• Title/Summary/Keyword: lR Curve

Search Result 328, Processing Time 0.026 seconds

Analysis of the Magnetic Properties of RFe11Ti and RFe11TiH (R=Tb,Ho)

  • Xu, S.W.;Yan, Y.;Jin, H.M.;Wang, X.F.;Wang, W.Q.;Su, F.
    • Journal of Magnetics
    • /
    • v.8 no.4
    • /
    • pp.153-156
    • /
    • 2003
  • The values of crystalline-electric-field parameters $A_{nm}$ for $RFe_{11}$Ti $H_{x}$ (R=Tb,Ho) (x=0,l) are obtained by fitting calculations to the magnetization curves along the crystal axes at 4.2 K and higher temperatures. The insertion of H element in RFe$_{11}$Ti significantly affects CEF parameters $A_{nm}$ . By using exchange field 2${\mu}$$_{B}$ $H_{ex}$ derived by inelastic neutron scattering and fitted $A_{nm}$ , the calculations reproduce the experimental curves well.

Simultaneous Determination of Plasma Lactate, Pyruvate, and Ketone Bodies following tert-Butyldimethylsilyl Derivatization using GC-MS-SIM

  • Yoon, Hye-Ran
    • Biomedical Science Letters
    • /
    • v.21 no.4
    • /
    • pp.241-247
    • /
    • 2015
  • Lactate and ketone bodies are considered biological markers for ketosis and several inherited metabolic disorders. In the current study, the specific ratios of lactate and ketone bodies as analytical tools for differential diagnosis of various lactic acidosis were devised. The study included a protein precipitation step following tert-butyldimethylsilyl derivatisation. Total run time was approximately 30 min including sample preparation and GS/MS analysis. The limits of detection were below 0.1 pg/mL over the targeted 4 analytes. The calibration curve was linear over the concentration range of $0.001{\sim}250{\mu}g/mL$ for pyruvate, beta-hydroxybutyrate, and acetoacetate ($R^2$ > 0.99). Inter-day accuracy and precision were 87.7~94.8% with RSD of 2.5~5.7% at 2 levels. Absolute recoveries (%) of target analytes were 87.0~98.4%. The method was validated for the quantification of lactate and ketone bodies for differentiation of lactic acidosis.

Large Cryosorption Pump for the NBI Test Stand

  • In, S.R.;Shim, H.J.
    • Journal of Korean Vacuum Science & Technology
    • /
    • v.7 no.2
    • /
    • pp.27-32
    • /
    • 2003
  • A large cryo-pumping system composed of 4 cryosorption pumps was designed and manufactured to satisfy the pressure requirements of the NBI test stand. The cryosorption pump consists of a thermal shield/baffle assembly and a cryopanel coated with activated carbon granules. The thermal shield is cooled by liquid nitrogen, and the cryopanel by a commercial helium refrigerator. The operation characteristics and vacuum performance of the cryosorption pump were investigated. The cooling down time of the cryopanel to 20 K was about 6 hours with a liquid nitrogen consumption rate of about 35 L/hr. The maximum pumping speed of the cryosorption pump for the hydrogen gas measured by the steady pressure method was about 90,000 L/s.

  • PDF

The Convective Drying Characteristics of garlic(Allium sativum L.) (마늘의 열풍건조 특성)

  • Jeong, Sin-Gyo;Gang, Jun-Su;Choe, Jong-Uk
    • Food Science and Preservation
    • /
    • v.2 no.1
    • /
    • pp.155-161
    • /
    • 1995
  • We examined the drying characteristics and the drying rate model equation of garlic(allium sativum L.) using computer aided convective drying. The drying chanacteristic curve of garlic divided into constant rate drying period and 2 stage of falling rate drying period. The drying rate was fairly affected by hot air temperatures during the total drying period, but air flow rates has nearly no effect on the drying rate except initial drying period. Of the several model equation, r2 values of page model equation was the highest, and the estimated drying profiles were comparatively coincided with the observed drying profiles. Page model equation was suitable to predict the drying rate and moisture content during drying of sliced garlic.

