• Title/Summary/Keyword: lattice pattern

Search Result 169, Processing Time 0.027 seconds

Charge Transformation of CU-ions in CuxFe3-xO4 (χ=0.1, 0.2)

  • Lee, Choong Sub;Lee, Chan Young;Kwon, Dong Wook
    • Journal of Magnetics
    • /
    • v.7 no.2
    • /
    • pp.25-28
    • /
    • 2002
  • Slowly cooled $Cu_xFe_{3-x}O_4$ ($\chi$=0.1, 0.2) have been investigated over a temperature range from 82 to 700 K using the M$\ddot{o}$ssbauer technique. X-ray diffraction shows that these have a single-phase cubic spinel structure of lattice parameters $\alpha$=8.396 and 8.398${\AA}$, respectively. Since Cu ions prefer B (octahedral) sites to A (tetrahedral) sites, the ionic distribution is $(Fe)_A[Fe_{2-x}Cu_x]_BO_4$. M$\ddot{o}$ssbauer spectra consisted of two sets of 6-line pattern from. A site in ferric state and B site in ferrous-ferric state. Intensity ratio of B to A subspectra is 1.0 at 82 K and increases to 2.0 at 700 K with increasing temperature. After annealing the samples under vacuum at $450^circ{C}$ for a half hour, x-ray diffraction patterns have the peaks of magnetite- and hematite-phase. Lattice constants of magnetite-phase are 8.395 and 8.392 ${\AA}$ smaller than 8.396 and 8.398 ${\AA}$ before annealing, respectively. M$\ddot{o}$ssbauer spectra reveal the conventional magnetite pattern with the additional hematite pattern. Intensity ratios of B to A subspectra fur magnetite-phase become 1.9-2.0 over all temperature ranges and Cu ions are distributed over A and B sites randomly. Ratios of hematite to total intensity in M$\ddot{o}$ssbauer spectra for $\chi$= 0.1 and $\chi$= 0.2 are 10 and 21%, respectively. These hematite ratios may be due to annealing under vacuum at $450^circ{C}$, which transforms $Cu^{2+}$ ionic states into $Cu^{1+}$. Verwey temperatures far $\chi$= 0.1 and $\chi$= 0.2 are $123\pm2$ K and $128\pm2$ K.

A Study on Tensile Strength Dependent on Variation of Output Condition of the X-shape Infill Pattern using FFF-type 3D Printing (융합 필라멘트 제조 방식의 3D 프린팅을 이용한 X자 형상 내부 채움 패턴의 출력 옵션 변화에 따른 인장강도 연구)

  • D. H. Na;H. J. Kim;Y. H. Lee
    • Transactions of Materials Processing
    • /
    • v.33 no.2
    • /
    • pp.123-131
    • /
    • 2024
  • Plastic, the main material of FFF-type 3D printing, exhibits lower strength compared to metal. research aimed at increasing strength is needed for use in various industrial fields. This study analyzed three X-shape infill patterns(grid, lines, zigzag) with similar internal lattice structure. Moreover, tensile test considering weight and printing time was conducted based on the infill line multiplier and infill overlap percentage. The three X-shape infill patterns(grid, lines, zigzag) showed differences in nozzle paths, material usage and printing time. When infill line multiplier increased, there was a proportional increase in tensile strength/weight and tensile strength/printing time. In terms of infill overlap percentage, the grid pattern at 50% and the zigzag and lines patterns at 75% demonstrated the most efficient performance.

Synthesis and Comparative Analysis of Crystallite Size and Lattice Strain of Pb2Ba1.7Sr0.3Ca2Cu3O10+δ Superconductor

  • Hasan, Maher Abd Ali;Jasim, Kareem Ali;Miran, Hussein Ali Jan
    • Korean Journal of Materials Research
    • /
    • v.32 no.2
    • /
    • pp.66-71
    • /
    • 2022
  • In this article, Pb2Ba1.7Sr0.3Ca2Cu3O10+δ superconductor material was synthesized using conventional solid-state reaction method. X-ray diffraction (XRD) analysis demonstrated one dominant phase 2223 and some impurities in the product powder. The strongest peaks in the XRD pattern were successfully indexed assuming a pseudo-tetragonal cell with lattice constants of a = 3.732, b = 3.733 and c = 14.75 Å for a Pb-Based compound. The crystallite size and lattice strain between the layers of the studied compound were estimated using several methods, namely the Scherrer, Williamson-Hall (W.H), size-strain plot (SSP) and Halder Wagner (H.W) approach. The values of crystallite size, calculated by Scherrer, W.H, SSP and H.W methods, were 89.4540774, 86.658638, 87.7555823 and 85.470086 Å, respectively. Moreover, the lattice strain values obtained by W.H, SSP and H.W methods were 0.0063240, 0.006325 and 0.006, respectively. It was noted that all crystallite size results are consistent; however, the best method is the size-strain plot because it gave a value of R2 approaching one. Furthermore, degree of crystallites was calculated and found to be 59.003321%. Resistivity analysis suggests zero-resistance, which is typical of superconducting materials at critical temperature. Four-probe technique was utilized to measure the critical temperature at onset Tc(onset), zero resistivity Tc(off set), and transition (width ΔT), corresponding to temperatures of 128 K, 116 K, and 12 K, respectively.

