• Korean Journal of Food Science and Technology
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• v.37 no.3
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• pp.352-359
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• 2005

Uncertainty involved during determination of vitamin C content in infant formula was quantified by indophenol titration method. Uncertainty sources in measurand, such as purity, weight, final volume of standard, volume of standard solution used for titration, sample weight, final volume of sample, extraction solution used for titration, titration of extraction solution and standard solution by indophenol solution were identified and used as parameters for combined standard uncertainty based on Guide to the expression of uncertainty in measurement (GUM) and Draft EURACHEM/CITAC Guide. Uncertainty parameters of each source in measurand were identified as resolution, reproducibility and stability of chemical balance, standard material purity, repeatability, reproducibility, end point of titration, 1 mL pipet, 5 mL autopipet, and 100 mL mass flask. Each uncertainty component was evaluated by types A and B and included to calculate combined uncertainty. Analytical test result for traceability under laboratorial conditions using Certified Reference Material (CRM) test was certified as $108.4{\pm}1.7mg/100g$, which was within CRM certification range of $114.6{\pm}6.6mg/100g$. Uncertainty test result of vitamin C content of 5 g sampling was $56.7{\pm}2.44mg/100g$. Uncertainty could be reduced by identification of uncertainty sources and components related with vitamin C determination by indophenol titration method and by decreasing uncertainty sources and components.

• Tunnel and Underground Space
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• v.13 no.5
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• pp.397-402
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• 2003

Generally it is likely that rock mass properties are expressed not by a mean value but by values with variation due to its characteristic uncertainty. This characteristic is one of the most important parts for the design of undergound structures, but yet to be fully examined. Stochastic finite element method (SFEM) is contrary to deterministic finite element method in its concept as the former has been developed in order to take the randomness of structural systems into account. Using SFEM, the response variability of structural system can be obtained and it leads probabilistic stability of structure to be analyzed. In this study, displacement response variability of circular opening with hydrostatic stress field are analyzed in terms of rock mass properties having a certain mean and a standard deviation using the SFEM. The analyzed response variability shows that the necessity of probabilistic stability analysis of underground structures using reliable mean value and standard deviation of deformation modulus.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.27 no.8
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• pp.1051-1060
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• 2003

The heat and mass transfer on two kinds of tube surfaces (bare stainless steel tube and Teflon coated tube) in steam-air mixture flow are experimentally studied to obtain design data for the heat exchanger of the latent heat recovery from flue gas. In the test section, 3-tubes are horizontally installed, and steam-air mixture is vertically flowed from the top to the bottom. The pitch between tubes is 67mm, the out-diameter of tube is 25.4mm, and the thickness is 1.2mm ; blockage factor (cross sectional tube area over the cross sectional area of the test section) is about 0.38. All of sensors and measurement systems (RTD, pressure sensor, flow-meter, relative humidity sensor, etc.) are calibrated with certificated standard sensors and the uncertainty for the heat transfer measurement is surveyed to have the uncertainty within 7%. As experimental results, overall heat transfer coefficient of the Teflon (FEP) coated tube is degraded about 20% compared to bare stainless tube. The degradation of overall heat transfer coefficient of Teflon coated tube comes from the additional heat transfer resistance due to Teflon coating. Its magnitude of heat transfer resistance is comparable to the in-tube heat transfer resistance. Nusselt and Sherwood numbers on Teflon (FEP) coated surface and bare stainless steel surface are discussed in detail with the contact angles of the condensate.

• Atmosphere
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• v.26 no.3
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• pp.435-444
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• 2016

In spite of considerable progress in the recent decades, there still remain large uncertainties in numerical cloud models. In this study, effects of uncertainty in terminal velocity of graupel on cloud simulation are investigated. For this, a two-dimensional bin microphysics cloud model is employed, and deep convective clouds are simulated under idealized environmental conditions. In the sensitivity experiments, the terminal velocity of graupel is changed to twice and half the velocity in the control experiment. In the experiment with fast graupel terminal velocity, a large amount of graupel mass is present in the lower layer. On the other hand, in the experiment with slow graupel terminal velocity, almost all graupel mass remains in the upper layer. The graupel size distribution exhibits that as graupel terminal velocity increases, in the lower layer, the number of graupel particles increases and the peak radius in the graupel mass size distribution decreases. In the experiment with fast graupel terminal velocity, the vertical velocity is decreased mainly due to a decrease in riming that leads to a decrease in latent heat release and an increase in evaporative cooling via evaporation, sublimation, and melting that leads to more stable atmosphere. This decrease in vertical velocity causes graupel particles to fall toward the ground easier. By the changes in graupel terminal velocity, the accumulated surface precipitation amount differs up to about two times. This study reveals that the terminal velocity of graupel should be estimated more accurately than it is now.

