• 제목/요약/키워드: material softening

검색결과 284건 처리시간 0.026초

강소성변형된 미세립 AM60 마그네슘 합금의 피로거동 (Fatigue Behavior of Fine Grained AM60 Magnesium Alloy Produced by Severe Plastic Deformation)

  • 유인동;이만석;김호경
    • 한국안전학회지
    • /
    • 제27권3호
    • /
    • pp.15-19
    • /
    • 2012
  • The fatigue behavior of AM60 magnesium alloy produced by equal channel angular pressing(ECAP) process was investigated through fatigue lifetime and fatigue crack propagation rate tests. The grain structure of the material was refined from 19.2 ${\mu}m$ to 2.3 ${\mu}m$ after 6 passes of ECAP at 493 K. The yield strength(YS) and ultimate tensile strength (UTS) increase after two passes but decrease with further pressing, although the grain size becomes finer with increasing pass number. The softening effect due to texture anisotropy overwhelmed the strengthening effect due to grain refinement after 2 passes. A large enhancement in fatigue strength was achieved after two ECAP passes. The current finding suggests that two passed material is better than the multi-passed material in view of the static strength and fatigue performance.

탄소분말을 함유한 도전성 고분자 PTCR의 전기적 특성 (Electrical properties of conducting polymer PTCR containing carbon powders)

  • 김경종;이재원;김영혁;김성훈;최문석;이재신
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2006년도 하계학술대회 논문집 Vol.7
    • /
    • pp.220-221
    • /
    • 2006
  • We investigated the electrical properties of polymer-carbon composite materials for temperature sensitive resistor applications. Cu/polymer/Cu sheets were fabricated by laminating low density polyethylene(LDPE) containing carbon powders. Weight ratio of carbon powder to LDPE was varied in a range of 0.9~2. With increasing the carbon concentration, the electrical resistance of the composite material was decreased from 0.75 to $0.08\;{\Omega}cm$. The composite layer showed a abrupt increase in the electrical resistance at $115^{\circ}C$ because of the softening of the polymer.

  • PDF

Low-cycle fatigue evaluation for girth-welded pipes based on the structural strain method considering cyclic material behavior

  • Lee, Jin-Ho;Dong, Pingsha;Kim, Myung-Hyun
    • International Journal of Naval Architecture and Ocean Engineering
    • /
    • 제12권1호
    • /
    • pp.868-880
    • /
    • 2020
  • One of the main concerns in the structural integrity of offshore pipelines is mechanical damage from external loads. Pipelines are exposed to fatigue failure in welded joints due to geometric discontinuity. In addition, fatigue loads such as currents, waves, and platform motions may cause significant plastic deformation and fracture or leakage within a relatively low-cycle regime. The 2007 ASME Div. 2 Code adopts the master S―N curve for the fatigue evaluation of welded joints based on the mesh-insensitive structural stress. An extension to the master S―N curve was introduced to evaluate the low-cycle fatigue strength. This structural strain method uses the tensile properties of the material. However, the monotonic tensile properties have limitations in describing the material behavior above the elastic range because most engineering materials exhibit hardening or softening behavior under cyclic loads. The goal of this study is to extend the cyclic stress-strain behavior to the structural strain method. To this end, structural strain-based procedure was established while considering the cyclic stress-strain behavior and compared to the structural strain method with monotonic tensile properties. Finally, the improved prediction method was validated using fatigue test data from full-scale girth-welded pipes.

국내산 소나무로 제조되는 열기계펄프 제조 기술 최적화 연구 (1) - 목재 칩의 전처리와 리파이닝 시 온도와 NaOH 처리의 효과 - (Optimization Technology of Thermomechanical Pulp Made from Pinus densiflora (I) - Effect of Temperature and NaOH at Presteaming and Refining -)

  • 남혜경;김철환;이지영;박형훈;권솔;조후승;이경선
    • 펄프종이기술
    • /
    • 제47권1호
    • /
    • pp.35-44
    • /
    • 2015
  • Thermomechanical pulping process uses large amounts of energy, mostly electricity to run electrical facilities. Thermomechanical pulp (TMP) made from Pinus densiflora also has a big drawback that refining consumes 90 per cent of the total energy used in TMP process. This study explored to draw up a way to save refining energy through different thermal treatment at the stages of presteaming and refining. Presteaming temperature was $80^{\circ}C$, $100^{\circ}C$, and $120^{\circ}C$. After presteaming at each temperature, refining was carried out at $100^{\circ}C$, $120^{\circ}C$, and $140^{\circ}C$ respectively. In a presteaming stage, steaming temperature over $120^{\circ}C$ greatly contributed to the decrease of refining energy leading to earlier attainment of a target freeness, irrespective of refining temperature. In addition, NaOH treatment with presteaming enhanced better development of fiber properties during refining than presteaming without NaOH. High temperature refining at $140^{\circ}C$ produced a high strength paper, and wood chips treated by alkali responded better to refining than at over $120^{\circ}C$. Improved softening effect on wood chips led to the decrease in shives contents but it gave no effect on pitch contents of TMP.

