• Progress in Medical Physics
• /
• v.24 no.4
• /
• pp.253-258
• /
• 2013

The purpose of this study is to evaluate and analyze the relationship between the external radiation dose reconstruction which is transmitted from the patient who receives radiation treatment through electronic portal imaging device (EPID) and the internal dose derived from the Monte Carlo simulation. As a comparative analysis of the two cases, it is performed to provide a basic indicator for similar studies. The geometric information of the experiment and that of the radiation source were entered into Monte Carlo n-particle (MCNPX) which is the computer simulation tool and to derive the EPID images, a tally card in MCNPX was used for visualizing and the imaging of the dose information. We set to source to surface distance (SSD) 100 cm for internal measurement and EPID. And the water phantom was set to be 100 cm of the source to surface distance (SSD) for the internal measurement and EPID was set to 90 cm of SSD which is 10 cm below. The internal dose was collected from the water phantom by using mesh tally function in MCNPX, accumulated dose data was acquired by four-portal beam exposures. At the same time, after getting the dose which had been passed through water phantom, dose reconstruction was performed using back-projection method. In order to analyze about two cases, we compared the penetrated dose by calibration of itself with the absorbed one. We also evaluated the reconstructed dose using EPID and partially accumulated (overlapped) dose in water phantom by four-portal beam exposures. The sum dose data of two cases were calculated as each 3.4580 MeV/g (absorbed dose in water) and 3.4354 MeV/g (EPID reconstruction). The result of sum dose match from two cases shows good agreement with 0.6536% dose error.

• Food Science and Biotechnology
• /
• v.14 no.4
• /
• pp.456-460
• /
• 2005

To enforce the maximum residue limit for residual hexane (0.005 g/kg) in commercially available Korean vegetable oil, convenient and accurate quantification methods were investigated. Using dual surrogate standards, pentane and heptane were dissolved in ethanol, and then added to hexane-tree sunflower oil for setting up the calibration curve. Gas Chromatograph-Flame Ionization Detector with a porous layer open tubular column, indicated good chromatographic separation of hexane from other inhibiting matrix components. The lowest calibration level was $0.5\;{\mu}g/g$, not exceeding a relative standard deviation of 10% (RSD%), and 1.0\;{\mu}g/g$ not exceeding a deviation of 22% RSD% using heptane as an internal standard for the Static headspace analysis by using a headspace auto-sampler and manual injection, respectively. The residual hexane was detected in nine of the samples among 87 vegetable oil samples purchased on the local market.

• Journal of Institute of Control, Robotics and Systems
• /
• v.7 no.10
• /
• pp.837-842
• /
• 2001

In this paper, we design and implement the DC characteristic measurement system for semiconductor devices. The proposed system is composed of 4 SMU(Source and Measure Unit) channels. Various efforts in hardware and software have been made to reduce the measurement errors. Internal and external sources of errors in measurement system especially in pA range measurement have been identified and removed. Also, various digital signal processing techniques are developed. Calibration is executed under the control of microprocessor periodically. Experimental results show that the implemented system can measure the DC characteristic of semiconductor devices with less than 0.2% error in various voltage and current source/measurement range.

• KOREAN JOURNAL OF CROP SCIENCE
• /
• v.51 no.spc1
• /
• pp.304-309
• /
• 2006

Near infrared reflectance spectroscopy (NIRS) was used to develop a rapid and nondestructive method for the determination of fatty acid composition in sesame (Sesamum indicum L.) seed oil. A total of ninety-three samples of intact seeds were scanned in the reflectance mode of a scanning monochromator, and reference values for fatty acid composition were measured by gas-liquid chromatography. Calibration equations were developed using modified partial least square regression with internal cross validation (n=63). The equations obtained had low standard errors of cross-validation and moderate $R^2$ (coefficient of determination in calibration). Prediction of an external validation set (n=30) showed significant correlation between reference values and NIRS estimated values based on the SEP (standard error of prediction), $r^2$ (coefficient of determination in prediction) and the ratio of standard deviation (SD) of reference data to SEP. The models developed in this study had relatively higher values (more than 2.0) of SD/SEP(C) for oleic and linoleic acid, having good correlation between reference and NIRS estimate. The results indicated that NIRS, a nondestructive screening method could be used to rapidly determine fatty acid composition in sesame seeds in the breeding programs for high quality sesame oil.

• Transactions of the Korean Society of Pressure Vessels and Piping
• /
• v.10 no.1
• /
• pp.75-81
• /
• 2014

A simulation of eddy current testing has been utilized for predicting the signal characteristics to the various defects and developing the probes. Especially, CIVA which is a simulation tool dedicated to nondestructive testing has a good accuracy and speed, and provides a three-dimensional graphical user interface for improved visualization and familiar data displays consistent with NDE technique. Although internal validations have been performed by the CIVA software development specialists, an independent validation study is necessary for the accuracy assessment of the software prior to practical use. For this purpose, in this study, eddy current testing signals of ASME FBH calibration standard tube for bobbin probe were simulated using CIVA and the results were compared to the experimental inspected signals based on the relationship between each flaw signal in terms of amplitude and phase, and the shape of the Lissajous curve. And then we verified the accuracy of the simulated signals and the possible range for simulation. Overall, there is a good qualitative agreement between the CIVA simulated and experimental results in the absolute and differential modes at the two inspection frequencies.