  • PDF

Determination of DBCP and n-Butylbenzene using SPME with GC-MS (SPME-GC-MS를 이용한 DBCP 및 n-Butylbenzene의 분석)

  • Park, Hyun-Mee;Kim, Young-Man;Lee, Dai-Woon;Lee, Kang-Bong
    • Analytical Science and Technology
    • /
    • v.14 no.6
    • /
    • pp.471-475
    • /
    • 2001
  • Solid phase microextraction(SPME) with $85{\mu}m$-polyacrylate (PA) and $100{\mu}m$-polydimethylsiloxane(PDMS) fibers, coupled to gas chromatography-mass spectrometry was used to determine 1,2-dibromo-3-chloropropane(DBCP) and n-butylbenzene in water. The conditions affecting the SPME process(i.e, extraction time, injection length, injection temperature, desorption time and temperature) were optimized. The linearity of the calibration curve (correlation coefficient, R) was over 0.99 and the limits of detection of the method were between 1.5 and $10.8{\mu}g/L$. Repeatability of the method was between 10.4 and 14.4 %.

  • PDF

Mesh selectivity of gill net for female Japanese sandfish (Arctoscopus japonicus) in spawning season (산란기 도루묵(Arctoscopus japonicus) 암컷의 자망에 대한 망목선택성)

  • Park, Hae-Hoon;Jeong, Eui-Cheol;Bae, Bong-Seong;Yang, Jae-Hyeong;Chol, Soo-Ha;Lee, Sung-Il
    • Journal of the Korean Society of Fisheries and Ocean Technology
    • /
    • v.43 no.4
    • /
    • pp.274-280
    • /
    • 2007
  • The mesh selectivity of gill net for Japanese sandfish (Arctoscopus japonicus) caught in the East Sea, Korea was described. The experiment was conducted with five different kinds of mesh size (39.4, 45.5, 51.5, 53.0, 57.6mm) between November and December 2006 in spawning season. The catch was mostly Japanese sandfish (93.3%) and some others (6.7%), and almost all of the female Japanese sandfish were larger than the fork length at 50% maturity (16.7cm). The selection curve for the female Japanese sandfish caught from the experiments was fitted by the Kitahara's method to a polynomial equation which was $s(R)={\exp}\{(0.2584R^3-5.3445R^2+32.269R-59.868)-0.6585\}$ where R=l/m, and l and m are fork length and mesh size, respectively.

Spectrophotometric Determination of Nickel (Ⅱ) in Tween80 Micellar Medium (Tween80 미셀 용액에서 Ni(Ⅱ)의 분광광도법 정량)

  • Lee, Seung-Kwon;Choi, Hee-Seon
    • Journal of the Korean Chemical Society
    • /
    • v.44 no.3
    • /
    • pp.207-211
    • /
    • 2000
  • We have studied on the determination of Ni(II) using APDC as a complexing agent in Tween80 micellar medium. The absorption spectrum of Ni(PDC)$_2$ complex in Tween80 medium was better defined and more sensitive than that in chloroform Ni(PDC)$_2$ complex was very stable at pH 7.0 and up to 100 minutes, and could be quantitatively chelated when APDC was added to over 10 times moles of Ni(II). The optimum concentration of Tween80 was 0.1%. The calibration curve of Ni(PDC)$_2$ complex with good linearity(R$^2$=0.9955) was obtained in 0.1% Tween80 medium. The detection limit and the determination limit were 0.09 ${\mu}g$/mL and 0.28 ${\mu}g$/mL, respectively. This technique was applied to the analysis of Suwon stream water samples, and about l00% of recoveries were obtained from the spiked samples. Although the formation of Ni(PDC)$_2$ complex was interfered by various metal ions, this technique could be applied to the practical determination of Ni(II).

  • PDF

Age and Growth of Epinephelus akaara in the South Western Sea of Korea (한반도 서남 연안 붉바리(Epinephelus akaara)의 연령과 성장)

  • Lee, Tae-Won;Lee, Chang-Gyu
    • Korean Journal of Ichthyology
    • /
    • v.8 no.2
    • /
    • pp.16-22
    • /
    • 1996
  • Age and growth of Epinephelus akaara were determined using samples collected from the south western sea of Korea. Thin - sectioned otoliths showed relatively well defined annuli when examined under dark - field microscope. Because the fish do not feed at the temperature under $10^{\circ}C$, the annuli in otoliths are considered to be formed during the period between December and April. Considering that the peak spawning season is July, the first annulus must have been formed in 0.5 year after birth. The oldest fish examined was 9 years old, and the largest one was 47cm. The body length(L, cm) was linearly related to the otolith radius (R, ${\mu}m$) : L= - 2.84+7.01 R. Back-calculated lengths for each age using the relationship between body and otolith size were well adjusted to the Von Bertalanffy growth curve : $L_t$=55.5[1-exp{-0.162(t+0.128)}]. Using relationship between length and weight ($W_t$=0.00608$L^{3.21}$), growth in weight was expressed by Wt=2409(1-exp{-0.162(t+0.128)}]$^{3.21}$.