지르코니아 함량에 따른 내알칼리 유리섬유의 특성 (The properties of AR(Alkali Resistant)-glass fiber by zirconia contents)

  • 이지선;임태영;이미재;황종희;김진호;현승균
    • 한국결정성장학회지
    • /
    • 제25권6호
    • /
    • pp.263-271
    • /
    • 2015
  • 기존의 내알칼리 유리섬유는 복합재료의 보강섬유로 가장 널리 사용되고 있는 일반적인 E-glass fiber보다 우수한 내화학 특성을 갖고 있으나 용융유리의 점도가 너무 높아 섬유화가 어려운 문제점을 가지고 있다. 본 연구에서는 지르코니아 함량이 상용 제품에 비해 낮은 범위에서 지르코니아 함량별로 내알칼리유리섬유를 제조하고 이들의 특성을 E-glass 섬유와 비교하였다. 지르코니아의 함량을 0.5~16 wt%까지 변화시키면서 제조한 각각의 배치원료를 $1600^{\circ}C$에서 2시간 용융하여 투명하고 맑은 유리를 얻을 수 있었다. 이들 유리는 약 90 %의 높은 가시광 투과율을 나타내었고, 열적특성에서 $703{\sim}887^{\circ}C$의 연화점을 나타내었으며, 지르코니아의 함량이 증가함에 따라 연화점이 상승하는 경향을 나타내었다. 지르코니아 함량이 4 wt%인 조성을 E-glass 조성과 비교한 결과, 연화점에서는 $-94^{\circ}C$의 차이를, 고온점도에 있어서는 log3 온도가 $+68^{\circ}C$, log5 온도가 $-13^{\circ}C$의 차이를 나타내었다. 내알칼리 유리섬유를 알칼리용액에 48시간 및 72시간 침적 후 SEM을 통해 섬유의 내침식성이 양호함을 확인할 수 있었고, 인장강도도 일반 E-glass 섬유에 비해 48시간에서 1.7배와 72시간에서 2.2배의 높은 값을 나타냄을 알 수 있었다. 결론적으로 이러한 내알칼리 유리섬유는 쉬운 제조조건과 낮은 지르코니아 함량에도 불구하고 좋은 특성 때문에 일반적인 내알칼리 유리섬유로서 널리 사용될 수 있을 것으로 판단되었다.

Effect of Lu3Al5O12:Ce3+ and (Sr,Ca)AlSiN3:Eu2+ Phosphor Content on Glass Conversion Lens for High-Power White LED

  • Lee, Hyo-Sung;Hwang, Jong Hee;Lim, Tae-Young;Kim, Jin-Ho;Jeon, Dae-Woo;Jung, Hyun-Suk;Lee, Mi Jai
    • 한국세라믹학회지
    • /
    • 제52권4호
    • /
    • pp.229-233
    • /
    • 2015
  • Currently, the majority of commercial white LEDs are phosphor converted LEDs made of a blue-emitting chip and YAG yellow phosphor dispersed in organic silicone. However, silicone in high-power devices results in long-term performance problems such as reacting with water, color transition, and shrinkage by heat. Additionally, yellow phosphor is not applicable to warm white LEDs that require a low CCT and high CRI. To solve these problems, mixing of green phosphor, red phosphor and glass, which are stable in high temperatures, is common a production method for high-power warm white LEDs. In this study, we fabricated conversion lenses with LUAG green phosphor, SCASN red phosphor and low-softening point glass for high-power warm white LEDs. Conversion lenses can be well controlled through the phosphor content and heat treatment temperature. Therefore, when the green phosphor content was increased, the CRI and luminance efficiency gradually intensified. Moreover, using high heat treatment temperatures, the fabricated conversion lenses had a high CRI and low luminance efficiency. Thus, the fabricated conversion lenses with green and red phosphor below 90 wt% and 10 wt% with a sintering temperature of $500^{\circ}C$ had the best optical properties. The measured values for the CCT, CRI and luminance efficiency were 3200 K, 80, and 85 lm/w.

고온 (750 ~ 850℃) SOFC용 밀봉재의 특성에 미치는 고열팽창계수를 갖는 필러의 영향 (The Effects of a Filler with a High Coefficient of Thermal Expansion on a Sealant for High-Temperature (750 ~ 850℃) SOFCs)

  • 김빛남;이미재;황종희;임태영;김진호;황해진;김일원;정운진
    • 한국세라믹학회지
    • /
    • 제50권6호
    • /
    • pp.470-475
    • /
    • 2013
  • In this study, we report that effects of a filler with a high coefficient of thermal expansion on a sealant for high-temperature ($750{\sim}850^{\circ}C$) SOFC. We designed a $SiO_2-BaO-ZnO-B_2O_3-Al_2O_3$ glass system with a softening temperature higher than $750^{\circ}C$. The properties of the glass system show not only low volumetric shrinking but also low swelling. The glass system did not create a crystal phase during along-term heat treatment. We fabricated a seal gasket with 0, 10, 15, and 20 wt% cristobalite added as filler materials with glass powder. The coefficient of thermal expansion of the seal gasket increased according to cristobalite content. During along-term heat treatment, the leak rate decreased by about 5% after a heat treatment in an oxidizing atmosphere at $750^{\circ}C$ for 2000 h, also decreasing by about 6% after a heat treatment in a reducing atmosphere at $750^{\circ}C$ for 1000 h.

