• Food Science of Animal Resources
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• v.35 no.6
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• pp.765-771
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• 2015

The development of a sample preparation method and optimization of the analytical instrumentation conditions were performed for the determination of the vitamin B₁₂ content in emulsified baby foods sold on the Korea market. After removal of the milk protein and fats by chloroform extraction and centrifugation, the vitamin B₁₂ was water extracted from the sample. Following filtration of the solution through a nylon filter, the water-soluble extract was purified by solid-phase extraction using a Liquid Chromatography Tandem Mass Spectrometry (LC-MS/MS). The solution eluted from the cartridge was dried under a stream of nitrogen gas and reconstituted with 1 mL of water. The sample solution was injected into an LC-MS/MS system after optimizing the mobile phase for vitamin B₁₂ detection. The calibration curve showed good linearity with the coefficient of correlation (r²) value of 0.9999. The limit of detection was 0.03 µg/L and the limit of quantitation was 0.1 µg/L. The method of detection limit was 0.02 µg/kg. The vitamin B₁₂ recovery from a spiking test was 99.62% for infant formula and 99.46% for cereal-based baby food. The sample preparation method developed in this study would be appropriate for the rapid determination of the vitamin B₁₂ content in infant formula and baby foods with emulsified milk characteristics. The ability to obtain stable results more quickly and efficiently would also allow governments to exercise a more extensive quality control inspection and monitoring of products expected to contain vitamin B₁₂. This method could be implemented in laboratories that require time and labor saving.

• Journal of Korean Academy of Oral and Maxillofacial Radiology
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• v.27 no.1
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• pp.87-97
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• 1997

The purpose of this study was to evaluate the method for quantitative assessment of bone mass from aluminum-equivalent value of hydroxyapatite by using digital imaging system consisted of Power Macintosh 7200/120, 15-inch color monitor, and GT-9000 scanner with transparency unit. After aluminum-equivalent image made from correlation between aluminum thickness and grey scale, the accuracy of conversion to mass from aluminum-equivalent value was evaluated. Measured bone mass was compared with converted bone mass from aluminum-equivalent value of hydroxyapatite block by correlation formula between aluminum-equivalent value of hydroxyapatite block and hydroxyapatite mass. The results of this study were as follow; 1. Correlation between aluminum thickness and grey level for obtaining aluminum-equivalent image was high positively associated(r²=0.99). Converted masses from aluminum-equivalent value were very similar to measured masses. There was, statistically, no significant difference(P<0.05) between them 2. Correlation between hydroxyapatite aluminum-equivalent and hydroxyapatite mass was shown to linear relation (r²=0.95). 3. Converted masses from aluminum-equivalent value of 3 dry mandible segments were similar to measured masses. The difference between the exposure directions was not significantly different(P<0.05).

• Tunnel and Underground Space
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• v.29 no.3
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• pp.172-183
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• 2019

The generalized Hoek-Brown (GHB) failure criterion developed by Hoek et al. (2002) is a nonlinear function which defines a stress condition at failure of rock mass. The relevant strength parameter values are systematically determined using the GSI value. Since GSI index is a value quantifying the condition of in-situ rock mass, the GHB criterion is a practical failure condition which can take into the consideration of in-situ rock mass quality. Considering that most rock mechanics engineers are familiar with the linear Mohr-Coulomb criterion and that many rock engineering softwares incorporate Mohr-Coulomb criterion, the equations for the equivalent friction angle and cohesion were also proposed along with the release of the GHB criterion. The proposed equations, however, fix the lower limit of the minor principal stress range, where the linear best-fitting is performed, with the tensile strength of the rock mass. Therefore, if the tensile stress is not expected in the domain of analysis, the calculated equivalent friction angle and cohesion based on the equations in Hoek et al. (2002) could be less accurate. In order to overcome this disadvantage of the existing equations for equivalent friction angle and cohesion, this study proposes the analytical formula which can calculate optimal equivalent friction angle and cohesion in any minor principal stress interval, and verified the accuracy of the derived formula.

• Journal of Community Nutrition
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• v.4 no.2
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• pp.99-108
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• 2002

Recently interests on raw-food diets are rapidly increasing in relation to chronic diseases prevention in Korea, but studies on raw-food diets have been hardly performed by nutritionists. This study was performed to investigate the effects of low-calorie diets using a raw-food formula in the form of freeze-dried powder on obesity and its complications in the obese women (body mass index (BMI) $\geq$ 25kg/㎡) for eight weeks. Forty premenopausal women (mean BMI 28.04kg/㎡, mean age 28.33years old) participated in this diet intervention, and were controlled by eating 1 regular meal, 1-2 snacks and 2 raw-food formula (140kcal/pack) meals a day within the 1500-1300kcal ranges. Anthropo-mentric measurements, body compositions, physical exercise, and obesity-related risk factors were assessed before (the initial), during (the 4th week) and after (the 8th week) the study. All the data was analyzed by paired t-test, repeated measures ANOVA, and nonparametric rank test at p<0.05 level. Obesity was significantly increased during this study, and it was decreased in weight (-4.59%, p<0.000), BMI (-4.56%, p<0.000), body fat percent (-6.18%, p<0.000), fat mass (-10.19%, p<0.000), waist and hip circumferences(-5.69%, p<0.000 and -2.55%, p<0.000) and WHR (-3.24%, p<0.000). Energy expenditure of physical exercise was increased as much as 70kca1/day during the study (p=0.000), but it did not have any correlations with weight loss and changes of body compositions. Biochemical measurements including blood triglyceride(p <0.006) and leptin(p<0.000) levels were significantly decreased, LDL cholesterol level was increased(p<0.05), but all the blood lipid levels were in the normal ranges. Fatty liver echogenicity and menstrual irregularity were improved after the diet intervention(p<0.000 and p<0.034). In conclusion, this B-week low-calorie diet intervention using raw-food formula was effective for obese premenopausal women in reducing obesity and its risk factors so as not to proceed towards comorbidities. However, the variation of blood lipid levels should be observed for a longer Period.

