• Journal of the Korean Society for Nondestructive Testing
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• v.21 no.5
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• pp.549-555
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• 2001

Ultrasonic is a powerful nondestructive technique for getting the information of flaws and material properties of in-services facilities. We prepared 4 different 1Cr-1Mo-0.25V specimens by Isothermal aging at $630^{\circ}C$. We evaluated material degradation using ultrasonic parameters, velocity, attenuation and harmonic generation. Attenuation and nonlinear parameter derived from harmonic generation efficiency increased as degradation. Especially the second harmonic of the fundamental wave in the 1,820h aging material was observed to exceed 20dB more than that in the un-aged material. But velocity remained virtually the same for all specimens. We concluded that nonlinear parameter and attenuation are sensitive to material degradation, but velocity was not. It'll be a good parameter for evaluating the material degradation.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.20 no.9
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• pp.2819-2832
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• 1996

The estimation of the remaining life for the aged components in power plant as well as chemical and petroleum plants has been recently concerned. The raw materials used in this study are the 1Cr-1Mo-0.25V steel which intensified P and S compositions along with the nominal compositions of ASTM A 470 standard. Five kinds of specimens with the different degradation levels were prepared by isothermal aging heat treatment at 630.deg.C. The mechanical properties and rotated bending fatigue strength of virgin and aged 1Cr-1Mo-0.25V steel have been investigated through the hardness, tensile, fatigue test, SEM fractograph and EDS analysis at 538.deg.C and room temperature, respectively. Thus the data of aged specimens were compared with those of virgin specimen to evaluate the aging effects. The main results obtained in this study are as follows ; The decrease of the yield and tensile strength due to degradation was distinguished until 50, 000hrs simulated service time. And it was confirmed that the considerable amount of P, Mn, Cr and S was precipitated at the grain boundary of aged material through the SEM and EDS analysis. The rotated bendingd fatigue strength at 538.deg.C of virgin, 25, 000, 50, 000, 75, 000 and 100, 000 hrs aged material was decreased 44.6 %, 49.6 %, 51.5 %, 52.4% and 53.8% than that of virgin material at 10$_{7}$cycles of room temperature, respectively. The major cracks of virgin and aged materials mainly initiated at the inclusions including Si, P and Mn compositions which were located at the outer periphery of the specimen.n.

• Journal of Ocean Engineering and Technology
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• v.10 no.2
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• pp.77-87
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• 1996

The estimation of the remaining life for the aged components in power plant as well as chemical and peroleum plants has been recently coberned. The raw materials used in this syudy are the 1Cr-1Mo-0.25V rotor steel which intensified P and S compositions along with the nominal compositions of ASTM A470 standard. Five kinds of specimens with the different degradation levels were prepared by isothermal aging teat treatment at $630^{\circ}C$ The mechanical properties and fatigue strength of virgin and aged 1Cr-1Mo-0.25V rotor steel have been inbestigated through the hardness, tensile, fatigue test, SEM fractograph and EDS analysis at room temperature. Thus, the data of aged specimens were compared with those of virgin specimen to evaluate the aging effects. The main results obtained in this study are as follows; The decrease of the hardness due to degradation was distinguished until 50, 000hrs simulated service time. And is was confirmed that the considerable amount of P, Mn, Cr and S was precipitated at the grain boundary of aged material through the SEM and EDS analysis. The fatigue strength of 25, 000, 50, 000, 75, 000 and 100, 000hrs aged material was decreased 29.5%, 24.4%, 28.6%, 35.7% than that of virgin material at $10^7$ cycles of room temperature. The major cracks of virgin and aged materials initiated at the inclusions including Si, P and Mn compositions which were located at the outer periphery of the specimen.

• Transactions of the Korean Society of Mechanical Engineers
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• v.18 no.11
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• pp.2860-2870
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• 1994

When crack are detected in aged turbine rotors of power plants, information on fracture resistance of the aged material at operating temperature is needed for determination of critical loading condition and residual life of the turbine. In this study, fracture toughness (J$_lc$) and tearing modulus(T$_mat$) of virgin and thermally degraded 1Cr-1Mo-0.25V steel, which is one of the most widely used rotor steels, were measured at 538.deg. C according to ASTM E813 and ASTM E1152, respectively. Five kinds of specimen with different degradation levels were prepared by isothermal aging heat treatment at $630^{\circ}C.$ It was observed that J$_lc$ and T$_mat$ value decreased as the degradation level increased. Analysis of microstructures using a scanning electron microscope showed that the decrement of J$_lc$ is related to segregation of impurities at grain boundaries. It was also verified that the DC electric potential drop method is accurate and reliable for crack length monitoring at elevated temperature.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2002.07a
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• pp.226-231
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• 2002