전기화학적 분극법에 의한 1.0Cr-0.5Mo강의 경년열화 평가에 관한 연구 (A study on the evaluation for material degradation of 0.0Cr-0.5Mo steel by a electrochemical polarization method)

  • 나의균;김훈;이종기
    • 대한기계학회논문집A
    • /
    • 제22권1호
    • /
    • pp.177-189
    • /
    • 1998
  • The contents of this paper include a non-destructive technique for evaluating the degradation of the boiler superheater tube in a fossil power plant through an electrochemical polarization test. Correlation between Ip of polarization parameter and SP-DBTT for the superheater tubes in long-term use was obtained. 1.0Cr-0.5Mo steel was degraded by softening, and the degree of degradation was dependent upon carbides with Cr and Mo elements. Since brittle fracture at low temperature and ductile fracture mode at high temperature were shown, similarity between standard Charpy and small punch tests could be found. In addition, SP-DBTT showing the degree of degradation was higher, as the time-in use of the materials got longer. Electrolyte including picric acid of 1.3 g in distilled water of 100ml at 25.deg. C temperature and sodium tridecylbenzene sulfonate with 1g could be applied to evaluate the degradation of 1.0Cr-0.5Mo steel by means of the electrochemical polarization test. Ip and Ipa values measured through the electrochemical test are the appropriate parameters for representing the degradation of the superheater tube(1.0Cr-0.5Mo steel) for the fossil power plant. It is poassible to evaluate the degradation of materials with different time histories electrochemically, by Ip value only, at field test.

PDP용 Ag전극 페이스트의 Bi계 프릿 제조 및 특성 (Preparation and Characterization of Bi based frit for Ag Electrode in PDP Application)

  • 김형수;최정철;이병옥;최승철
    • 마이크로전자및패키징학회지
    • /
    • 제10권4호
    • /
    • pp.47-52
    • /
    • 2003
  • PDP전극용 Ag전극 페이스트의 프릿으로 기존의 Pb-based 프릿을 대신 할 수 있는 Bi-based 조성의 새로운 유리조성의 가능성을 검토하였다. PDP디스플레이 응용을 위해 프릿의 저융점화 및 열팽창계수 제어를 행하였고, 이를 전극 페이스트 제조에 적용하여 스크린 프린팅된 전극을 평가하였다. $Bi_2O_3$를 50-60wt%이상 첨가된 $Bi_2O_3-B_2O_3-Al_2O_3$계 조성의 프릿은 연화점이 400∼$480^{\circ}C$, 열팽창계수가 7.31∼$10.02\times 10^{-6}/^{\circ}C$이며, 전극의 단자저항은 4.1∼4.8$\Omega$ 이었다. 본 연구에서 새로이 개발된 Bi계 프릿조성은 Pb계 조성의 프릿에 상당하는 물성을 얻을 수 있었으며, 이를 전극용 페이스트에 적용한 결과, 전극 프린팅에서 퍼짐성과 균일성이 우수하였다. PDP전극용 무연, 무 알카리 프릿으로 Bi계 조성의 적용가능성을 확인할 수 있었다.

  • PDF

페라이트기 11Cr 저탄소강의 자기적 특성에 대한 고온 장시간 시효열화 효과 (Effect of Long-Term Aging Degradation on Magnetic Properties of Ferritic 11Cr Low-Carbon Steel)

  • 김정석;류권상
    • 비파괴검사학회지
    • /
    • 제36권5호
    • /
    • pp.377-383
    • /
    • 2016
  • 페라이트기 11Cr 저탄소강의 자기적 특성에 대한 고온 장시간 시효열화의 영향에 대해서 연구하였다. 장시간 시효시간이 증가함에 따라서 자기이력곡선으로부터 구한 보자력, 자기이력손실은 감소하였고 이들은 시효시간에 대해 2차 지수함수 관계를 나타내었다. 비커스 경도 역시 시효시간의 증가에 따라서 감소하여 기계적 물성의 연화를 나타내었다. 미세조직적 분석으로 주사전자현미경, 후방산란전자 및 X-선 회절시험을 수행하였다. 입계에서는 $Cr_{23}C_6$ 석출물의 급격한 성장과 입내의 래스 경계부에서 Laves ($Fe_2W$)상이 발달하였다. 조대한 석출물들로 인해 장시간 시효열화에 따라서 고용원소의 고갈과 래스 하부조직이 소멸되었다. 이는 자기적 물성과 기계적 물성의 연화현상과 밀접한 관련을 갖게 된다.