• Title/Summary/Keyword: material softening

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Thermal Properties and Refractive Index of $B_2O_3-Al_2O_3-SiO_2$ Glasses for Photolithographic Process of Barrier Ribs in PDP (PDP의 격벽 형성 공정인 감광성 공법에서 $B_2O_3-Al_2O_3-SiO_2$계 유리 조성의 열적 특성과 굴절률 변화)

  • Hwang, Seong-Jin;Won, Ju-Yeon;Kim, Hyung-Sun
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.11a
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    • pp.321-321
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    • 2008
  • To obtaingood resolution in PDP, one of the important factors is to achieve the accuracy of barrier ribs. The photolithographic process can be used to form patterns of barrier rib with high accuracy and a high aspect ratio. The composition for photolithography is based on the $B_2O_3-SiO_2-Al_2O_3$ glass system including additives such as alkali oxides and alkali earth oxides. The refractive index and thermal properties in glass system are changed by amount of alkali oxides and alkali earth oxides. Therefore, it is important that additives are controlled to have proper refractive index and thermal properties. The additives are contributed to non-bridging oxygen within the glass network, causing a change of density. In addition to a change of the structural cross-link density, the refractive index, dielectric and thermal properties glass are correlated with ionic radius and polarizability of cations. In this study, we investigated the refractive index and the thermal properties such as glass transition temperature, glass softening temperature and coefficient of thermal expansion by changing composition in the $B_2O_3-SiO_2-Al_2O_3$ glass system.

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Characterization of Dynamic Deformation Behavior of Al 7075-T6 at High Temperature by Using SHPB Technique (SHPB 기법을 사용한 고온에서의 Al 7075-T6 의 동적 변형 거동)

  • Lee, Ouk-Sub;Park, Jin-Su;Choi, Hye-Bin;Kim, Hong-Min
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.34 no.8
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    • pp.981-987
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    • 2010
  • The split Hopkinson pressure bar (SHPB) technique is extensively used to characterize material deformation behavior under high strain rate condition. In this study, the dynamic deformation behavior of aluminum 7075-T6 under a high strain rate and at a high temperature is investigated by using a modified SHPB set-up with the pulse shaper technique. The parameters used in the Johnson-Cook constitutive equation are determined by using the SHPB experimental results including the data on the effects of strain rate, temperature, strain hardening, and thermal softening of the material.

A study on the thermally-stimulated displacement current(TSDC) of the PAAS Langmuir-B1odgett(LB) films (PAAS LB 박막의 열자격 변위 전류에 관한 연구)

  • Lee, Ho-Sik;Kim, Sang-Keol;Song, Min-Jong;Choi, Myung-Kyue;Lee, Won-Jae;Kim, Tae-Wan;Kang, Dou-Yol
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.10a
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    • pp.11-14
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    • 2000
  • This paper describes a thennally stimulated displacement current(TSDC) of polyamic acid alkylamine salts(PAAS) Langmuir-Blodgett(LB) films, which is a precursor of polyimide(PI). The TSDC measurements of PAAS LB film were performed from room temperature to about $250^{\circ}C$ and the temperature was increased at a rate of $0.2^{\circ}C/s$. This show that this is TSDC peaks at about $70^{\circ}C$ in the arachidic acid LB films, and at about $70^{\circ}C$ and $160^{\circ}C$ in the PAAS LB films. Results of this measurements indicate that one small peak at $70^{\circ}C$ is resulted from a softening of the alkyl group and the large peak at $160^{\circ}C$ is possibly due to dipole moment of C-O group in the PAAS molecule. We have calculated the vertical component of dipole moment of the P AAS LB film out of the TSDC curves. It shows that the dipole moment of PAAS LB film is about -40mD at $70^{\circ}C$ and about 200mD at $160^{\circ}C$ in the first measurement of TSDC. In the second measurement of TSDC of PAAS LB film after cooling down to room temperature, the TSDC peaks are almost disappeared.

