• Title/Summary/Keyword: linearity test

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A Study on the Application of PbI2 Dosimetry for QA in the Electron Beam Therapy (전자선 치료의 선량 측정 QA를 위한 PbI2 선량계 적용 연구)

  • Yang, Seungwoo;Han, Moojae;Jung, Jaehoon;Choi, Yunseon;Cho, Heunglae;Park, Sungkwang
    • Journal of the Korean Society of Radiology
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    • v.14 no.5
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    • pp.517-522
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    • 2020
  • Electron beam have many factors that affect dose distribution, so even if identical settings are used, they should be identified and used for radiation treatment, and the effects on the structures in the body are sensitive, making it difficult to investigate uniform dose distribution on tumors. In this study, a dosimeter was produced using PbI2 which is a photoelectric material, and electrical characteristics were analyzed for 6, 9, and 12 MeV electronics in linear accelerators. The reproducibility test results showed that RSD were 1.1215%, 1.0160%, and 0.05137% respectively at 6, 9, and 12 MeV energies, indicating that the output signals were stable. The linearity evaluation results showed that the R2 values of the reliability indicator for straight line trend lines were 0.9999, 0.9999, and 0.9994, respectively, at 6, 9, and 12 MeV, to confirm that the output signal was proportional to PbI2 as dose increased. The PbI2 dosimeter in this study is judged to be highly applicable to electromagnet measurement and is thought to be able to be used as a basic study of electron detector through photoelectric material.

A 3.2Gb/s Clock and Data Recovery Circuit without Reference Clock for Serial Data Communication (시리얼 데이터 통신을 위한 기준 클록이 없는 3.2Gb/s 클록 데이터 복원회로)

  • Kim, Kang-Jik;Jung, Ki-Sang;Cho, Seong-Ik
    • Journal of the Institute of Electronics Engineers of Korea SC
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    • v.46 no.2
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    • pp.72-77
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    • 2009
  • In this paper, a 3.2Gb/s clock and data recovery (CDR) circuit for a high-speed serial data communication without the reference clock is described This CDR circuit consists of 5 parts as Phase and frequency detector(PD and FD), multi-phase Voltage Controlled-Oscillator(VCO), Charge-pumps (CP) and external Loop-Filter(KF). It is adapted the PD and FD, which incorporates a half-rate bang-bang type oversampling PD and a half-rate FD that can improve pull-in range. The VCO consists of four fully differential delay cells with rail-to-rail current bias scheme that can increase the tuning range and tuning linearity. Each delay cell has output buffers as a full-swing generator and a duty-cycle mismatch compensation. This materialized CDR can achieve wide pull-in range without an extra reference clock and it can be also reduced chip area and power consumption effectively because there is no additional Phase Locked- Loop(PLL) for generating reference clock. The CDR circuit was designed for fabrication using 0.18um 1P6M CMOS process and total chip area excepted LF is $1{\times}1mm^2$. The pk-pk jitter of recovered clock is 26ps at 3.2Gb/s input data rate and total power consumes 63mW from 1.8V supply voltage according to simulation results. According to test result, the pk-pk jitter of recovered clock is 55ps at the same input data-rate and the reliable range of input data-rate is about from 2.4Gb/s to 3.4Gb/s.

Prediction of the Fractures at Inexcavation Spaces Based on the Existing Data (터널의 굴착면 전반부에 분포하는 절리의 예측)

