• 제목/요약/키워드: magnetic particle

검색결과 601건 처리시간 0.023초

In situ analysis of capturing dynamics of magnetic nanoparticles in a microfluidic system

  • Munir, Ahsan;Zhu, Zanzan;Wang, Jianlong;Zhou, H. Susan
    • Smart Structures and Systems
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    • 제12권1호
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    • pp.1-22
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    • 2013
  • Magnetic nanoparticle based bioseparation in microfluidics is a multiphysics phenomenon that involves interplay of various parameters. The ability to understand the dynamics of these parameters is a prerequisite for designing and developing more efficient magnetic cell/bio-particle separation systems. Therefore, in this work proof-of-concept experiments are combined with advanced numerical simulation to design and optimize the capturing process of magnetic nanoparticles responsible for efficient microfluidic bioseparation. A low cost generic microfluidic platform was developed using a novel micromolding method that can be done without a clean room techniques and at much lower cost and time. Parametric analysis using both experiments and theoretical predictions were performed. It was found that flow rate and magnetic field strength greatly influence the transport of magnetic nanoparticles in the microchannel and control the capturing efficiency. The results from mathematical model agree very well with experiments. The model further demonstrated that a 12% increase in capturing efficiency can be achieved by introducing of iron-grooved bar in the microfluidic setup that resulted in increase in magnetic field gradient. The numerical simulations were helpful in testing and optimizing key design parameters. Overall, this work demonstrated that a simple low cost experimental proof-of-concept setup can be synchronized with advanced numerical simulation not only to enhance the functional performance of magneto-fluidic capturing systems but also to efficiently design and develop microfluidic bioseparation systems for biomedical applications.

전기폭발법에 의한 Ni 및 Ni-Cu 나노 금속 분말의 제조와 자기적 특성연구 (Study of Synthesis and Magnetic Properties of Ni and Ni-Cu Nano Metal Powders Prepared by the Pulsed Wire Evaporation(PWE) Method)

  • 박중학;엄영랑;김경호;김흥희;이창규
    • 한국분말재료학회지
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    • 제10권2호
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    • pp.83-88
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    • 2003
  • Nanocrystalline materials of Ni and Ni-Cu alloy have been synthesized by the pulsed wire evaporation (PWE) method and these abnormal magnetic properties in the magnetic ordered state have been characterized using both VSM and SQUID in the range of high and low magnetic fields. Ni and Ni-Cu particles with an average size of 20 to 80 nm were found to influence magnetic hysterisis behavior and the results of powder neutron diffraction patterns and saturation magnetization curves are shown to indicate the absence of the NiO phase. The shifted hysterisis loop and irreversibility of the magnetization curve in the high field region were observed in the magnetic-ordered state of both Ni and Ni-Cu. The virgin magnetization curve for Ni slightly spillover on the limited hysterisis loop ($\pm$20kOe). This irreversibility in the high field of 50 kOe can be explained by non-col-linear behavior and the existence of the metastable states of the magnetization at the surface layer (or core) of the particle in the applied magnetic field. Immiscible alloy of Cu-Ni was also found to show irreversibility having two different magnetic phases.

Development of Moving Alternating Magnetic Filter Using Permanent Magnet for Removal of Radioactive Corrosion Product from Nuclear Power Plant

  • M. C. Song;Kim, S. I.;Lee, K. J.
    • Nuclear Engineering and Technology
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    • 제34권5호
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    • pp.494-501
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    • 2002
  • Radioactive Corrosion Products (CRUD) which are generated by the neutron activation of general corrosion products at the nuclear power plant are the major source of occupational radiation exposure. Most of the CRUD has a characteristic of showing strong ferrimagnetisms. Along with the new development and production of permanent magnet (rare earth magnet) which generates much stronger magnetic field than the conventional magnet, new type of magnetic filter that can separate CRUD efficiently and eventually reduce radiation exposure of personnel at nuclear power plant is suggested. This separator consists of inner and outer magnet assemblies, coolant channel and container surrounding the outer magnet assembly. The rotational motion of the inner and outer permanent magnet assemblies surrounding the coolant channel by driving motor system produces moving alternating magnetic fields in the coolant channel. The CRUD can be separated from the coolant by the moving alternating magnetic field. This study describes the results of preliminary experiment performed with the different flow rates of coolant and rotation velocities of magnet assemblies. This new magnetic filter shows better performance results of filtering the magnetite at coolant (water). How rates, rotating velocities of magnet assemblies and particle sizes turn out to be very important design parameters.