Adaptive Image Binarization for Automated Surface Strain Measurment (판재 곡면변형률 자동측정을 위한 적응 2치영상화)

  • Shin, Gun Il;Kwon, Ho Yeol;Kim, Hyong-Jong
    • Journal of Industrial Technology
    • /
    • v.17
    • /
    • pp.21-29
    • /
    • 1997
  • In this paper, an adaptive image binarization scheme is proposed for automated surface strain measurement. At first, we reviewed an image based 3D deformation factor measurement briefly. Then, a new adaptive thresholding method is proposed for the extraction of lattice pattern from a deformed plate image using its local mean and variance. Some experimental results are presented to verify the effectiveness of our approaches.

  • PDF

Model identification of spatial autoregressive data analysis (공간 자기회귀모형의 식별)

  • 손건태;백지선
    • The Korean Journal of Applied Statistics
    • /
    • v.10 no.1
    • /
    • pp.121-136
    • /
    • 1997
  • Spatial data is collected on a regular Cartesian lattice. In this paper we consider the model indentification of spatial autoregressive(SAR) models using AIC, BIC, pattern method. The proposed methods are considered as an application of AIC, BIC, 3-patterns for SAR models through three directions; row, column and diagonal directions. Using the Monte Carlo simulation, we test the efficiency of the proposed methods for various SAR models.

  • PDF

The Design of Self-Organizing Map Using Pseudo Gaussian Function Network

  • Kim, Byung-Man;Cho, Hyung-Suck
    • 제어로봇시스템학회:학술대회논문집
    • /
    • 2002.10a
    • /
    • pp.42.6-42
    • /
    • 2002
  • Kohonen's self organizing feature map (SOFM) converts arbitrary dimensional patterns into one or two dimensional arrays of nodes. Among the many competitive learning algorithms, SOFM proposed by Kohonen is considered to be powerful in the sense that it not only clusters the input pattern adaptively but also organize the output node topologically. SOFM is usually used for a preprocessor or cluster. It can perform dimensional reduction of input patterns and obtain a topology-preserving map that preserves neighborhood relations of the input patterns. The traditional SOFM algorithm[1] is a competitive learning neural network that maps inputs to discrete points that are called nodes on a lattice...

  • PDF

니켈기 전열관 소재에서의 결정립계 Misorientation 분석

  • 이용복;이덕열;장진성;이창규;국일현
    • Proceedings of the Korean Nuclear Society Conference
    • /
    • 1997.05b
    • /
    • pp.189-194
    • /
    • 1997
  • 니켈기 전열관 소재에서 결정립계의 misorientation을 분석하였다. 일반적으로 대부분의 결정립계에서 석출물을 관찰 할 수 있지만 쌍정과 만나게 되면서 석출물의 분포가 갑작스럽게 변하는 것을 관찰 할 수 있다. 이러한 현상은 결정립계의 구조와 에너지에 관련되는 결정립계의 misorientation 특성에 갑작스런 변화가 생겨나기 때문이라. 이러한 결정립계의 misorientation 특성은 T.E.M (Transmission Electro Microscope)에서 얻은 각 결정립의 Kikuchi pattern을 이용하여 분석하었다. 석출물을 갖는 결정립계들은 random high angle 결정립계이고 석출물이 존재하지않는 결정립계들은 특정한 C.S.L ( Coincidence Site Lattice) 결정립계이었다.