  • Hwang, Sang-Gi
    • The Journal of Engineering Geology
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    • v.24 no.4
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    • pp.643-648
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    • 2014
  • Understanding of fracture networks and rock mass properties during tunnel construction is extremely important for the prediction of dangers during excavation, and for deciding on appropriate excavation techniques and support. However, rapid construction process do not allow sufficient time for surveys and interpretations for spatial distributions of fractures and rock mass properties. This study introduces a new statistical approach for predicting joint distributions at foreside of current excavation face during the excavation process. The proposed methodology is based on a cumulative space diagram for joint sets. The diagram displays the cumulative spacing between adjacent joints on the vertical axis and the sequential position of each joint plotted at equally spaced intervals on the horizontal axis. According to the diagram, the degree of linearity of points representing the regularity of joint spacing; a linear trend of the points indicates that the joints are evenly spaced, with the slope of the line being directly related to the spacing. The linear points which are stepped indicates that the fracture set show clustered distribution. A clustered pattern within the linear group of points indicates a clustered joint distribution. Fractures surveyed from an excavated space can be plotted on this diagram, and the diagram can then be extended further according to the plotted diagram pattern. The extension of the diagram allows predictions about joint spacing in areas that have not yet been excavated. To test the model, we collected and analyzed data during excavation of a 10-m-long tunnel. Fractures in a 3-m zone behind the excavation face were predicted during the excavation, and the predictions were compared with observations. The methodology yielded reasonably good predictions of joint locations.

Analytical Method Development and Monitoring of Residual Solvents in Dietary Supplements (건강기능식품 중 잔류용매 분석법 개발 및 모니터링)

  • Lee, Hwa-Mi;Shin, Ji-Eun;Jang, Young-Mi;Kim, Hee-Yun;Kim, Mee-Hye
    • Korean Journal of Food Science and Technology
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    • v.42 no.4
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    • pp.390-397
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    • 2010
  • Residual solvents in foods are defined as organic volatile chemicals used or produced in manufacturing of extracts or additives, or functional foods. The solvents are not completely eliminated by practical manufacturing techniques and they also may become contaminated by solvents from packing, transportation or storage in warehouses. Because residual solvents have no nutritional value but may be hazardous to human health, there is a need to remove them from the final products or reduce their amounts to below acceptable levels. The purpose of this study was to develop and evaluate an analytical method for the screening of residual solvents in health functional foods. Furthermore, the aim of this study was to constitute a reasonable management system based on the current state of the market and case studies of foreign countries. Eleven volatile solvents such as MeOH, EtOH, trichloroethylene and hexane were separated depending on their column properties, temp. and time using Gas Chromatography (GC). After determining the GC conditions, a sample preparation method using HSS (Head Space Sampling) was developed. From the results, a method for analyzing residual solvents in health functional foods was developed considering matrix effect and interference from the sample obtained from the solution of solvents-free health functional foods spiked with 11 standards solutions. Validation test using the developed GC/HSS/MS (Mass Spectrometry) method was followed by tests for precision, accuracy, recovery, linearity and adequate sensitivity. Finally, examination of 104 samples grouped in suits was performed by the developed HSS/GC/MS for screening the solvents. The 11 solvents were isolated from health functional foods based on vapor pressure difference, and followed by separation within 15 minutes in a single run. The limt of detection (LOD), limit of quantification (LOQ), recovery and coefficient of variation (C.V.) of these compounds determined by the HSS/GC/MS were found to be 0.1 pg/mL, 0.1-125 pg/g, 51.0-104.6%, and less than 15%, respectively. Using the developed HSS/GC/MS method, residual solvent from 16 out of 104 health functional products were detected as a EtOH. This method therefore seems t o be a valuable extension ofanalytical method for the identification of residual solvents in health functional food.

Determination of trace impurities of HFC-134a by gas chromatograph with atomic emission detector (GC/AED) (GC/AED를 이용한 HFC-134a의 미량 불순물 분석)

