• Title/Summary/Keyword: interfacial characteristic

Search Result 74, Processing Time 0.022 seconds

Mechanical and interfacial characterization of laser welded Co-Cr alloy with different joint configurations

  • Kokolis, John;Chakmakchi, Makdad;Theocharopoulos, Antonios;Prombonas, Anthony;Zinelis, Spiros
    • The Journal of Advanced Prosthodontics
    • /
    • v.7 no.1
    • /
    • pp.39-46
    • /
    • 2015
  • PURPOSE. The mechanical and interfacial characterization of laser welded Co-Cr alloy with two different joint designs. MATERIALS AND METHODS. Dumbbell cast specimens (n=30) were divided into 3 groups (R, I, K, n=10). Group R consisted of intact specimens, group I of specimens sectioned with a straight cut, and group K of specimens with a $45^{\circ}$ bevel made at the one welding edge. The microstructure and the elemental distributions of alloy and welding regions were examined by an SEM/EDX analysis and then specimens were loaded in tension up to fracture. The tensile strength (TS) and elongation (${\varepsilon}$) were determined and statistically compared among groups employing 1-way ANOVA, SNK multiple comparison test (${\alpha}$=.05) and Weibull analysis where Weibull modulus m and characteristic strength ${\sigma}_0$ were identified. Fractured surfaces were imaged by a SEM. RESULTS. SEM/EDX analysis showed that cast alloy consists of two phases with differences in mean atomic number contrast, while no mean atomic number was identified for welded regions. EDX analysis revealed an increased Cr and Mo content at the alloy-joint interface. All mechanical properties of group I (TS, ${\varepsilon}$, m and ${\sigma}_0$) were found inferior to R while group K showed intermediated values without significant differences to R and I, apart from elongation with group R. The fractured surfaces of all groups showed extensive dendritic pattern although with a finer structure in the case of welded groups. CONCLUSION. The K shape joint configuration should be preferred over the I, as it demonstrates improved mechanical strength and survival probability.

Preparation and Characterization of Pitch-based Carbon Paper for Low Energy and High Efficiency Surface Heating Elements (저전력 및 고효율 면상발열체를 위한 피치기반 탄소종이 제조 및 특성)

  • Yang, Jae-Yeon;Yoon, Dong-Ho;Kim, Byoung-Suhk;Seo, Min-Kang
    • Composites Research
    • /
    • v.31 no.6
    • /
    • pp.412-420
    • /
    • 2018
  • In this work, phenolic resins containing conductive carbon fillers, such as, petroleum coke, carbon black, and graphite, were used to improve the surface heating elements by impregnating a pitch-based carbon paper. The influence of conductive carbon fillers on physicochemical properties of the carbon paper was investigated through electrical resistance measurement and thermal analysis. As a result, the surface resistance and interfacial contact resistivity of the carbon paper were decreased linearly by impregnating the carbon fillers with phenol resins. The increase of carbon filler contents led to the improvement of electrical and thermal conductivity of the carbon paper. Also, the heating characteristics of the surface heating element were examined through the applied voltage of 1~5 V. With the applied voltage, it was confirmed that the surface heating element exhibited a maximum heating characteristic of about $125.01^{\circ}C$(5 V). These results were attributed to the formation of electrical networks by filled micropore between the carbon fibers, which led to the improvement of electrical and thermal properties of the carbon paper.

Evaluation of Microscopic Deformation Behaviors of Metal Matrix Composite due to Heat Treatment by means of SFC Test and Acoustic Emission (음향방출과 SFC 시험법에 의한 금속복합재료의 기지재 열처리 효과에 따른 미시적 변형기구 특성 평가)

  • Kang, Moon-Phil;Lee, Joon-Hyun
    • Journal of the Korean Society for Nondestructive Testing
    • /
    • v.20 no.5
    • /
    • pp.381-389
    • /
    • 2000
  • Metal matrix composite(MMCs) have been rapidly becoming one of the strongest candidates for structural materials for high temperature application. It is well recognized that MMCs always experience at least one large cool-down from processing temperature before my significant applied service loading. Due to the large difference in thermal expansion coefficient between the fiber and matrix, large thermal residual stresses generally develop in composites. It was reported from many previous studies that the effects of thermal residual stress on mechanical properties and fracture behavior were much more complex and dramatic than conventional engineering materials. Therefore it is crucial to evaluate the effect of heat treatment which changes the characteristic of distribution of thermal residual stress in MMCs. Single fiber composite(SFC) test based on the balance in a micromechanical model is a quite convenient method to evaluate interfacial shear strength(IFSS) and the failure mode of composite. In this study the effect of heat treatment on IFSS and the microscopic failure mechanism of MMC is investigated by combining acoustic emission(AE) technique with SFC test. The characteristic of AE signal, IFSS and microscopic failure mechanism due to heat treatment condition is discussed.