  • PDF

Study on The Wine Mini-bar Design Using Chinese 卍 Shape Window-pattern (중국의 전통 만(卍)자 문창살이 적용된 와인장 디자인 연구)

  • Cai, Quan;Kim, Chung-Ho
    • Journal of the Korea Furniture Society
    • /
    • v.28 no.1
    • /
    • pp.47-52
    • /
    • 2017
  • With the rapid economical and technological progress in China, the demand for wine increased tremendously along with the need for wine storage furniture and wine related products. Although demand for furniture increased, consumers' emotional need toward high quality design product has not been met properly. As the quality of people's life improves, they pursue better materials providing them with higher mental satisfaction. To meet the specific demand of Chinese market stated above, the direction of this report is set as to study pattern elements of Chinese traditional lattice and combine them with wine storage furniture design and crafting, which is originated from western culture. By doing that, the study is aimed to suggest a new direction of Chinese modern design and to improve the fundamental notion of Chinese furniture design. Although wine and wine racks are from western world, the wine mini-bar designed in this study stands out for its beauty and taste of eastern culture. It not only fits perfectly to the habits and taste of wine lovers, but also goes very well with fusion style interior design trend in modern China. The furniture carries the charm of eastern cultural tradition and elegance of modern furniture design in one.

Development of Traditional Cultural Products Using Persimmon Dyeing (감물염색을 활용한 전통 문화상품의 개발)

  • Lee, Eun-Jin;Kim, Sun-Kyung;Cho, Hyo-Sook
    • The Research Journal of the Costume Culture
    • /
    • v.15 no.6
    • /
    • pp.1053-1062
    • /
    • 2007
  • This study purposed to restructure representative traditional patterns formatively, manufacture actual cultural products with traditional dyeing technique using persimmon, and commercialize the results of the research. Traditionally in Korea, the dying of natural fiber such as cotton, flax and silk with persimmon was called Galmul dyeing, and clothes made through Galmul dyeing were called Galot. Galot was very useful because it is strong, does not pick up dirt easily, dries easily, and is cool in summer. In addition, cloth dyed with persimmon becomes stiff, so it does not need to be starched or ironed after washing. Moreover, it does not transmit heat under direct rays and is highly air-permeable, so it is cool and useful for standing the heat. In this study, we used traditional persimmon dyeing technique, printing traditional patterns fit for contemporary people's aesthetic sense not through dip-dying but through printing. When persimmon dyeing is used in expressing patterns, it produces not only visual effect but also embossing effect due to the characteristic of persimmon that makes printed patterns stiff, so we can obtain unique texture distinguished from other printing methods. We chose seven motive patterns, which were lotus pattern symbolizing eternal life, peony pattern symbolizing wealth and rank and prosperity, character Su(壽) pattern widely used as a symbol of health, bird and cloud pattern in the Goryeo Dynasty, Sahapyeoeuisohwa(四合如意小花) pattern printed on brocade in the Goryeo Dynasty, lattice pattern, cloth pattern on wall paintings from the Period of the Three Kingdoms. From each pattern chosen as a motive was extracted unit patterns and the original pattern was restored using Adobe Illustrator. Restored patterns were restructured to be applied to cultural products fit for contemporary formative sense. Fabrics used in dyeing were cotton, linen, ramie, silk, and polyester. Although the same persimmon dyeing was applied, we produced different feelings of patterns using various fabrics and in some cases gold and silver powder was added for the effect of gloss in addition to the embossing of patterns. Using printed fabrics we manufactured tea pads, place mats, cushions, wrapping cloth for gifts, wallet, lampshades.

  • PDF

Biosynthesis of Silver Nanoparticles by Phytopathogen Xanthomonas oryzae pv. oryzae Strain BXO8

  • Narayanan, Kannan Badri;Sakthivel, Natarajan
    • Journal of Microbiology and Biotechnology
    • /
    • v.23 no.9
    • /
    • pp.1287-1292
    • /
    • 2013
  • Extracellular biogenic synthesis of silver nanoparticles with various shapes using the rice bacterial blight bacterium Xanthomonas oryzae pv. oryzae BXO8 is reported. The synthesized silver nanoparticles were characterized by UV-Vis spectroscopy, powder X-ray diffractometry (XRD), scanning electron microscopy, energy dispersive X-ray spectrometry, and high-resolution transmission electron microscopy (HR-TEM). Based on the evidence of HR-TEM, the synthesized particles were found to be spherical, with anisotropic structures such as triangles and rods, with an average size of 14.86 nm. The crystalline nature of silver nanoparticles was evident from the bright circular spots in the SAED pattern, clear lattice fringes in the high-resolution TEM images, and peaks in the XRD pattern. The FTIR spectrum showed that biomolecules containing amide and carboxylate groups are involved in the reduction and stabilization of the silver nanoparticles. Using such a biological method for the synthesis of silver nanoparticles is a simple, viable, cost-effective, and environmentally friendly process, which can be used in antimicrobial therapy.