• Journal of Korean Society on Water Environment
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• v.36 no.6
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• pp.508-520
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• 2020

Dam reservoirs have been reported to contribute significantly to global carbon emissions, but unlike natural lakes, there is considerable uncertainty in calculating carbon emissions due to the complex of emission pathways. In particular, the method of calculating carbon dioxide (CO2) net atmospheric flux (NAF) based on a simple gas exchange theory from sporadic data has limitations in explaining the spatiotemporal variations in the CO2 flux in stratified reservoirs. This study was aimed to analyze the spatial and temporal CO2 distribution and mass balance in Daecheong Reservoir, located in the mid-latitude monsoon climate zone, by applying a two-dimensional hydrodynamic and water quality model (CE-QUAL-W2). Simulation results showed that the Daecheong Reservoir is a heterotrophic system in which CO2 is supersaturated as a whole and releases CO2 to the atmosphere. Spatially, CO2 emissions were greater in the lacustrine zone than in the riverine and transition zones. In terms of time, CO2 emissions changed dynamically according to the temporal stratification structure of the reservoir and temporal variations of algae biomass. CO2 emissions were greater at night than during the day and were seasonally greatest in winter. The CO2 NAF calculated by the CE-QUAL-W2 model and the gas exchange theory showed a similar range, but there was a difference in the point of occurrence of the peak value. The findings provide useful information to improve the quantification of CO2 emissions from reservoirs. In order to reduce the uncertainty in the estimation of reservoir carbon emissions, more precise monitoring in time and space is required.

• Analytical Science and Technology
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• v.21 no.6
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• pp.502-509
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• 2008

An ID LC/MS (isotope dilution liquid chromatography/mass spectrometry) was used as a primary method for the quantitative analysis of cholesterol in human serum. The separation of cholesterol was carried out by Thermo ODS hypersil $C^{18}$ column. The mobile phase was 100% methanol, and flow rate was $0.3m{\ell}/min$. Cholesterol and cholesterol-$3,4-13C_2$ were monitored at m/z 369.4 and 371.3, which correspond to $[M-H_2O+H]^+$ respectively. In order to verify the measurement method, NIST SRM 909b was analyzed. The results agreed well with certified values within uncertainty. The four kinds of serum certified reference material were prepared and certified. The repeatabilities of measurement were ranged from 0.1 to 0.8% (RSD), which were relatively good. The reproducibility between independent measurement run was below 0.24% (RSD). The expanded uncertainty was about 1.43% within the 95% confidence interval.

• Geomechanics and Engineering
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• v.22 no.3
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• pp.207-217
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• 2020

Slope reliability analysis and risk assessment for spatially variable soils under rainfall infiltration are important subjects but they have not been well addressed. This lack of study may in part be due to the multiple and diverse evaluation indexes and the low computational efficiency of Monte-Carlo simulations. To remedy this, this paper proposes a highly efficient computational method for investigating random field problems for slopes. First, the probability density evolution method (PDEM) is introduced. This method has high computational efficiency and does not need the tens of thousands of numerical simulation samples required by other methods. Second, the influence of rainfall on slope reliability is investigated, where the reliability is calculated from based on the safety factor curves during the rainfall. Finally, the uncertainty of the sliding mass for the slope random field problem is analyzed. Slope failure consequences are considered to be directly correlated with the sliding mass. Calculations showed that the mass that slides is smaller than the potential sliding mass (shallow surface sliding in rainfall). Sliding mass-based risk assessment is both needed and feasible for engineered slope design. The efficient PDEM is recommended for problems requiring lengthy calculations such as random field problems coupled with rainfall infiltration.

• Journal of the Korean Geotechnical Society
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• v.19 no.5
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• pp.319-326
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• 2003

In site investigation for tunnel designs, nowadays, geophysical exploration such as seismic exploration and electric resistivity exploration as well as drilling logging is frequently carried out. A method which can systematically make the utmost use of all available data obtained from investigation, therefore, is strongly required for the optimal evaluation of ground conditions in terms of rock mass class, etc. Many researchers have proposed using qualitative data to cope with the lack of quantitative data. In this study, an evaluation technique of rock mass classes in undrilled region was proposed based upon multiple indicator kriging method which is a geostatistical technique. It was shown that two types of data with different degree of uncertainty, for example, drilling logging data and geophysical exploration data, could be simultaneously utilized in evaluating rock mass classes for a real tunnel design.

• The Journal of Engineering Geology
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• v.17 no.4
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• pp.535-544
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• 2007

Discontinuities developed in a sedimentary rock mass are the most important factor to determine mechanical properties of the rock mass. Parameters described discontinuities in rock mass generally connote heterogeneity and uncertainty. In this study, probabilistic statistics method was used to determine parameters of discontinuities quantitatively and objectively. The field survey was conducted at 33 sedimentary rock slopes in Ulsan area, according to the suggested methods for the quantitative description of discontinuities in rock mass(ISRM, 1978). The engineering geological characteristics of the sedimentary rocks at Ulsan area was determined as probability distribution function deduced by analyzing parameters of discontinuities.

• Proceedings of the KIEE Conference
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• 1997.07f
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• pp.1982-1984
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• 1997

In this paper, adaptive variable structure control is proposed for Electromagnetic Suspension(EMS). Although variable structure control shows excellent robustness to unstructured modelling uncertainty, such as flux leakage and saturation, it has several drawbacks that severely limit practical applicability such as high control activity and control chattering. To minimize these effects, the mass of the electromagnet and efficiency of levitation force are estimated on-line to reduce the range of system uncertainty. The effectiveness of the proposed control scheme is verified by experimental results using a 1.5kg electromagnet and DSP (TMS320C31).