  • PDF

Experimental study on air-water countercurrent flow limitation in a vertical tube based on measurement of film thickness behavior

  • Wan, Jie;Sun, Wan;Deng, Jian;Pan, Liang-ming;Ding, Shu-hua
    • Nuclear Engineering and Technology
    • /
    • v.53 no.6
    • /
    • pp.1821-1833
    • /
    • 2021
  • The gas-liquid counter-current flow limitation (CCFL) is closely related to efficient and safety operation of many equipment in industrial cycle. Air-water countercurrent flow experiments were performed in a tube with diameter of 25 mm to understand the triggering mechanism of CCFL. A parallel electrode probe was utilized to measure film thickness whereby the time domain and frequency domain characteristics of liquid film was obtained. The amplitude of the interface wave is small at low liquid flow rate while it becomes large at high liquid flow rate after being disturbed by the airflow. The spectral characteristic curve shows a peak-shaped distribution. The crest exists between 0 and 10 Hz and the amplitude decreases with the frequency increase. The analysis of visual observation and characteristic of film thickness indicate that two flooding mechanisms were identified at low and high liquid flow rate, respectively. At low liquid flow rate, the interfacial waves upward propagation is responsible for the formation of CCFL onset. While flooding at high liquid flow rate takes place as a direct consequence of the liquid bridging in tube due to the turbulent flow pattern. Moreover, it is believed that there is a transition region between the low and high liquid flow rate.

An Experimental Research About Settling and Consolidation Characteristic of Dredged Soil in West Coast (서해안 준설토의 침강압밀특성에 관한 실험적 연구)

  • Lee, Seung-Ho;Lee, Jeong-Hak
    • Journal of the Korean GEO-environmental Society
    • /
    • v.12 no.5
    • /
    • pp.29-36
    • /
    • 2011
  • In this study, settling experiment was performed about cohesive and sandy soils among representative sample expected to dredge and dump for analysis of settling and consolidation characteristic. The analysis showed the definite difference between cohesive soils and sandy soils of relationships with settling and consolidation coefficient, a water content, interfacial heights. But directly after a dredged reclamation, prediction results about a initial volume change showed that cohesive soil of a water content change was decreased rapidly as time goes by, but sandy soils made no difference in a water content change. Results were compared and analyzed with the settling and consolidation coefficient and a initial settling velocity by real soil amounts for a feasibility check about test conditions applied to these experiment: we judge that test conditions are appropriate, each material by such these analyses suggests the scope of settling and consolidation coefficient, average and the representative relational formula.

Partitioned coupling strategies for fluid-structure interaction with large displacement: Explicit, implicit and semi-implicit schemes

  • He, Tao
    • Wind and Structures
    • /
    • v.20 no.3
    • /
    • pp.423-448
    • /
    • 2015
  • In this paper the unsteady fluid-structure interaction (FSI) problems with large structural displacement are solved by partitioned solution approaches in the arbitrary Lagrangian-Eulerian finite element framework. The incompressible Navier-Stokes equations are solved by the characteristic-based split (CBS) scheme. Both a rigid body and a geometrically nonlinear solid are considered as the structural models. The latter is solved by Newton-Raphson procedure. The equation governing the structural motion is advanced by Newmark-${\beta}$ method in time. The dynamic mesh is updated by using moving submesh approach that cooperates with the ortho-semi-torsional spring analogy method. A mass source term (MST) is introduced into the CBS scheme to satisfy geometric conservation law. Three partitioned coupling strategies are developed to take FSI into account, involving the explicit, implicit and semi-implicit schemes. The semi-implicit scheme is a mixture of the explicit and implicit coupling schemes due to the fluid projection splitting. In this scheme MST is renewed for interfacial elements. Fixed-point algorithm with Aitken's ${\Delta}^2$ method is carried out to couple different solvers within the implicit and semi-implicit schemes. Flow-induced vibrations of a bridge deck and a flexible cantilever behind an obstacle are analyzed to test the performance of the proposed methods. The overall numerical results agree well with the existing data, demonstrating the validity and applicability of the present approaches.

INTERCONNECTION TECHNOLOGY IN ELECTRONIC PACKAGING AND ASSEMBLY

  • Wang, Chunqing;Li, Mingyu;Tian, Yanhong
    • Proceedings of the KWS Conference
    • /
    • 2002.10a
    • /
    • pp.439-449
    • /
    • 2002
  • This paper reviews our recent research works on the interconnection technologies in electronic packaging and assembly. At the aspect of advanced joining methods, laser-ultrasonic fluxless soldering technology was proposed. The characteristic of this technology is that the oxide film was removed through the vibration excitated by high frequency laser change in the molten solder droplet. Application researches of laser soldering technology on solder bumping of BGA packages were carried out. Furthermore, interfacial reaction between SnPb eutectic solder and Au/Ni/Cu pad during laser reflow was analyzed. At the aspect of soldered joints' reliability, the system for predicting and analyzing SMT solder joint shape and reliability(PSAR) has been designed. Optimization design method of soldered joints' structure was brought forward after the investigation of fatigue failure of RC chip devices and BGA packages under temperature cyclic conditions with FEM analysis and experimental study. At the aspect of solder alloy design, alloy design method based on quantum was proposed. The macroproperties such as melting point, wettability and strength were described by the electron parameters. In this way, a great deal of the experimental investigations was replaced, so as to realize the design and research of any kinds of solder alloys with low cost and high efficiency.

