• Applied Microscopy
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• 제29권1호
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• pp.75-81
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• 1999

본 실험에서 얻어진 결론을 요약하면 아래와 같다. (1) 저진공도의 sputter coater를 이용하여 Au 내부 표준시편을 제작하는 최적 조건은 9mA의 전류로 100 초간 coating하는 것이다. (2) 고진공도의 evaporation coater를 이용하여 Al 내부 표준시편을 제작하는 최적 조건은 7kV의 전압으로 10분간 coating하는 것이다. (3) Au 내부 표준시편을 이용하여 측정한 홍주석 격자상수 값의 측정오차는 정밀도가 1.2% 이하이고, 정확도는 0.3% 이하이다. (4) Au 내부 표준시편을 이용하여 측정한 알바이트 장석 격자상수 값의 측정오차는 정밀도가 0.5% 이하이고, 정확도는 1.1% 이하이다. (5) 내부 표준시편을 사용하여 격자상수를 측정할 때 가장 심각한 오차는 전자회절도형의 거리 및 각도 측정시 발생한다. 체계적인 측정 방법과 정밀도 높은 측정 도구의 사용이 필요하다. (6) 시료나 TEM 조건 때문에 분말 XRD 방법이나 수렴성빔 전자회절법으로 격자상수를 구할 수 없는 경우에는 내부 표준시편을 이용한 TEM 격자상수 측정법이 좋은 대안이 된다.

• 한국재료학회지
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• 제21권12호
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• pp.697-702
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• 2011

Two-dimensional (2D) nano patterns including a two-dimensional Bravais lattice were fabricated by laser interference lithography using a two step exposure process. After the first exposure, the substrate itself was rotated by a certain angle, $90^{\circ}$ for a square or rectangular lattice, $75^{\circ}$ for an oblique lattice, and $60^{\circ}$ for a hexagonal lattice, and the $90^{\circ}$ and laser incident angle changed for rectangular and the $45^{\circ}$ and laser incident angle changed for a centered rectangular; we then carried out a second exposure process to form 2D bravais lattices. The band structure of five different 2D nano patterns was simulated by a beam propagation program. The presence of the band-gap effect was shown in an oblique and hexagonal structure. The oblique latticed ZnO nano-photonic crystal array had a pseudo-bandgap at a frequency of 0.337-0.375, 0.575-0.596 and 0.858-0.870. The hexagonal latticed ZnO nano-crystallite array had a pseudo-bandgap at a frequency of 0.335-0.384 and 0.585-0.645. The ZnO nano structure with an oblique and hexagonal structure was grown through the patterned opening window area by a hydrothermal method. The morphology of 2D nano patterns and ZnO nano structures were investigated by atomic force microscopy and scanning electron microscopy. The diameter of the opening window was approximately 250 nm. The height and width of ZnO nano-photonic crystals were 380 nm and 250 nm, respectively.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2007년도 춘계학술대회B
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• pp.2731-2736
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• 2007

In this paper, incompressible flow over a cylinder near a plane wall using the Immersed Boundary. Finite Difference Lattice Boltzmann Method (IB-FDLBM) is implemented. In this present method, FDLBM is mixed with IBM by using the equilibrium velocity. We introduce IBM so that we can easy to simulate bluff-bodies. With this numerical procedure, the flow past a circular cylinder near a wall is simulated. We calculated the flow patterns about various Reynolds numbers and gap ratios between a circular cylinder and plane wall. So these are enabled to observe for vortex shedding. The numerical results are found to be in good agreement with those of previous studies.

• 한국소음진동공학회:학술대회논문집
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• 한국소음진동공학회 2007년도 춘계학술대회논문집
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• pp.978-982
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• 2007

A new neuro-control scheme for active control of structures is proposed. It utilizes lattice pattern of state vector as training data of probabilistic neural network (PNN). Therefore, it is the so-called lattice probabilistic neural network (LPNN). PNN makes control forces by using all the training patterns. Therefore, it takes much time to obtain a control force in application. This inevitably may delay the control action. However, control force of LPNN is calculated by using only the adjacent information of LPNN input. So, the response of LPNN is greatly faster than PNN. The proposed control algorithm is applied for one story building under California and El Centro earthquakes. Also, control results of the LPNN are compared with those of the conventional PNN. The structural responses have been suppressed effectively by the proposed algorithm.

• Bulletin of the Korean Chemical Society
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• 제29권10호
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• pp.1969-1972
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• 2008

In this study, horse spleen apoferritins were induced to form biominerals using up to 3000 Fe atoms per protein molecule. The morphology and crystallinity of the nanometer-sized biominerals formed in the ferritins were then analyzed using field emission-energy filtering-transmission electron microscopy (FE-TEM). The ferritins were found to have reconstitution yields of 60-70% in the experiments. The mean core size of the ferritins varied somewhat with protein concentrations, indicating that crystal growth in ferritins could be controlled via protein concentrations. The core mineral size increased with the amount of Fe used. Lattice fringes of the core, associated with good crystallinity, were found in all samples. The lattice fringe images of a single domain ferrihydrite mineral appeared frequently in the (011) planes (d-spacing of 0.246 nm) under [100] zone axis in all samples of this study. In addition, the lattice image occasionally revealed fringes corresponding to the (100) planes (d = 0.254 nm) from the [001] zone axis, indicating the characteristic pattern of hexagonal crystal lattice. Diffraction patterns in the minerals identified as ferrihydrite were fitted well into the space group of $P3_{1c}$.