Analysis of Mobile Lead in Soil Using Carboxylated Magnetic Particle

  • So, Hyung-Suk;Shin, Hyun-Chul;Yoo, Yeong-Seok;Schaeffer Andreas
    • Journal of Magnetics
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    • 제10권3호
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    • pp.89-92
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    • 2005
  • The analytic possibility of mobile lead contained in soil has been studied using carboxylated magnetic beads. Extraction of heavy metal was performed to contaminated soil that has been collected and supplied for tests. As experiment materials, soil sample, distilled water and magnetic beads were only used. It means that the lead was extracted under neutral condition. In this condition, only the mobile fraction of lead could be extracted by magnetic beads. The mobile lead in the soil was quickly combined with magnetic beads in the mixture process. Then, the magnetic beads were dissolved into acids after collection by external magnetic force, and the lead combined with the beads was eluted and analyzed by Graphite Furnace Atomic Absorption Spectroscopy (GFAAS). In the results of extraction experiments for 3 sandy soils, the efficiency using beads was similar to or higher than that of EDTA (Ethylendiamintetraacetic acid), which is normally used for analyzing mobile heavy metal concentration in soil. With this, it was shown that this method is a more accurate and simple method to analyze mobile lead when analyzing mobile heavy metal concentration in sandy soil, rather than conventional method using EDTA.

필릿 용접의 기계적 시험 특성 평가 (Evaluation of Mechanical Test Characteristics of Fillet Welding)

  • 조병준;이성준;임종국
    • 한국산학기술학회논문지
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    • 제21권2호
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    • pp.535-541
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    • 2020
  • FCAW는 모든 자세에서 용접이 가능하고 작업여건 변수가 많은 현장에서 우수한 품질을 얻을 수 있는 장점이 있어 탄소강과 합금강의 중판, 후판 용접에 많이 사용되고 있다. 최근 국내에서 진행한 연구논문의 대부분이 피로 강도 평가 방법 연구, 잔류응력 및 변형, 필릿 용접 공정 개발 등의 연구가 시행되었으나 필릿 용접을 대상으로 경도, 매크로, 자분탐상 결과를 토대로 하여 기계적 특성을 나타낸 연구가 부족함에 따라 본 연구에서는 FCAW를 이용하여 상부는 SS400(일반구조용 압연강재) 후판은 SM490A(용접구조용 압연강재)를 이용하여 필릿 용접 후 경도시험, 매크로 시험, 자분탐상시험을 통해 아래와 같은 결론을 도출하였다. 경도시험 결과, 모든 결과 값이 KS B 0893의 규격치 350Hv보다 낮게 나타나 양호한 것으로 판단되었고, 매크로 시험 결과 용접부의 형상별로 균일한 조직 상태를 나타냈으며, 용접부 전 단면에 걸쳐 내부 결함, 기포 또는 불순물 등이 발견되지 않아 lamination의 우려가 없었으며, 자분탐상검사 결과 별도의 문제점이 발견되지 않았다.

국소 자기장의 순/역 배열을 이용한 미세유체 채널 내에서의 강자성 입자 패턴 형성 (In-situ Patterning of Magnetic Particles in Microfluidic Channels by Forward/Reverse Local Magnet Arrangement)

  • 박현향;이지혜;유영은;김정엽;장성환
    • 대한기계학회논문집 C: 기술과 교육
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    • 제3권3호
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    • pp.217-223
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    • 2015
  • 유체채널 내에서의 미세입자의 패터닝은 생물 및 의료 응용분야에서 활용될 가치가 높은 응용 기술이다. 본 연구는 미세유체 채널 내에서 구조물 없이 외부 자석의 배열만을 이용한 미세입자 패터닝 방법을 제안한다. 자석의 같은 극과 서로 다른 극끼리의 배열을 이용한 일렬 배열, 적층 배열 등을 고안하여, 다양한 미세입자 패터닝에 실험적으로 적용하였다. 서로 같은 극끼리의 배열은 입자 포획에 쉽게 적용 가능하여, 독립적 배열이 가능하였다. 특히 적층 배열은 다양한 패터닝을 할 수 있음을 확인할 수 있었다. 자기력 1.08mT 수준에서까지 자석 배열에 의한 일정한 패턴을 관찰할 수 있었고, 패터닝된 입자들은 20 ml/hr 의 유체 속도에서도 안정하게 유지되었다. 본 연구는 간단하면서도 자성 입자의 다양한 패터닝을 가능케 하는 방법으로 면역자기성 입자를 이용한 의학/바이오 분야로의 폭넓은 응용을 기대케 한다.