The present study discusses the results of the controlled precipitation of HgTe nanocrystals in a PbTe semiconductor matrix and demonstrates its effectiveness in producing well-organized and crystallographically aligned semiconductor nanocrystals. Following the similar procedure used in metallic alloys, the semiconductor alloys are treated at 600$^{\circ}C$ for 48 hours, quenched and aged up to 500 hours at 300$^{\circ}C$ and 450$^{\circ}C$ to induce homogeneous nucleation and growth of HgTe nanocrystalline precipitates. Examination of the resulting precipitates using transmission electron microscopy (TEM) and high resolution TEM (HRTEM) reveals that the coherent HgTe precipitates form as thin discs along the {100} habit planes making a crystallographic relation of {100}$\sub$HgTe///{100}$\sub$PbTe/ and [100]$\sub$HgTe///[100]$\sub$PbTe/. It is also found that the nato-disc undergoes a gradual thickening and a faceting under isothermal aging up to 500 hours without any noticeable coarsening. These results, combined with the extreme dimension of the precipitates (4 nm in length and sub-nanometer in thickness) and the simplicity of the formation process, leads to the conclusion that controlled precipitation is an effective method for the preparation of the desirable quantum-dot nanostructures.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.26 no.7
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• pp.1262-1269
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• 2002

It is inevitable to evaluate the life of turbine rotor because the operating periods of power plants need to be extended. For the test, seven kinds of specimens with different degradation levels were prepared by the isothermal heat treatment at $630^{\circ}C$. Magnetic methods utilizing Barkhausen noise coercive force($BN_c$) were applied to detect the degradation caused by thermal aging. Magnetic property of material is related with domain dynamics and that is affected by the microstructure of material. Therefore $BN_c$ is very sensitive to the microstructure change of the material. With the increase of degradation, $BN_c$ was decreased and this phenomenon is considered due to precipitations and grain size. The result was compared with Vickers hardness($H_v$) and coercive force($H_c$) to detect the relative variation, and was related with $H_v$ and YS to estimate the change of the mechanical properties with the degradation.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.24 no.12
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• pp.2995-3002
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• 2000

The remaining life estimation for the aged components in power plants as well as chemical plants are very important beacuse mechanical properties of the components are degraded with time of service exposure in high temperature. Since it is difficult to take specimens from the operating components to evaluate mechanical properties of components nondestructive techniques are needed to estimate the degradation. In this study, test materials with 4 different degradation levels were prepared by isothermal aging heat treatment at 630$\^{C}$. And the DC potential drop method and destructive methods such as tensile, K(sub)IC and hardness tests were used in order to evaluate the degradation of 1-Cr-1Mo-0.25V steels. The objective of this study is to investigate the possibility of the application of DCPD method to estimated the material degradation, and to analyse the relationship between the electrical relationship between the electrical resistivity and the degree material degradation.

• Proceedings of the KSME Conference
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• 2001.06a
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• pp.250-255
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• 2001

It is inevitable to evaluate the life of turbine rotor because the operating periods of power plants need to be extended. The magnetic methods utilizing Magnetic Barkhausen noise curve were applied to detect the degradation caused by thermal aging. The Magnetic property of material depends on the domain dynamics and it is affected by the microstructure of material. Therefore the magnetic property is very sensitive to the microstructure change of the material. It is, thus, very useful to detect the state of degradation of varying materials. The test specimen made of 1Cr-1Mo-0.25V steel was used widely for turbine rotor material, and seven kinds of specimens with different degradation levels were prepared by the isothermal heat treatment at $630^{\circ}C$. With the increase of degradation, BHN was decreased. The result was compared with coercive force and vickers hardness.

• Current Photovoltaic Research
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• v.5 no.3
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• pp.83-88
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• 2017

The growth of intermetallic compounds is an important factor in the reliability of solar cells. Especially, the temperature change in the soldering process greatly affects the thickness of the intermetallic compound layer. In this study, we investigated the intermetallic compound growth by Sn-diffusion in solder joints of solar cells. The thickness of the intermetallic compound layer was analyzed by IR lamp power and hot plate temperature control, and the correlation between the intermetallic compound layer and the adhesive strength was confirmed by a $90^{\circ}$ peel test. In order to investigate the growth of the intermetallic compound layer during isothermal aging, the growth of the intermetallic compound layer was analyzed at $85^{\circ}C$ and 85% for 500 h. In addition, the activation energy of Sn was calculated. The diffusion coefficient of the intermetallic compound layer was simulated and compared with experimental results to predict the long-term reliability.

• Journal of Welding and Joining
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• v.20 no.5
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• pp.93-98
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• 2002

The effect of bonding misfit on single crystallization of transient liquid phase (TLP) bonded joints of single crystal superalloy CMSX-2 was investigated using MBF-80 insert metal. The bonding misfit was defined by (100) twist angle (rotating angle) at bonded interface. TLP bonding of specimens was carried out at 1523K for 1.8ks in vacuum. The post-bond heat treatment consisted of the solution and sequential two step aging treatment was conducted in the Ar atmosphere. The crystallographic orientation analysis across the TLP bonded joints was conducted three dimensionally using the electron back scattering pattern (EBSP) method. EBSP analyses f3r the bonded and post bonded heat treated specimens were conducted. All bonded joints had misorientation centering around the bonded interface for as-bonded and post-bond heat treated specimens with rotating angle. The average misorientation angle between both solid phases in bonded interlayer was almost identical to the rotating angle at bonded interface. HRTEM observation revealed that the atom arrangement of both solid phases in bonded interlayer was quite different across the bonded interface. It followed that grain boundary was formed in bonded interface. It was confirmed that epitaxial growth of the solid phase occurred from the base metal substrates during TLP bonding and single crystallization could not be achieved in joints with rotating angle.