• 한국정보처리학회논문지
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• 제6권8호
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• pp.2088-2097
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• 1999

소프트웨어 도메인모형(Domain Model)으로부터 행위패턴을 식별하고, 개발 시스템의 동적 행위를 구체화한 사용 사례추출 및 구조화로 재사용을 증진시키는 소프트웨어 프레임워크(Framework) 구축방법을 제안한다. 대부분의 소프트웨어 행위모형이 이질적인 개발자의 요구사항이나 의도를 일관성 있게 모형화 하지 못하며, 재개발과 유지보수를 위한 구체적인 활용방안이 마련되어 있지 못하다. 따라서, 행위패턴을 식별하고 시스템에 반응하는 구체적인 기능성 항목인 사용 사례(Use Case)를 구조화하여 개발된 모형의 일관성을 보완하고, 재사용과 유지보수를 하는 재사용 프레임워크를 구축한다. 사용 사례의 구조화를 위해 격자모형(Lattice Model)이 이용되며, 재사용 구성항목을 추출하도록 유도할 수 있는 재사용 프로세스 구조와 세부절차를 소개한다.

• 한국멀티미디어학회논문지
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• 제3권6호
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• pp.566-574
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• 2000

HMM이 시계열 모델로써 우수함이 널리 입증되면서 이차원 모델로 확장해 보려는 연구 결과도 늘어났지만 아직까지 임의의 객 체 패턴의 다양한 변형을 모델링하기에는 너무 단순한 경우가 대부분이다. 따라서 HMM이 시계열 데이터에서 보여준 성과를 영상 데이터에서 기대하기는 어렵다. 즉, 아직 대부분의 모델이 2D HMM으로 보기에는 부족하다고 판단된다. 본 논문에서 제안하는 모델은 이 차원 공간에서 상하, 좌우 방향의 진행 관계(causality)가 존재하는 은닉 마르코프 격자 또는 HML이다. 여기에 격자 구성 조건을 추가하여 모델 평가와 디코딩, 그리고 MLE 매개변수 추정법에 의한 훈련 알고리즘을 이론적으로 유도, 개발하였다. 본 모델은 기존의 필드형 모델과 달리 필기 문자 영상과 같이 다양한 국소적 형태 변형을 효과적으로 모델링하는 유용한 방법으로 사용될 수 있다.

• 한국전기전자재료학회논문지
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• 제15권1호
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• pp.24-29
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• 2002

In this paper, the microstructure and the dielectric properties of Sr$\_$1-x/CaxTiO$_3$(0$\leq$x$\leq$0.2)-based grain boundary layer ceramics were investigated. The sintering temperature and time were 1420∼152 0$\^{C}$ and 4 hours in N$_2$ gas, respectively. The average grain size and the lattice constant were decreased with increasing content of Ca, but the average grain size was increased with increase of sintering temperature. The second phase foamed by the thermal diffusion of CuO from the surface leads to verb high apparent dielectric constant, $\xi$$\_$r/>50000 and low dielectric loss, tan$\delta$<0.05. X-ray diffraction patterns of Sr$\_$1-x/CaxTiO$_3$ exhibited cubic structure, and the peaks shifted upward and the peak intensity were decreased with x. This is due to the lattice contraction as Sr is replaced by Ca with a smaller ionic radius. The specimens treated thermal diffusion for 2hrs in 1150$\^{C}$ exhibited nonlinear current-voltage characteristic, and its nonlinear coefficient(a) was overt 7.

• Applied Microscopy
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• 제44권4호
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• pp.144-149
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• 2014

A strategy for phase identification of precipitates in high Al-containing austenitic and ferritic steels using electron diffraction (ED) is studied. Comparative studies of the various Al-containing precipitates (k-carbide, $Ni_3Al$, $Fe_3Al$, FeAl) show the similarities of crystal structure and lattice parameter. However, the slight differences of lattice parameter and structure display characteristic ED patterns (EDPs) which can be identified. $L1_2$ k-carbide and $Ni_3Al$ can be differentiated by the length of ${\rightarrow}_g$ (the reciprocal lattice vector), even though they show perfectly identical shapes of EDPs. $DO_3$ $Fe_3Al$ and $B_2$ FeAl show the characteristic EDs in [110] and [112] beam directions due to the differences of Fe site occupancies in unit cells. k-carbide, $Ni_3Al$, and FeAl show also the similar EDs in [112], [112], and [110] beam directions, respectively. All the possible similarities of EDs among each phases and the strategy for phase identification are discussed on the bases of kinematical ED simulation.

• 한국세라믹학회지
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• 제35권10호
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• pp.1113-1119
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• 1998

Crystal structure of needle-shaped maghemite(${\gamma}$-{{{{ { {Fe }_{2 }O }_{3 } }}) has been studied by the Rieveld analysis of powder X-ray diffraction patterns. The tetragonal space group P41,.3212 and cubic space group P41,.32 have been have been used for the refinement of X-ray diffraction patterns. The crystal system of maghemite is closed to tetragonal more than cubic. The tetragonal lattice parameters are a=8.3460$\AA$ and c=25.034$\AA$ The standard X-ray diffraction pattern of the tetragonal maghemite analyzed with space group P41,.3212 is proposed.