• Title/Summary/Keyword: magnetic saturation

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Feasibility Study on Magnetic Nanoparticle Hyperthermia in Low Field MRI (저자장 자기공명영상 시스템 내에서 초상자성 나노입자 온열치료를 위한 발열 평가)

  • Kim, Ki Soo;Cho, Min Hyoung;Lee, Soo Yeol
    • Journal of Biomedical Engineering Research
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    • v.35 no.4
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    • pp.105-110
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    • 2014
  • For the combination of MRI and magnetic particle hyperthermia(MPH), we investigated the relative heating efficiency with respect to the strength of the static magnetic field under which the magnetic nanoparticles are to be heated by RF magnetic field. We performed nanoparticle heating experiments at the fringe field of 3T MRI magnet with applying the RF magnetic field perpendicularly to the static magnetic field. The static field strengths were 0T, 0.1T, 0.2T, and 0.3T. To prevent the coil heat from conducting to the nanoparticle suspension, we cooled the heating solenoid coil with temperature-controlled water with applying heat insulators between the solenoid coil and the nanoparticle container. We observed significant decrease of heat generation, up to 6% at 0.3T(100% at 0T), due to the magnetic saturation of the nanoparticles of 15 nm diameter under the static field. We think MPH is still feasible at low magnetic field lower than 0.3T if stronger RF magnetic field generation is permitted.

Magnetic and Magnetostrictive Properties of Amorphous Sm-Fe and Sm-Fe-B Thin Films

  • Choi, Y.S.;Lee, S.R.;Han, S.H.;Kim, H.J.;Lim, S.H.
    • Journal of Magnetics
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    • v.3 no.2
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    • pp.55-63
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    • 1998
  • Magnetic and magnetostrictive properties of amorphous Sm-Fe and Sm-Fe-B thin films are systematically investigated over a wide composition range from 14.1 to 71.7 at.% Sm. The films were fabricated by rf magnetron sputtering using a composite target composed of an Fe (or Fe-B) plate and Sm chips. The amount of B added ranges from 0.3 to 0.8 at. %. The microstructure, examined by X-ray diffraction, mainly consists of an amorphous phase in the intermediate Sm content range from 20 to 45 at.%. Together with an amorphous phase, crystalline phases of Fe and Sm also exist at low and high ends of the Sm content, respectively. Well-developed in-plane anisotropy is formed over the whole compositionrange, except for the low Sm content below 15 at.% and the high Sm content above 55 at %. As the Sm content increases, the saturation magnetization decreases linearly and the coercive force tends to increase, with the exception of the low Sm content where very large magnitudes of the saturation magnetization and the coercive force are observed due to the existence of the crystalline $\alpha$-Fe phase. The coercive force is affected rather substantially by the B addition, resulting in lower values of the coercive force in the practically important Sm content range of 30 to 40 at.%. Good magnetic softness indicated by well-developed in-plane anisotropy, a square-shaped hysteresis loop and a low magnitude of the coercive force results in good magnetostrictive characteristics in both Sm-Fe-B thin films. The magnetostrictive characteristics, particularly at low magnetic fields, are further improved by the addition of B; for example, at a magnetic field of 100 Oe, the magnitude of magnetostriction is -350 ppm in a Sm-Fe thin film and it is -470 ppm in a B containing Sm-Fe thin film.

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Research on MFL PIG Design for the Inspection of Underground Gas Pipeline (지하매설 가스관의 검사를 위한 누설자속탐상 PIG 설계에 관한 연구)

  • Park, Sang-Ho;Park, Gwan-Soo
    • Journal of the Korean Society for Nondestructive Testing
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    • v.22 no.2
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    • pp.177-186
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    • 2002
  • This paper describes the magnetic flux leakage(MFL) type non-destructive testing(NDT) system to detect the 3D defects in underground gas pipe. Magnetic systems with permanent magnets and yokes are analyzed by 3D non-lineal finite element method(FEM) with optimum design. In case of under-saturation of gas pipe, sensing signals are too weak to detect. In case of over-saturation, the changes of the sensing signals are too low to detect the defects sensitively. So, the operating points of the magnetic system are optimized to increase the changes of the MFL signals. The effects of the depth and size of the defects on the sensing signals are analyzed to define the range and resolution of the MFL sensors. To increase the sensor's sensitivity, the back-yoke sensors are introduced and tested.

