해 역해석법을 사용하였으며, 역해석으로 구한 인장연화곡선이 실험결과와 아주 잘 일치함을 보였다. 하중-균열폭 관계를 입력값으로 사용한 역해석 결과와 하중-CMOD 관계를 사용한 역해석 결과는 서로 잘 일치하는 경향을 나타냈다. 이 논문에서는 실험으로부터 측정된 균열폭 데이터와 수치해석시의 손상지수와의 관계를 도출하여으며, 이와 같은 결과는 향후 균열탐사를 통한 구조물의 잔존 구조내력 산정에 적용할 수 있으리라 판단된다.

B2O3-Bi2O3-ZnO계 유리를 이용한 백색 LED용 색변환 렌즈의 광 특성 (Optical Properties of Color Conversion Lens for White LED Using B2O3-Bi2O3-ZnO Glass)

  • 채유진;이미재;김진호;황종희;임태영;정희석;이영식;김득중
    • 한국전기전자재료학회논문지
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    • 제26권8호
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    • pp.614-619
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    • 2013
  • Recently, remote phosphor is reported for white LED enhancing of phosphor efficiency compared with conventional phosphor-based W-LED. In this study, Remote phosphor was produced by screen printing coating on glass substrate with phosphor contents rated paste and heat treatment. The paste consists of phosphor, lowest softening glass frit and organic binders. Remote phosphor can be well controlled by varying the phosphor content rated paste. After mounting remote phosphor on top of blue LED chip, CCT, CRI, and luminance efficiency were measured. The measurement results showed that CCT, CRI, and luminance efficiency were 6,645, 68, and 1,16l m/W in phosphor 80 wt.% remote phosphor sintered at $600^{\circ}C$.

Langmuir-Blodgett(LB) 유기 초박막의 열자격 변위 전류에 관한 연구 (A Study on the Thermally-Stimulated Displacement Current (TSDC) of the Organic Ultra-Thin Langmuir-Blodgett(LB) Films)

  • 이호식;이원재;김태완;;강도열
    • 한국전기전자재료학회논문지
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    • 제11권8호
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    • pp.581-586
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    • 1998
  • This paper describes athermally stimulated displacement current (TSDC) of arachidic acid(AA) and polyamic acid alkylamine salts(PAAS) Langmuir-Blodgett(LB) films, which is a precursor of polyimide(PI). The TSDC measurements of AA LB film were performed from temperature to about 11$0^{\circ}C$ at a rate of 0.2$^{\circ}C$/s inside a vacuum chamber for a reference. And the TSDC measurements PAAS LB film were performed from room temperature to about 25$0^{\circ}C$ and temperature was increased at the same rate as that of AA LB film. They show that there are TSDC peaks at about 7$0^{\circ}C$ in the arachidic acid LB films, and at about 7$0^{\circ}C$ and 16$0^{\circ}C$ in the PAAs LB films. Results of these measurements indicate the one small peak at 7$0^{\circ}C$ is resulted from a softening of the alkyl group and the large peak at 16$0^{\circ}C$ is possibly due to dipole of C-O group in the PASS molecule. We have calculated the vertical component of the AA and PAAs L film out of the TSDC curves. It shows that the dipole moment of the AA LB film is about 70-mD at 7$0^{\circ}C$. And the dipole moment of PAAS LB film is about 040mD at 7$0^{\circ}C$ and about 200mD at 16$0^{\circ}C$ in the first measurement of TSDC. In the second measurement of TSDC of PASS LB film after cooling down to room temperature, the TSDC peaks are almost disappeared.

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대추 천일건조 중 세포벽 구성성분의 변화 (Changes on the Cell Wall Components of Jujube Fruits during Drying)

  • 손미애;김미현;신승렬;송준희;김광수
    • 한국식품저장유통학회지
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    • 제5권4호
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    • pp.350-354
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    • 1998
  • 대추의 연화현상을 연구하고자 건조중에 세포벽 구성성분의 변화를 조사하였다. 알코올 불용성 물질, 세포벽 및 수용성 물질의 함량은 건조 6일까지는 변화가 없었으나 건조 9일째에는 알코올 불용성 물질과 세포벽은 감소하였으나 수용성 물질은 증가하였다. 펙틴질과 헤미셀룰로오스는 건조 6일까지는 거의 변화가 없었으나 건조 P일째에는 펙틴질과 알칼리 가용성 헤미셀룰로오스가 감소한 반면 산가용성 헤미셀룰로오스는 증가하였다. 셀룰로오스는 건조 중에 증가하였다. 수용성 펙틴질은 건조 6일째까지는 뚜렷한 변화가 없었으나 건조 9일째에 현저히 증가하였다. EDTA-soluble 펙틴, 불용성 펙틴, 총 펙틴의 함량은 건조 6일째 이후에 감소하였다. 세포벽의 비섬유성 중성당은 건조 6일째까지는 뚜렷한 변화가 없었으나 arabinose와 galactose의 함량은 건조 9일에 감소하였다. 총 비섬유성 중성당도 건조 6일까지는 변화가 없었으나 9일째에는 뚜렷이 감소하였다.

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Ta 치환이 (Li0.04(Na0.54K0.46)0.96(Nb0.96-xTaxSb0.04)O3 세라믹스의 유전 및 압전 특성에 미치는 영향 (Effect of Ta Substitution on the Dielectric and Piezoelectric Properties of (Li0.04(Na0.54K0.46)0.96(Nb0.96-xTaxSb0.04)O3Ceramics)

  • 노정래;류주현
    • 한국전기전자재료학회논문지
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    • 제24권8호
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    • pp.627-631
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    • 2011
  • [ $[Li_{0.04}(Na_{0.54}K_{0.46})_{0.96}](Nb_{1-0.04-X}TaxSb_{0.04})O_3$ ]lead-free piezoelectric ceramics have been prepared by normal sintering at $1,100^{\circ}C$ for 5 h. X-ray diffraction analysis indicated that specimens demonstrate orthorhombic symmetry when $Ta\leq5$ mol%. While transforming into tetragonal symmetry when $x\geq20$ mol%. These suggest that the orthorhombic and tetragonal phases co-exist in the ceramics with 5 mol% $cm^3$. As the result of SEM images, the grain growth was decreased with the increase of Ta substitution. The ceramics become 'softening', leading to improvements in $k_p$, $\varepsilon_r$ and $d_{33}$, but a decrease in $Q_m$. Excellent properties of $k_p$= 0.46, $d_{33}$= 293 pC/N, ${\varepsilon}_r$= 1,583 and Tc= $340^{\circ}C$ were obtained when Ta= 15 mol%.