• Journal of Dairy Science and Biotechnology
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• v.25 no.1
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• pp.55-60
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• 2007

Contents of scorched particles in infant formula were studied to provide a scientific evidence for standardization of Food Regulation in Korea. The specification of scorched particles in infant formula in Korea was satisfied with CODEX, USDA and so on. But food regulations for scorched particles in baby food are not mentioned in Korea. Nowadays social interests of scorched particles in infant formula are being increased in the respect of safety for baby food. The composition and contents of scorched particles were analyzed with Scanning Electron Microscope-Energy Dispersive X-ray Spectrometer(SEM-EDS) and Inductively Coupled Plasma Mass Spectrometer(ICP-MS). The results indicate that the scorched particles consist Ca, Na, Fe, Mg and trace elements derived from the ingredient of infant formula. Infant formula are composed of milk, skimmed milk, whey, mixed vegetable oils, minerals and vitamins. These results also show that the contents of scorched particles of infant formula in Korea are little or similar level to those reported in other countries. In general, heavy metals derived from scorched particle are originally used as a source of minerals in infant formula. And it has been thought that they doesn't effect on Provisional Tolerable Weekly Intake set by FAO/WHO for contents and composition of scorched particles.

• Transactions of the Korean Society of Machine Tool Engineers
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• v.11 no.5
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• pp.88-92
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• 2002

This research is about slurry wear of SM45C and SUS304, which using standard sand and KUM river sand. The results are as follows ; 1. Mass loss rates of both standard sand and KUM river sand were linearly increased as increasement of time and velocity. 2. The average diameter of sand from relatively, less wear rate and portion of larger particles. 3. Wear resistance was linear with time and velocity of liquid jet regardless of type of sand. Also, it was able to evaluate with the formula, $HV^2$/E calibrated with n, the velocity index. 4. The wear surface in liquid jet experiment was smooth. The maximum wear depth was observed at the location 2~4mm apart from the center in the condition of $90^{\circ}$ of collision angle 6mm of nozzle diameter, and 20mm of collision distance. The sectional shape in radial appeared as 'W'shape.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2001.04a
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• pp.798-801
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• 2001

This research is about slurry wear of SM45C and SUS304, which using standard sand and KUM river sand. The results are as follows ; 1. Mass loss rates of both standard sand and KUM river sand were linearly increased as increasement of time and velocity. 2. The average diameter of sand from relatively, less wear rate and portion of larger particles. 3. Wear resistance was linear with time and velocity of liquid jet regardless of type of sand. Also it was able to evaluate with the formula, HV2/E calibrated with n, the velocity index. 4. The wear surface in liquid jet experiment was smooth. The maximum wear depth was observed at the location, 2~4mm apart from the center in the condition of 90$^{\circ}$of collision angle 6mm of nozzle diameter, and 20mm of collision distance. The sectional shape in radial appeared as 'W' shape.

• Journal of the Society of Naval Architects of Korea
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• v.45 no.3
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• pp.309-314
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• 2008

An experimental method to estimate the added mass of a marine propeller has been developed for the axial rigid body motion in still water, and the experiments have been carried out. The experimental result has been compared to the theoretical result by PRODAS based on the unsteady lifting surface theory. The experimental method developed in this research and the theoretical method by PRODAS have been validated by confirming good agreements between the experimental results and the theoretical ones. Also the comparison to the results by empirical formula has been made and discussed.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2004.10a
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• pp.166-169
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• 2004

A fatigue test was used to evaluate the fatigue life of an actual structure. The loaded state and the constraint condition of an actual structure must be same as the specimen in order to apply the test results to an actual structure by the specimen. The loaded state and constraint conditions can't be same as the specimen in the actual structure which is complicated. In order to reduce these differences, an actual structure test with a lot of frequencies is need to get a fatigue life curve. Therefore, ten sets of accelerated test units which attached unbalanced mass were composed in this study. Acceleration history about the vibration of an actual structure was acquired. Rainflow counting was used on acceleration history, and the life curve return formula was assumed. The return formula that damage satisfied `1' was acquired in a feedback process by the Miner's rule, which was the linear cumulative damage theory. A conservative fatigue life curve was determined with a return formula to have been presumed by each set. The fatigue life of regular rpm condition was calculated by these conservative fatigue life curves.

• Earthquakes and Structures
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• v.14 no.4
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• pp.305-312
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• 2018

Significant research efforts were undertaken to evaluate seismic performance of vertically irregular buildings on flat ground. However, there is scarcity of study on seismic performance of buildings on hill slopes. The present study attempts to investigate seismic behaviour of reinforced concrete irregular stepback building frames with different configurations on sloping ground. Based on extensive regression study of free vibration results of four hundred seventeen frames with varying ground slope, number of story and span number, a modification is proposed to the code based empirical fundamental time period estimation formula. The modification to the fundamental time period estimation formula is a simplified function of ground slope and a newly introduced equivalent height parameter to reflect the effect of stiffness and mass irregularity. The derived empirical formula is successfully validated with various combinations of slope and framing configurations of buildings. The correlation between the predicted and the actual time period obtained from the free vibration analysis results are in good agreement. The various statistical parameters e.g., the root mean square error, coefficient of determination, standard average error generally used for validation of such regression equations also ensure the prediction capability of the proposed empirical relation with reasonable accuracy.