  • Kim, Myeongja;Lim, Jeongsik;Lee, Jinbok;Lee, Jeongsoon
    • Analytical Science and Technology
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    • v.30 no.5
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    • pp.240-251
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    • 2017
  • 1,1,1,2-Tetrafluoroethane (HFC-134a), which is used as refrigerant in air conditioners, has been recently regulated as a greenhouse gas and is recommended for reuse by refining. It is very important to quantitatively analyze trace impurities present in the refrigerant to evaluate the criteria for reuse. In this study, trace impurities including C, H, Cl, and F, which are difficult to quantify because there are no reference materials, were quantitatively analyzed by a gas chromatograph-atomic emission detector (GC/AED); for this analysis, this was preceded by a qualitative analysis with a GC-mass selective detector (GC/MSD). In addition, the AED response was investigated using a hydrocarbon mixed reference material, which was proportional to the number of atoms in the component. Fifteen refrigerant components were detected as trace impurities in HFC-134a by qualitative analysis of trace impurities including C, H, Cl, and F in the samples. Based on the results of the qualitative analysis, quantitative analysis of trace impurities using AED showed that the highest mole fractions were for the $CHClF_2$ component ($45438.38{\mu}mol/mol$) in one sample and for the $C_2H_2ClF_3$ component ($1311.47{\mu}mol/mol$) in another sample. From this study, it has been shown that it is possible for this analytical method to be applied to the qualitative and quantitative analysis of trace compounds in refrigerants, which are difficult to quantify because of the absence of reference materials.

Improvement in the Dispersion Stability of Iron Oxide (Magnetite, Fe3O4) Particles with Polymer Dispersant Inject (고분자 분산제 주입을 통한 철산화물(Magnetite, Fe3O4) 입자의 분산 안정성 향상)

  • Song, Geun Dong;Kim, Mun Hwan;Lee, Yong Taek;Maeng, Wan Young
    • Applied Chemistry for Engineering
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    • v.24 no.6
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    • pp.656-662
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    • 2013
  • The iron oxide ($Fe_3O_4$) particles in the coolant of the secondary system of a nuclear power plant reduce the heat transfer performance or induce corrosion on the surface of the heat transfer tube. To prevent these problems, we conducted a study to improve the dispersion stability of iron oxide using polymeric dispersant injection in simulated secondary system water. The three kinds of anionic polymers containing carboxyl groups were selected. The dispersion characteristics of the iron oxide particles with the polymeric dispersants were evaluated by performing a settling test and measuring the transmission, the zeta potential, and the hydrodynamic particle size of the colloid solutions. Polymeric dispersants had a significant impact on the iron oxide dispersion stability in an aqueous solution. While the dispersant injection tended to improve the dispersion stability, the dispersion stability of iron oxide did not increase linearly with an increase in the dispersant concentration. This non-linearity is due to the agglomerations between the iron oxide particles above a critical dispersant concentration. The effect of the dispersant on the dispersion stability improvement was significant when the dispersant concentration ratio (ppm, dispersant/magnetite) was in the range of 0.1 to 0.01. This suggests that the optimization of dispersant concentration is required to maximize the iron oxide removal effect with the dispersant injection considering the applied environments, the iron oxide concentration and the concentration ratio of dispersant to iron oxide.

Flexural Behavior of RC Beam Repaired with Polymer Mortar (폴리머 모르타르로 보수된 철근콘크리트 보의 휨 거동)

  • Cho, Yong-In;Han, Sang-Hoon;Park, Jea-Kyu;Yeon, Yeong-Mo;Hong, Ki-Nam
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.21 no.1
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    • pp.91-99
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    • 2017
  • The purpose of this paper is to evaluate the flexural performance of reinforced concrete (RC) beams repaired with polymer mortar. The repaired and non-repaired 13th beams which was fabricated by considering repair position, repair depth, and curing age of polymer mortar as test variables were tested under three point loading. All specimens repaired in compressive and tensile zone did not fail due to interfacial failure between polymer mortar and concrete but failed when the strain of repaired mortar exceeded the ultimate tensile strain of polymer mortar. Maximum load of specimens repaired in compressive zone was similar to that of non-repaired specimen, reference specimen. Additionally, their ductility index was higher than that of reference specimen. On the other hand, specimens repaired in tensile zone failed very brittlely and have a lower ductility index than reference specimen. Nonlinear analysis by using OpenSees was performed to predict the behavior of RC beam repaired with polymer mortar. Two dimension frame element was used to simplify an analysis model and fiber model was applied to consider the material non-linearity. It was confirmed from the analysis results that nonlinear analysis properly predicts the behavior of specimens repaired in compressive zone and overestimates the behavior of specimens repaired in tensile zone.

