• 제목/요약/키워드: low temperature reduction

검색결과 1,041건 처리시간 0.022초

나노입자를 첨가한 전극용 무연 silver 페이스트의 제조 (Preparation of Lead-free Silver Paste with Nanoparticles for Electrode)

  • 박성현;박근주;장우양;이종국
    • 열처리공학회지
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    • 제19권4호
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    • pp.219-224
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    • 2006
  • Silver paste with low sintered temperature has been developed in order to apply electronic parts, such as bus electrode, address electrode in PDP (Plasma Display Panel) with large screen area. In this study, nano-sized silver particles with 10-30 nm were synthesized from silver nitrate ($AgNO_3$) solution by chemical reduction method and silver paste with low sintered temperature was prepared by mixing silver nanoparticles, conventional silver powder with the particle size 1.6 um and Pb-free frit. Conductive thick film from silver paste was fabricated by screen printing on alumina substrate. After firing at $540^{\circ}C$, the cross section and surface morphology of the thick films were analyzed by FE-SEM. Also, the sheet resistivity of the fired thick films was measured using the four-point technique.

정제방법에 따른 저온추출 죽력의 특성비교 (Property Comparison of Purified Bambusae Caulis in Liqamen extracted at low temperature)

  • 오영준;김해진;황병길;김선민;장경선;김재창
    • 동의생리병리학회지
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    • 제16권3호
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    • pp.532-536
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    • 2002
  • Jookrhyuk (Bambusae Caulis in Liqamen) was extracted at low temperature (100℃ - 160℃) and purified by adsorption and distillation and their physicochemical properties were compared. In case of colour among all Jookrhyuk samples the L value appeared to be higher in the purified Jookrhyuk,and the b value appeared to be higher in crude Jookrhyuk. Purified Jookrhyuk showed much lower level of total sugar and tar contents than crude Jookrhyuk. A considerable reduction in concentration of methanol and phenolic compounds was achieved by purification process, whereas the content of acetic acid was increased. Therefore it was suggested that adsoption and distillation could be used as one of effective purification methods of various Joockrhyuk samples.

Chromatic Dispersion Compensation via Mid-span Spectral Inversion with Periodically Poled $LiNbO_3$ Wavelength Converter at Low Pump Power

  • Kim, Min-Su;Ahn, Joon-Tae;Kim, Jong-Bae;Ju, Jung-Jin;Lee, Myung-Hyun
    • ETRI Journal
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    • 제27권3호
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    • pp.312-318
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    • 2005
  • Mid-span spectral inversion (MSSI) has to utilize high optical pump power, for its operation principle is based on a nonlinear optical wavelength conversion. In this paper, a low pump-power operation of MSSI-based chromatic dispersion compensation (CDC) has been achieved successfully, for the first time to our knowledge, by introducing a noise pre-reduction scheme in cascaded wavelength conversions with periodically poled $LiNbO_3$ waveguides at a relatively low operation temperature. As preliminary studies, phase-matching properties and operation-temperature dependence of the wavelength converter (WC) were characterized. The WC pumped at 1549 nm exhibited a wide conversion bandwidth of 59 nm covering the entire C-band and a conversion efficiency of -23.6 dB at 11 dBm pump power. CDC experiments were implemented with 2.5 and 10 Gb/s transmission systems over 100 km single-mode fiber. Although it is well-known that the signal distortion due to chromatic dispersion is not critical at a 2.5 Gb/s transmission, the clear recovery of eye patterns was identified. At 10 Gb/s transmission experiments, eye patterns were retrieved distinctly from seriously distorted ones, and notable improvements in bit-error rates were acquired at a low pump power of 14 dBm.