Magnetic Properties of Fe-Zr-N Soft Magnetic Thin Films (Fe-Zr-N 연자성 박막의 자기적 성질)

  • 김택수;김종오;이중환;윤선진;김좌연
    • Journal of the Korean Magnetics Society
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    • v.6 no.5
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    • pp.317-322
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    • 1996
  • Thin films of Fe-Zr-N were fabricated by rf magnetron reactive sputtering method. The saturation magnetization and coercivity as functions of annealing temperature and partial pressure of nitrogen gas, effective permeability at high frequencies, and thermal stability were investigated. Magnetic softness was exhibited in the composition range of $Fe_{72-78}Zr_{7-10}N_{15-18}$ which was boundary between polycrystalline and amorphous structure. These films exhibited magnetic softness with saturation magentic flux density of 1.55 T and effective permeability of about 3000 at 1 MHz. These films also exhibited thermal stability by sustaining effective permeability of 2500 or above as the temperature was raised to $550^{\circ}C$. It is asswned that good magnetic softness is obtained because grain growth of $\alpha-Fe$ is prohibited due to the precipitation of ZrN nanocrystals. The grain sizes of $\alpha-Fe$ films were $40~50\AA$ and the grain sizes of ZrN nanocrystals were $10~15\AA$.

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Magnetic and Magnetostrictive Properties of Amorphous Tb-Fe- and Tb-Fe-B Thin Films

  • Park, Y. S.;Lee, S. R.;S. H. Han;Kim, H. J.;S. H. Lim
    • Journal of Magnetics
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    • v.2 no.3
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    • pp.76-85
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    • 1997
  • Magnetic and magnetostrictive properties of Tb-Fe and Tb-Fe-B thin films are systematically investigated over a wide composition range from 40.2 to 68.1 at. % Tb. The films were fabricated by rf magnetron sputtering using a composite target which consists of an Fe plate and Tb chips. The microstructure, examined by X-ray diffraction, mainly consists of an amorphous phase and, at high Tb contents, a pure Tb phase also exists. A progressive change in the direction of anisotropy from the perpendicular to in-plane occurs as the Tb content increases and the boundary at which the anisotropy change occurs shifts significantly towards to higher Tb contents with the addition of B. The saturation magnetization exhibits maxima at the Tb contents of 42 and 48 at. % for Tb-Fe and Tb-Fe-B thin films, respectively, and it is decreased by the addition of B. The coercive force, measured in the easy direction, decreases monotonically with the Tb content. Excellent magnetostrictive characteristics, particularly at low magnetic fields, are achieved in both Tb-Fe and Tb-Fe-B thin films; for example, a magnetostriction of 138 ppm is obtained in a Tb-Fe-B thin film at a magnetic field as low as 30 Oe. The excellent magnetostrictive properties of the present thin films are supported by the equally excellent magnetic softness, the coercivity below 10 Oe and a typical squared-loop shape with the saturation field as low as 1 kOe. Due to the excellent low field magnetostrictive characteristics, the present Tb-Fe based thin films are thought to be suitable for Si based microdevices.

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Research on MFL PIG Design for caustic and defect the Inspection of Underground Gas Pipeline (지하매설 가스관의 부식 및 결함 탐지를 위한 비파괴 누설 탐상시스템 개발에 관한 연구)

  • Park, Sang-Ho;Park, Gwan-Soo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.05a
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    • pp.11-20
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    • 2002
  • This paper describes the magnetic flux leakage(MFL) type non-destructive testing(NDT) system to detect the 3D defects on underground gas pipe. Magnetic systems with permanent magnets and yokes are analyzed by 3D non-lineal finite element method(FEM) with optimum design. In case of under-saturation of gas pipe, sensing signals are too weak to detect. In case of over-saturation, the changes of the sensing signals are too low to detect the defects sensitively. So, the operating points of the magnetic system are optimized to increase the changes of the MFL signals. The effects of the depth and size of the defects on the sensing signals are analyzed to define the range and resolution of the MFL sensors. To increase the sensor's sensitivity, the back-yoke sensors are introduced and tested.