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Study on the Evaluation of Fracture Toughness at Welded Zone for the Pipe Steel by $CO_2$ Gas Welding ($CO_2$가스 배관용접부의 파괴인성평가에 관한 연구)

  • Na, Ui-Gyun;Yu, Hyo-Seon;O, Seok-Hyeong
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.24 no.7 s.178
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    • pp.1817-1825
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    • 2000
  • The purpose of this study is to examine the fracture toughness of the welded pipe from the viewpoint of FATT for the S38 and S42 steels used widely as the pipe material. Post weld heat treatment(PW HT) was carried out like following conditions: temperature of 67$0^{\circ}C$, I hour of holding time and cooling in furnace. Fracture toughness was obtained by measuring the crack opening displacement(COD) of the notched specimens over the range of temperature from -14$0^{\circ}C$ to -$25^{\circ}C$. Hardness values at fusion line near around were the highest and the microstructures at welded zone were coarsened. Regardless of the pipe materials, COD and temperature curves of the as-welds were moved toward higher temperature compared with those of the parents. However, COD and temperature curves of the PWHT specimens were positioned at lower temperature compared with those of the as-welds. The more heat input causes to decrease the COD values at the constant temperature. It was verified through the recrystallization treatment that PWHT was attributed to move toward lower temperature region considerably due to the improved plastic deformation at the same applied COD value of 0.3mm and softening effect. In case of the weldment of S38 steel, cleavage fracture was observed at -105$^{\circ}C$ unlike the structural steels, in which brittle fracture mode was generally shown at - 196$^{\circ}C$.

Analysis of Mechanical and Ultrasonic Properties for the Evaluation of Material Degradation in Modified 9Cr-1Mo Steel (개량형 9Cr-1Mo 강의 열화도 평가를 위한 기계적 성질 및 초음파 특성 분석)

  • Hyun, Y.K.;Won, S.H.;Lee, S.H.;Son, Y.H.;Lee, J.H.;Kim, I.B.
    • Journal of the Korean Society for Heat Treatment
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    • v.23 no.4
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    • pp.198-204
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    • 2010
  • Modified 9Cr-1Mo steels possess excellent high-temperature mechanical properties and are widely used in energy conversion industries. However, in-service materials degradation, such as softening, carbide-induced embrittlement, temper embrittlement, etc., can take place during long-term operation. Evolution of microstructure due to service exposure to high temperature has a strong effect on the performance of heat resistant steels. In case of modified 9Cr-1Mo steels, precipitation of $Fe_2Mo$-type laves phases and coarsening of $M_{23}C_6$-type carbides are the primary cause of degradation of mechanical properties such as toughness, hardness, tensile strength and creep resistance. This study was aimed at finding reliable parameter for assessing the integrity of modified 9Cr-1Mo steels. Characteristic parameters were attained between mechanical and ultrasonic properties.

Numerical Analysis of Load Carrying Capacity of RC Structures Based on Concrete Damage Model (콘크리트 손상 모델을 적용한 콘크리트 구조물 구조내력 해석)

  • Woo, Sang Kyun;Lee, Yun;Yi, Seong Tae
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.16 no.5
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    • pp.121-128
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    • 2012
  • In this paper, nonlinear analysis for reinforced concrete structure for power transmission line is performed by considering the characteristics of the failure, which are depend on loading conditions and concrete material models. On the numerical evaluation for the failure behavior, the finite element analysis is applied. For the concrete material model, microplane model based on concrete damage is introduced. However, to describe the crack bridging effect of long and short fiber of steel fiber reinforced concrete (SFRC), tensile softening model is suggested and applied for SFRC. An numerical results by finite element technique are compared with the experiment results for box culvert specimen. Comparing on the experimental and analytical results, validity and reliability of numerical analysis are investigated.

Optical Properties of Color Conversion Lens for White LED Using B2O3-Bi2O3-ZnO Glass (B2O3-Bi2O3-ZnO계 유리를 이용한 백색 LED용 색변환 렌즈의 광 특성)

  • Chae, Yoo-Jin;Lee, Mi-Jai;Kim, Jin-Ho;Hwang, Jong-Hee;Lim, Tae-Young;Jeong, Hee-Suk;Lee, Young-Sik;Kim, Deuk-Jung
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.26 no.8
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    • pp.614-619
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    • 2013
  • Recently, remote phosphor is reported for white LED enhancing of phosphor efficiency compared with conventional phosphor-based W-LED. In this study, Remote phosphor was produced by screen printing coating on glass substrate with phosphor contents rated paste and heat treatment. The paste consists of phosphor, lowest softening glass frit and organic binders. Remote phosphor can be well controlled by varying the phosphor content rated paste. After mounting remote phosphor on top of blue LED chip, CCT, CRI, and luminance efficiency were measured. The measurement results showed that CCT, CRI, and luminance efficiency were 6,645, 68, and 1,16l m/W in phosphor 80 wt.% remote phosphor sintered at $600^{\circ}C$.