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기생 요소 효과들을 고려한 얇은 두께의 LTCC 저역 통과 필터 설계 (A Thin LTCC Low Pass Filter Design Considering Parasitic Elements Effects)

  • 김유선;임영석
    • 대한전자공학회논문지TC
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    • 제45권12호
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    • pp.128-132
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    • 2008
  • 본 논문에서는 LTCC(low temperature co-fired ceramic) 공정을 이용한 삽입된 수동 소자들을 갖는 필터 설계를 하였다. 우수한 성능과 소형화를 위해서 제안된 적층 구조의 기생 성분들은 제안된 회로 변환 과정을 통해 전체 필터 회로에서 긍정적인 효과를 갖도록 하였다. 그 결과 소형화된 저역 통과 필터는 다른 논문들의 소형화된 구조들에 비해 50프로 이상의 적은 두께를 갖을 뿐만 아니라 0.5 GHz와 5 GHz 사이에서 이상적인 저역 통과 필터의 응답을 보였다.

$Si_2H_6$를 이용한LPCVD 실리콘 박막의 결정 성장 및 구조적 성질에 관한 연구 (A Study on the Grain Growth and Structure Properties of LPCVD Films Using $Si_2H_6$ GAS)

  • 홍찬희;박창엽
    • 대한전기학회논문지
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    • 제40권7호
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    • pp.670-674
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    • 1991
  • This paper presents the material properties of LPCVD silicon films formed using Si2H6 gas at various deposition temperatures. To study the structural properties depending on the deposition temperature, XRD, EBD and TEM analyses were used. The maximum grain size in this experiment was obtained at the deposition temperature of 485ø C. It is discussed that LPCVD films formed below the deposition temperature of 485ø C are promising for low temperature TFT applications. The enhancement of the film characteristics results from the reduction of grain boundary density. We also observed that the film properties of Si2H6 at 600ø C was quite different from those of Si H4 at 600ø C. It has shown that the grain structure from a TEM analysis was elliptical and not dependent on the deposition temperature.

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감압 플라즈마를 이용한 Escherichia coli 살균 (Low-Pressure Plasma Inactivation of Escherichia coli)

  • 목철균;송동명
    • 산업식품공학
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    • 제14권3호
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    • pp.202-207
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    • 2010
  • 저온에서 미생물을 사멸시킬 수 있는 비열살균기술로 감압 플라즈마를 활용하고자 생성기체별 감압 플라즈마 특성을 비교하고 Escherichia coli 살균효과를 조사하였다. 1 Torr이하로 감압시킨 상태에서 공기, 산소, 질소를 350 mL/min으로 공급하며 플라즈마를 발생시킨 결과 아크발생 없이 균일한 플라즈마가 생성되었다. 감압 플라즈마에 의한 온도 상승은 5분 처리 시 ${10^{\circ}C}$ 내외, 10분 처리 시 ${25^{\circ}C}$ 미만이었으며, 기체 종류별로는 공기, 산소, 질소 순으로 상승도가 낮았다. 감압 플라즈마 5분간 처리로 E. coli는 5 log 이상 감소하였으며, 이후 감소율이 둔화되어 10분간 처리 후 6-7 log 정도의 감소를 보였다. 감압 플라즈마에 의한 E. coli 살균패턴은 살균속도가 높은 초기와 낮은 후기로 구분되는 2단계 1차 반응으로 확인되었으며, 초기 살균속도상수($k_{1}$)는 공기, 산소, 질소 순으로 감소하였다. 감압 공기플라즈마 살균의 작은 D값 또한 식품 표면의 오염도를 낮추기 위한 비열살균기술로서의 가능성을 제시하였다.

압연조건에 따른 AZ31 마그네슘합금판재의 변형거동 및 미세조직 변화 (Rolling of AZ31 Alloy and Microstructure of Rolled Plates)