• Transactions of the Korean Society of Pressure Vessels and Piping
• /
• v.9 no.1
• /
• pp.25-30
• /
• 2013

The periodic inspection of piping and pressure vessels welds in nuclear power plant has to provide reliable result related to weld flaws, such as location, maximum amplitude response, ultrasonic length, height and finally the nature or flaw pattern. The founded flaw in ultrasonic inspection is accepted or rejected based on these data. Specially, the amplitude of flaw response is used as basic parameter for flaw sizing and it may cause some deviation in length sizing result. Currently the ultrasonic inspections in nuclear power plant components are performed by specific inspection procedure which describing inspection technique include inspection system, calibration methodology and flaw characterizing. To perform ultrasonic inspection during in-service inspection, reference gain should be established before starting ultrasonic inspection by the requirement of ASME code. This reference gain used as basic criteria to evaluate flaw sizing. Sometimes, a little difference in establishing reference gain between calibration and field condition can lead to deviation in flaw sizing. Due to this difference, the inspection result may cause flaw sizing error. Therefore, the objective of this study is to compare and evaluate the ultrasonic amplitude difference between air filled and water filled pipe in nuclear power plant. Additionally, the accuracy of flaw sizing is estimated by comparing both conditions.

• Bulletin of the Korean Chemical Society
• /
• v.28 no.12
• /
• pp.2354-2358
• /
• 2007

MALDI-TOF-MS technique was applied to obtain structural and compositional information of synthetic polyamides, Nylon6 and Nylon66. Mass spectra of both the original and the hydrolyzed polyamide samples were analyzed using the self calibration method as well as the internal calibration method with the standard materials of known masses. The MALDI-TOF mass spectra of Nylon6 samples showed the presence of protonated, sodiated, and potassiated ions that were assigned to cyclic and NH2/COOH terminated linear oligomers. From the MALDI-TOF mass spectra of Nylon66 samples, the potassiated linear oligomers with three different end groups are identified as well as the cyclic oligomers, i.e., NH2/COOH terminated oligomers, NH2/NH2 terminated oligomers, and COOH/COOH terminated oligomers. Full characterization of the molecular species and end groups present in the polyamide samples has been achieved, and also the changes in mass spectral patterns after the hydrolysis of the samples are presented.

• Bulletin of the Korean Chemical Society
• /
• v.28 no.12
• /
• pp.2359-2362
• /
• 2007

MALDI-TOF-MS technique was applied to obtain structural and compositional information of synthetic polyamides, Nylon6 and Nylon66. Mass spectra of both the original and the hydrolyzed polyamide samples were analyzed using the self calibration method as well as the internal calibration method with the standard materials of known masses. The MALDI-TOF mass spectra of Nylon6 samples showed the presence of protonated, sodiated, and potassiated ions that were assigned to cyclic and NH2/COOH terminated linear oligomers. From the MALDI-TOF mass spectra of Nylon66 samples, the potassiated linear oligomers with three different end groups are identified as well as the cyclic oligomers, i.e., NH2/COOH terminated oligomers, NH2/NH2 terminated oligomers, and COOH/COOH terminated oligomers. Full characterization of the molecular species and end groups present in the polyamide samples has been achieved, and also the changes in mass spectral patterns after the hydrolysis of the samples are presented.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.30 no.10
• /
• pp.677-682
• /
• 2017

Lamination is used extensively in various industries. The type of lamination applied to the material depends on the precision level required, which varies for materials needed for everyday use, materials used in high-tech industries, and processes employed to fabricate finished products. Especially in hot lamination, the distribution of the surface temperature of the heating roller is very important to avoid the generation of internal bubbles and ensure flatness of the attached materials, and thus maintain a good standard of quality and productivity. In this study, we have developed a system to monitor the surface temperature of the heating rollerby applying a heterogeneous controller and a non - contact temperature sensor. This monitoring system accurately measures the surface temperature of the heating roller and applies the RS485 MODBUS communication method for easy expansion. Using this system, a laminated prototype was fabricated, and its efficacy for non-contact temperature sensor calibration, Ethernet IP communication, stoppage of the heating roller, and determination of temperature distribution with rotation was examined for its potential usage in industries.

• Bulletin of the Korean Chemical Society
• /
• v.32 no.2
• /
• pp.477-482
• /
• 2011

The structural analysis of polytrimethylene terephthalate (PTT) and characterization of the hydrolytic degradation products after acid hydrolysis were performed using MALDI-TOF mass spectrometry. Mass spectra of the PTT samples were analyzed using a self-calibration method as well as an internal calibration method with standard materials of known masses. PTT structures constituting the samples were determined from the analyses of the spectra, and their relative compositions were estimated. The MALDI-TOF mass spectra of the acid-hydrolyzed PTT sample showed three main series of oligomer products with different end groups in accordance with the hydrolysis schemes. From the spectra of both $Na^+$ and $K^+$ adducts, it was concluded that the PTT samples have higher affinity for $Na^+$ compared with $K^+$ and therefore show higher ionization efficiency with sodium ions when dithranol is used as a matrix. Two different wavelength laser beams ($\lambda$ = 337 nm and 355 nm) were tested and it was observed that the 355 nm beam was more efficient in obtaining the MALDI spectra of PTT using dithranol as a matrix under our experimental conditions.