  • PDF

A Study on Mechanical Properties of Wood-Polymer Composites due to Environmental Characteristic (목재 고분자 복합재료의 환경 특성에 따른 기계적 물성연구)

  • Lee, Joong-Hee;Jeon, Sang-Jin;Heo, Seok-Bong;Kim, Hong-Gun
    • Proceedings of the Korean Society For Composite Materials Conference
    • /
    • 2005.11a
    • /
    • pp.91-94
    • /
    • 2005
  • Polypropylene as a matrix has been used for wood polymer composites(WPC). In preparing WPC, the coupling agent, Polypropylene grafted Maleic Anhydride(PP-G-MA) was used in order to obtain a good interfacial bonding force between matrix and fillers and dispersion of wood powders. In this study, the effects of wood powder contents and water absorption on the mechanical properties were experimentally investigated. The tensile strength and flexural strength of composites reached its peak value when the wood powder content was around 60 wt%. However, the peak value of the impact was observed about 30 wt% of wood powder content. The tensile strength and flexural strength increase with increasing the wood power contents. But the impact strength decrease with increasing the wood powder contents. The slight change was observed with the water absorption in the WPC. The optimal condition of the compositions such as Anti-oxidant and UV stabilizers for the outdoor application was suggested in this research.

  • PDF

Inverse Heat Transfer Analysis at the Mold/Casting Interface in the Aluminum Alloy Casting Process with Precision Metal Mold (정밀금형 알루미늄 합금주조공정시 주물/금형 접촉면에서의 Inverse 열전달해석에 관한 연구)

  • Moon, Su-Dong;Kang, Shin-Ill
    • Journal of Korea Foundry Society
    • /
    • v.18 no.3
    • /
    • pp.246-253
    • /
    • 1998
  • Precision metal mold casting process is a casting method manufacturing mechanical elements with high precision, having heavy/light alloys as casting materials and using permanent mold. To improve dimensional accuracy and the final mechanical properties of the castings, the solidification speed and the cooling rate of the casting should be controlled with the optimum mold cooling system, and moreover, to obtain more accurate control of the whole process interfacial heat transfer characteristic at the mold/casting interface must be studied in advance. In the present study, aluminum alloy casting system with metal mold equipped with electrical heating elements and water cooling system was designed and the temperature histories at points inside the metal mold were measured during the casting process. The heat transfer phenomena at the mold/casting interface was characterized by the heat flux between solidifying casting metal and metal mold, and the heat flux history was obtained using inverse heat conduction method. The effect of mold cooling condition upon the heat flux profile was examined, and the analysis shows that the heat flux value has its maximum at the beginning of the process.

  • PDF

Frequency-dependent electrical properties of $C_22$ -quinolinium(TCNQ) langmuir-blodgett films (C$_22$ -quinolinium(TCNQ) LB막의 주파수에 따른 전기적 특성)

  • 김태완;이상국;신동명;강도열
    • Electrical & Electronic Materials
    • /
    • v.8 no.2
    • /
    • pp.151-157
    • /
    • 1995
  • Frequency-dependent electrical properties of $C_{22}$-Quinolinium(TCNQ) LB films were investigated in a frequency range of 10[Hz]-13[MHz] along a perpendicular direction. The films were heat-treated to understand an electrodynamic response in a temperature range of 20-240[.deg. C]. Frequencydependent dielectric constants show that there are two characteristic dispersions; one is a dispersion occuring near 1[MHz] coming from the orientational polarization of the molecules and the other one is an interfacial polarization effect below 1[kHz] or so when the annealing temperature is above 80 [.deg. C]. The overall frequency-dependent dielectric constant is higher near 80[.deg. C]. It may be due to a softness of the alkyl chains. Several other methods were employed to identify the internal structure change of the films. DSC(differential scanning calorimetry) data of the $C_{22}$-Quinolinium(TCNQ) molecules shows that there is an endothermic process near 110[.deg. C] and a weak exothermic process near 180[.deg. C]. While the endothermic process is related to a disordering of the alkyl chains, the exothermic process seems to be due to a chemical structure change of the TCNQ molecules. Thickness measurement by ellipsometry shows that there is a thickness drop near 100[.deg. C], and the thickness above 120[.deg. C] becomes around 20[%] of the room-temperature value.lue.

  • PDF