  • 하태권;정효태;성환진;박우진
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2006년도 춘계학술대회 논문집
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    • pp.63-66
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    • 2006
  • The effect of warm rolling under various conditions on the microstructure and mechanical property was investigated using an AZ31 Mg alloy sheet. Several processing parameters such as initial thickness, thickness reduction by a single pass rolling, rolling temperature, roll speed, and roll temperature were varied to elicit an optimum condition for the warm rolling process of AZ31 Mg alloy. Microstructure and mechanical properties were measured for specimens subjected to rolling experiments of various conditions. Warm rolling of 30% thickness reduction per pass was possible without any side-crack at temperatures as low as $200^{\circ}C$ under the roll speed of 30 m/min. The initial microstructure before rolling was the mixed one consisting of partially recrystallized and cast structures. Grain refinement was found to occur actively during the warm rolling, producing a very fine grain size of 7 mm after 50% reduction in single pass rolling at $200^{\circ}C$. Yield strength of 204MPa, tensile strength of 330MPa and uniform elongation of 32% have been obtained in warm rolled sheets.

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가압 유동층 반응기에서 산소공여입자의 합성가스 연소 특성 (Syngas Combustion Characteristics of Oxygen Carrier Particle in a Pressurized Fluidized Bed Reactor)

  • 박상수;이동호;최원길;류호정;이영우
    • 한국수소및신에너지학회논문집
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    • 제23권1호
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    • pp.83-92
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    • 2012
  • Syngas combustion characteristics of mass produced oxygen carrier particle (OCN706-1100) were investigated in a pressurized fluidized bed reactor using simulated syngas and air as reactants for reduction and oxidation, respectively. The oxygen carrier showed high fuel conversion, high $CO_2$ selectivity, and low CO concentration at reduction conditions and no NO emission at oxidation conditions. Moreover, OCN706-1100 particle showed good regeneration ability during successive reduction-oxidation cyclic tests up to the 10th cycle. Fuel conversion and $CO_2$ selectivity decreased and CO emission increased as temperature increased. These results can be explained by trend of calculated equilibrium CO concentration with temperature. However, fuel conversion and $CO_2$ selectivity increased and CO emission decreased as pressure and gas residence time increased.

$NH_3$-SCR 반응기 내에서의 $NH_3$/NOx 및 SCR 촉매 온도가 DeNOx 성능에 미치는 영향 (Effect of $NH_3$/NOx ratio and Catalyst Temperature on DeNOx Performance in the $NH_3$-SCR reactor)

  • 홍길화;공호정;황인구;박심수
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2008년도 추계학술대회B
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    • pp.3096-3101
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    • 2008
  • Selective Catalytic Reduction (SCR) technology is well-known to be effective for the reduction of NOx emission. So car manufacturers has adopted Ures-SCR system to be satisfied with emission regulation. This paper discusses the effective of $NH_3/NOx$ ratio and SCR catalyst temperature in the $NH_3$-SCR reactor on DeNOx performance. So it is shown the characteristic of NOx conversion and ammonia slip using the $NH_3$ instead of Urea-Solution. From the result of this study, it is found to optimize $NH_3/NOx$ ratio to have the best case of high NOx conversion and low ammonia slip at variable SCR catalyst temperatures. Lastly, it is also found the characteristics of NOx conversion and ammonia slip with compared with Urea.

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가압 기포유동층에서 산소전달입자들의 환원반응특성 (Reduction Characteristics of Oxygen Carriers in a Pressurized Bubbling Fluidized Bed)

  • 윤주영;배달희;백점인;류호정
    • 한국수소및신에너지학회논문집
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    • 제27권5호
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    • pp.589-596
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    • 2016
  • Effects of pressure, temperature, gas velocity, and fuel flow rate on reduction of three oxygen carriers, SDN70, OC-1, OC-2, were measured and investigated in a pressurized bubbling fluidized bed reactor. Among three oxygen carriers OC-2 was selected as the best oxygen carrier in view of fuel conversion and $CO_2$ selectivity. However, all oxygen carriers showed good reactivity even at high pressure conditions. SDN70 particle showed maximum reactivity at $900^{\circ}C$ and low reactivity at $950^{\circ}C$. However, reactivity decay of OC-1 and OC-2 particles at high temperature condition was negligible. The fuel conversion and the $CO_2$ selectivity slightly decreased as the gas velocity increased, whereas they are slightly increased as the fuel concentration increased.