Preparation and Physical Characterizations of Superparamagnetic Maghemite Nanoparticles

  • Yoon, Sunghyun
    • Journal of Magnetics
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    • 제19권4호
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    • pp.323-326
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    • 2014
  • Superparamagnetic maghemite nanoparticles were prepared by chemical co-precipitation, followed by a temperate oxidation stage, and investigated using FE-SEM, XRD, TGA, VSM, and M$\ddot{o}$ssbauer spectroscopy. Through SEM image and XRD analysis, its average particle size was found to be 13.9 nm. While VSM magnetic measurement showed typical superparamagnetic behavior at room temperature, M$\ddot{o}$ssbauer spectroscopic investigation revealed that non-vanishing magnetic hyperfine structure were retained. Cation distribution estimated from M$\ddot{o}$ssbauer spectroscopy confirmed the formation of maghemite nanophase in the sample.

가스터빈 로터 재질에 따른 표면결함 와전류 특성연구 (The Study on Eddy Current Characteristic for Surface Defect of Gas Turbine Rotor Material)

  • 안연식;길두송;박상기
    • 동력기계공학회지
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    • 제14권4호
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    • pp.63-67
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    • 2010
  • This paper introduces the eddy current signal characteristic of magnetic and non-magnetic gas turbine rotor. In the past, Magnetic particle inspection method was used in magnetic material for qualitative defect evaluation and the ultrasonic test method was used for quantitative evaluation. Nowadays, eddy current method is used in magnetic gas turbine rotor inspection due to advanced sensor design technology. We are studying on the magnetic gas turbine rotor by using eddy current method. We prepared diverse depth specimens made by magnetic and non-magnetic materials. We select optimum frequency according to material standard penetration data and experiment results. We got the signal on magnetic and non-magnetic material about 0.2 mm, 05 mm, 1.0 mm, 1.5 mm 2.0 mm and 2.5 mm depth defects and compare the signal amplitude and signal trend according to defect depth and frequency. The results show that signal amplitudes of magnetic are bigger than non-magnetic material and the trends are similar on every defect depth and frequency. The detection and resolution capabilities of eddy current are more effective in magnetic material than in non-magnetic materials. So, the eddy current method is effective inspection method on magnetic gas turbine rotor. And it has the merits of time saving and simple procedure by elimination of the ultrasonic inspection in traditional inspection method.

Designing a Magnetically Controlled Soft Gripper with Versatile Grasping Based on Magneto-Active Elastomer

  • Li, Rui;Li, Xinyan;Wang, Hao;Tang, Xianlun;Li, Penghua;Shou, Mengjie
    • Journal of Information Processing Systems
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    • 제18권5호
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    • pp.688-700
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    • 2022
  • A composite bionic soft gripper integrated with electromagnets and magneto-active elastomers is designed by combining the structure of the human hand and the snake's behavior of enhancing friction by actively adjusting the scales. A silicon-based polymer containing magnetized hard magnetic particles is proposed as a soft finger, and it can be reversibly bent by adjusting the magnetic field. Experiments show that the length, width, and height of rectangular soft fingers and the volume ratio of neodymium-iron-boron have different effects on bending angle. The flexible fingers with 20 vol% are the most efficient, which can bend to 90° when the magnetic field is 22 mT. The flexible gripper with four fingers can pick up 10.51 g of objects at the magnetic field of 105 mT. In addition, this composite bionic soft gripper has excellent magnetron performance, and it can change surface like snakes and operate like human hands. This research may help develop soft devices for magnetic field control and try to provide new solutions for soft grasping.

자기기록용 $Fe_4N$ 분말의 합성 및 자기특성 (Synthesis of $Fe_4N$ Powder and Its Magnetic Properties for Magnetic Recording)

  • 변태봉;오재희
    • 한국세라믹학회지
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    • 제28권2호
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    • pp.93-100
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    • 1991
  • For determination the optimum manufacturing condition Fe4N powder for magnetic recording media, we have studied the following important conditions : the effect of particle size of metal powder on the nitridation, the condition of nitridation on the formation and magnetic properties of Fe4N, and stability of Fe4N powder against temperature and change on standing. The results can be summarized as : 1) Single phase Fe4N is formed at 50v/o of ammonia concentration during the nitridation reaction, 2) Single phase Fe4N is formed above 40$0^{\circ}C$, 15min regardless of the metal powder sizes, 3) Coercivity and saturation magnetization of Fe4N powder almost constant value until 20 day-passing from preparation date.

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