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Microstructure and Magnetic Properties in Fe-Co-B/M Films for Soft Magnetic Underlayer of Perpendicular Magnetic Recording Media (수직자기기록매체용 Fe-Co-B/M 하지연자성층의 미세결정구조 및 자기특성)

  • 공석현;손인환;금민종;최형욱;박용서;김경환
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.17 no.8
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    • pp.888-892
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    • 2004
  • It is necessary to develop soft magnetic layer with high saturation magnetization 4 $\pi{M}_s$ and in-plane magnetic anisotropy field Hk for soft magnetic underlayer of perpendicular magnetic recording media with high signal to noise ratio. Fe-Co-B layer with high 4 $\pi$Ms of about 23 kG deposited on Ni-Fe and Ni-Fe/Si seedlayer exhibited very high in-plane magnetic anisotropy filed Hk of about 280 and 380 Oe, respectively, In-plane XRD studies clarified that the lattice spacing of planes along the easy axis direction was longer than that along the hard axis direction in the Fe-Co-B layers with high Hk. These results indicate that high Hk of Fe-Co-B/Ni-Fe and Fe-Co-B/[Ni-Fe/si] layers were resulted from magnetoelastic anisotropy owing to a residual stress. Moreover, the high Hk in the Fe-Co-B/Ni-Fe layer was maintained until 30$0^{\circ}C$ annealing temperature.

Effect of Shape Magnetic Anisotropy of Amorphous Fe-B-P Nanoparticles on Permeability

  • Lee, Ji Eun;Tsedenbal, Bulgan;Koo, Bon Heun;Huh, Seok Hwan
    • Korean Journal of Materials Research
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    • v.30 no.11
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    • pp.589-594
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    • 2020
  • Many electronic applications require magnetic materials with high permeability and frequency properties. We improve the magnetic permeability of soft magnetic powder by controlling the shape magnetic anisotropy of the powders and through the preparation of amorphous nanoparticles. For this purpose, the effect of the shape magnetic anisotropy of amorphous Fe-B-P nanoparticles is observed through a magnetic field and the frequency characteristics and permeability of these amorphous nanoparticles are observed. These characteristics are investigated by analyzing the composition of particles, crystal structure, microstructure, magnetic properties, and permeability of particles. The composition, crystal structure, and microstructure of the particles are analyzed using inductively coupled plasma optical emission spectrometry-, X-ray diffraction, scanning electron microscopy and focused ion beam analysis. The saturation magnetization and permeability are measured using a vibrating sample magnetometer and an LCR meter, respectively. It is confirmed that the shape magnetic anisotropy of the particles influences the permeability. Finally, the permeability and frequency characteristics of the amorphous Fe-B-P nanoparticles are improved.

A Study of Magnetic Properties in $Fe_{73.9}Cu_{1.0}Nb_{3.5}Si_{14.0}B_{7.6}$ by Magnetic Annelaing

  • Kim, Eng-Chan;Kim, Jin-Eui;Nam, Hyo-Duk
    • Transactions on Electrical and Electronic Materials
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    • v.1 no.3
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    • pp.29-33
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    • 2000
  • The crystallographic and high frequency characteristics of $Fe_{73.9}Cu_{1.0}Nb_{3.5}Si_{14.0}B_{7.6}$ soft magnetic alloys were investigated under magnetic field annealing, The crystallization fraction of annealed samples with longitudinal magnetic fields is higher than that of samples without magnetic field. When the transverse magnetic field is applied, the crystallization fraction does not increases but decreases until $500^{circ}C$. It is found that for samples, the saturation induction are all same with 1.3 T. The coercive field of as-cast samples is 1.03 A/cm, but in annealed samples it decrease from 0.56 to 0.1A/cm with increasing annealing temperature from 400 to $550^{circ}C$. The squareness of annealed samples under transverse magnetic field has a small value than that of both without field and with longitudinal field annealing. It is noted that the magnetic field annealing with transverse direction to amorphous $Fe_{73.9}Cu_{1.0}Nb_{3.5}Si_{14.0}B_{7.6}$ profoundly influenced on the Mossbauer spectra in contrast to that with longitudinal direction and without magnetic field.

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AR Model and LSQ Based Compensation Method for the Saturated Secondary Current of a Current Transformer (AR 모델 및 LSQ 기반 변류기 2차 전류 복원 기법)

  • Chang, Soo-Young;Lee, Dong-Gyu;Kang, Sang-Hee
    • The Transactions of the Korean Institute of Electrical Engineers A
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    • v.55 no.6
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    • pp.221-226
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    • 2006
  • The current flowing though a power line is measured by a current transformer (CT). Since a CT is a kind of transformer, saturation of magnetic flux in the core may occur when a large primary current flows. This saturation makes the secondary current of a CT distorted and causes problems in the protection point of view. Because of the current distortion, a protection relay cannot collect the correct information showing how the primary power system changed. Consequently, the current distortion may cause the mal-operation or operation time delay of protective relay. In this paper, an algorithm based on AR model and LSQ is proposed to compensate the saturated CT secondary currents. Various test results indicate that the proposed algorithm can accurately compensate a severely distorted secondary current and is not affected by remanence.