GEOMETRIC NINLINEAR ANALYSIS OF UNERGROUND LAMINATED COMPISITE PIPES (기하학적 비선형을 고려한 지하매설 복합재료 파이프의 해석)

  • 김덕현;이인원;변문주
    • Computational Structural Engineering
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    • v.2 no.1
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    • pp.65-70
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    • 1989
  • An analytical study was conducted using the Galerkin technique to determine behaviour of thin fibrereinforced and laminated composite pipes under soil pressure. Geometric nonlinearity and material linearity have been assumed. It is assumed that vertical and lateral soil pressure are proportional to the depth and lateral displacement of the pipe respectively. It is also assumed that radial shear stress is negligible because the ratio of thickness to the radius of pipe is very small. The above results are verified by the finite element analysis.

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Improvement of the Method using the Coefficient of Variation for Automatic Multi-segmentation Method of a Rating Curve (수위-유량관계곡선의 자동구간분할을 위한 변동계수 활용기법의 개선)

  • Kim, Yeonsu;Kim, Jeongyup;An, Hyunuk;Jung, Kwansue
    • Journal of Korea Water Resources Association
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    • v.48 no.10
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    • pp.807-816
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    • 2015
  • In general, the water stage-discharge relationship curve is established based on the assumptions of linearity and homoscedasticity. However, the relationship between the water stage and discharge is affected from geomorphological factors, which violates the basic assumptions of the water stage-discharge relationship curve. In order to reduce the error due to the violations, the curve is divided into several sections based on the manager's judgement considering change of cross-sectional shape. In this research, the objective-splitting criteria of the curve is proposed based on the measured data without the subjective decision. First, it is assumed that the coefficient of variation follows the normal distribution. Then, if the newly calculated coefficient of variation is outside of the 95% confidential interval, the curve is divided. Namely, the groups is divided by the characteristics of the coefficient of variation and the reasonable criteria is provided for establishing a multi-segmented rating curve. To validate the proposed method, it was applied to the data generated by three artificial power functions. In addition, to confirm the applicability of the proposed method, it is applied to the water stage and discharge data of the Muju water stage gauging station and Sangegyo water stage gauging station. As a result, it is found that the automatically divided rating curve improves the accuracy and extrapolation accuracy of the rating curve. Finally, through the residual analysis using Shapiro-Wilk normality test, it is confirmed that the residual of water stage-discharge relationship curve tends to follow the normal distribution.

Analytical Method Validation of Quercetin in Changnyeong Onion Extract as a Functional Ingredient for Functional Health Food (건강기능식품 기능성원료로서 창녕양파추출액의 지표성분 Quercetin 분석법)

  • Jeon, Seon-Young;Jeong, Eun-Jeong;Baek, Jeong-Hwa;Cha, Yong-Jun
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.40 no.4
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    • pp.565-569
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    • 2011
  • Validation of quercetin as a marker compound in the standardization of Changnyeong onion extract developed for functional health food was attempted by analytical method. The specificity was satisfied with retention time and photo diode array (PDA) spectrum by analysis of quercetin using HPLC and comparison with standard compound. It showed a high linearity in the calibration curve as coefficient of correlation ($R^2$) of 0.9986, and the limit of detection (LOD) and limit of quantitation (LOQ) were 0.2 mg/L and 0.5 mg/L, respectively. Recovery rate test with quercetin concentration of 0.05, 0.075 and 0.1 mg/mL was revealed in the high range of 82.36~95.26%, 82.70~98.24% and 87.91~95.11%, respectively. The intra-day and inter-day precision in quercetin for Changnyeong onion extracts was 0.10~3.28% and 0.96~5.79%, respectively. Therefore, application of quercetin was validated in analytical method as a marker compound in Changnyeong onion extracts.