  • PDF

The Usability of Sit to Stand Test Performance in Chronic Stroke (만성 뇌졸중 환자들의 Sit to Stand Test의 임상적 유용성)

  • Cho, Hwi-Young;An, Seung-Heon;Lee, Yun-Bok;Hong, Hyun-Hwa;Lee, Gyu-Chang
    • Journal of the Korean Society of Physical Medicine
    • /
    • v.8 no.4
    • /
    • pp.549-558
    • /
    • 2013
  • PURPOSE: This study is designed as a retrospective study, and identified the clinical usability of Sit to Stand (STS) test for predicting of fall incidence in stroke patients who experienced a fall within 1 year. METHODS: Between July 2011 and November 2012, 69 inpatients with stroke in K rehabilitation hospital were participated under voluntarily signing the informed consent form. STS test and 10m walk test (10MWT) were used to assess the muscle strength of lower-extremity and walking velocity, respectively. Also, we tested dynamic balance and motor function of lower-extremity in affected-side using with the Berg balance scale (BBS) and the Fugl-Meyer assessment of lower extremity (FM-L/E). METHODS: There were significant differences between subjects with fall-experienced group and without subjects without fall-experienced group in STS test, 10MWT, BBS scores and FM-L/E. STS test significantly showed a negative correlation between 10MWT (r=-.657), BBS (r=-.512), and FM-L/E (r=-.563). And, 10MWT have a influence on the performance of STS test (the capacity of explanation = 20%). The cut-off value of STS performance predicting falls experience is ${\geq}14.36$ seconds (sensitivity=76%; specificity=79%, area under curve=.785). According to logistic regression analysis of falls experience, subjects ${\geq}14.36$ s showed that 4.164 times (odd ratio) increased in falls than subjects < 14.36 s in STS test. CONCLUSION: This study demonstrated that STS test may be a useful tool predicting and measuring falls in patients with stroke. Further study will be needed to elucidate the kinematic analysis of STS test and the relationship between physical activity level and falls in stroke patients.

Developing Suspended Sediment Delivery Ratio in the Lake Imha Watershed (임하호유역 유사유달공식 개발)

  • Jeon, Ji-Hong;Choi, Donghyuk;Kim, Jae-Kwon;Kim, Taedong
    • Journal of Korean Society on Water Environment
    • /
    • v.33 no.6
    • /
    • pp.744-753
    • /
    • 2017
  • The sediment delivery ratio (SDR) is widely used to estimate sediment loads by multiplying soil loss through the Revised Universal Equation (RUSLE). In this study, the SDR equation was developed for the Lake Imha watershed using soil loss calculated by RUSLE and sediment loads by the calibrated Hydrological Simulation. Program Fortran (HSPF). The ratio of watershed relief and channel length ($R_f/L_{ch}$), the ratio of watershed relief and watershed length ($R_f/L_b$), curve number (CN), area (A), and channel slope ($SLP_{ch}$) demonstrated strong correlations with SDR. SDR equations were developed by a combination of subwatershed parameters by referring to the correlation analysis. The area based power functional SDR developed in this study showed significant errors at the point right after entering major tributaries, because SDR was unrealistically reduced when the watershed area increased significantly. The $SLP_{ch}$-based power functional SDR also showed extraordinary values when the channel slope was gradual. The SDR equation that showed the highest value of the coefficient of determination also presented unrealistic changes in the sediment loads within a relatively short river distance. The SDR equation $SDR=0.0003A^{0.198}R_f/L{_w}^{1.167}$ was recommended for application to the Lake Imha watershed. Using this equation, sediment loads at the outlet of the Lake Imha watershed were calculated, and the HSPF parameters related to sediment in the uncalibrated subwatersheds were determined by referring to the sediment loads calculated with the SDR equation.