A Study on the Thermally-Stimulated Displacement Current (TSDC) of the Organic Ultra-Thin Langmuir-Blodgett(LB) Films (Langmuir-Blodgett(LB) 유기 초박막의 열자격 변위 전류에 관한 연구)

  • ;;;M. lwamoto
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.11 no.8
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    • pp.581-586
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    • 1998
  • This paper describes athermally stimulated displacement current (TSDC) of arachidic acid(AA) and polyamic acid alkylamine salts(PAAS) Langmuir-Blodgett(LB) films, which is a precursor of polyimide(PI). The TSDC measurements of AA LB film were performed from temperature to about 11$0^{\circ}C$ at a rate of 0.2$^{\circ}C$/s inside a vacuum chamber for a reference. And the TSDC measurements PAAS LB film were performed from room temperature to about 25$0^{\circ}C$ and temperature was increased at the same rate as that of AA LB film. They show that there are TSDC peaks at about 7$0^{\circ}C$ in the arachidic acid LB films, and at about 7$0^{\circ}C$ and 16$0^{\circ}C$ in the PAAs LB films. Results of these measurements indicate the one small peak at 7$0^{\circ}C$ is resulted from a softening of the alkyl group and the large peak at 16$0^{\circ}C$ is possibly due to dipole of C-O group in the PASS molecule. We have calculated the vertical component of the AA and PAAs L film out of the TSDC curves. It shows that the dipole moment of the AA LB film is about 70-mD at 7$0^{\circ}C$. And the dipole moment of PAAS LB film is about 040mD at 7$0^{\circ}C$ and about 200mD at 16$0^{\circ}C$ in the first measurement of TSDC. In the second measurement of TSDC of PASS LB film after cooling down to room temperature, the TSDC peaks are almost disappeared.

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Changes on the Cell Wall Components of Jujube Fruits during Drying (대추 천일건조 중 세포벽 구성성분의 변화)

  • 손미애;김미현;신승렬;송준희;김광수
    • Food Science and Preservation
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    • v.5 no.4
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    • pp.350-354
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    • 1998
  • This paper was investigated to changes of cell components during drying for studies on the softening of jujube fruits. The contents of alcohol-insoluble material, cell wall and water-soluble material were not changed at 6 days of drying, but alcohol-insoluble materials and cell wall were decreased at 9 days of drying, however water-soluble materials were increased. Pectin and hemicellulose were not changed at 6 days of drying. Pectin and alkali-soluble hemicellulose were remarkable decreased at 9 days of drying, but acid-soluble hemicellulose was increased. Water-soluble pectin was not changed at 6 days of drying, but increased at 9 days of drying. EDTA-soluble and insoluble pectin were decreased after 6 days of drying. The non-cellulosic neutral sugars were not changed at 6 days of drying. The contents of arabinose, galactose and total neutral suger were decreased at 9 days of drying.

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Effect of Ta Substitution on the Dielectric and Piezoelectric Properties of (Li0.04(Na0.54K0.46)0.96(Nb0.96-xTaxSb0.04)O3Ceramics (Ta 치환이 (Li0.04(Na0.54K0.46)0.96(Nb0.96-xTaxSb0.04)O3 세라믹스의 유전 및 압전 특성에 미치는 영향)

  • Noh, Jung-Rae;Yoo, Ju-Hyun
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.24 no.8
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    • pp.627-631
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    • 2011
  • [ $[Li_{0.04}(Na_{0.54}K_{0.46})_{0.96}](Nb_{1-0.04-X}TaxSb_{0.04})O_3$ ]lead-free piezoelectric ceramics have been prepared by normal sintering at $1,100^{\circ}C$ for 5 h. X-ray diffraction analysis indicated that specimens demonstrate orthorhombic symmetry when $Ta\leq5$ mol%. While transforming into tetragonal symmetry when $x\geq20$ mol%. These suggest that the orthorhombic and tetragonal phases co-exist in the ceramics with 5 mol% $cm^3$. As the result of SEM images, the grain growth was decreased with the increase of Ta substitution. The ceramics become 'softening', leading to improvements in $k_p$, $\varepsilon_r$ and $d_{33}$, but a decrease in $Q_m$. Excellent properties of $k_p$= 0.46, $d_{33}$= 293 pC/N, ${\varepsilon}_r$= 1,583 and Tc= $340^{\circ}C$ were obtained when Ta= 15 mol%.